IP Library Granted Patent US 10,450,652
Granted Patent B2
US 10,450,652 · App. 15/487,696 · Granted Oct 22, 2019

Synthesis of structured carbon material from organic materials

Inventors: Haitao Liu (Pittsburgh, PA); Feng Zhou (New York, NY)
Assignee: University of Pittsburgh—Of the Commonwealth System of Higher Education
C23C16/45525C01B32/90C23C16/403C23C18/1283C01P2002/82C01P2004/04
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Quick Facts
Patent No.
US 10,450,652
App. No.
15/487,696
Granted
Oct 22, 2019
Kind
B2
Abstract

A method of forming a carbonized composition includes providing an organic composition, forming a protective layer over the organic composition, increasing temperature to carbonize the organic composition and for a period of time to form the carbonized composition, and removing the protective layer from the carbonized composition.

Claims (19)

1. A method of forming a carbonized composition, comprising:

providing an organic composition comprising a nucleic acid;

forming a protective layer over the organic composition;

increasing temperature to carbonize the organic composition and for a period of time to form the carbonized composition; and

removing the protective layer from the carbonized composition.

2. The method of claim 1 wherein the organic composition consists of a nucleic acid.

3. The method of claim 1 wherein the nucleic acid is DNA.

4. The method of claim 1 wherein the nucleic acid is formed to have a predetermined shape or conformation.

5. The method of claim 4 wherein the predetermined shape or conformation of the nucleic acid is substantially maintained in the carbonized composition.

6. The method of claim 5 wherein the nucleic acid is deposited upon a substrate before forming the protective layer over the organic composition.

7. The method of claim 1 wherein the carbonized composition is a porous carbon material.

8. The method of claim 1 wherein the temperature is increased to a temperature within the range of approximately 780° C. to approximately 2072° C.

9. The method of claim 1 wherein the protective layer is deposited via a thin film deposition technique.

10. The method of claim 9 wherein the protective layer is deposited via atomic layer deposition, vacuum deposition, sputtering, chemical vapor deposition or laser assisted deposition.

11. The method of claim 10 wherein the protective layer is deposited via atomic layer deposition.

12. The method of claim 9 wherein the thickness of the protective layer is in the range of 2 nm to 100 micrometers.

13. The method of claim 1 wherein the protective layer comprises Al 2 O 3 .

14. The method of claim 13 wherein the protective layer is removed via etching with H 3 PO 4 .

15. The method of claim 1 wherein the protective layer is impermeable to decomposition gases of the organic composition during carbonization.

Assignments (4)
GOVERNMENT INTEREST AGREEMENT Recorded Oct 1, 2025
From: UNIVERSITY OF PITTSBURGH
To: THE GOVERNMENT OF THE UNITED STATES OF AMERICA AS REPRESENTED BY THE SECRETARY OF THE NAVY
Reel/Frame 072984/0762 →
GOVERNMENT INTEREST AGREEMENT Recorded Sep 18, 2025
From: UNIVERSITY OF PITTSBURGH
To: THE GOVERNMENT OF THE UNITED STATES OF AMERICA AS REPRESENTED BY THE SECRETARY OF THE NAVY
Reel/Frame 072889/0852 →
CONFIRMATORY LICENSE Recorded Jan 13, 2020
From: PITTSBURGH, UNIVERSITY OF
To: NAVY, SECRETARY OF THE UNITED STATES OF AMERICA
Reel/Frame 052268/0957 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 10, 2017
From: LIU, HAITAO; ZHOU, FENG
To: PITTSBURGH, UNIVERSITY OF - OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION
Reel/Frame 042323/0695 →
Continuity (2)
Provisional Application 62322337 · Apr 14, 2016
Related Publication 20170298517A1 · Oct 19, 2017
Cited By (1)
US 12,590,000