IP Library Granted Patent US 10,240,258
Granted Patent B2
US 10,240,258 · App. 15/509,918 · Granted Mar 26, 2019

Thermal energy storage and heat insulation polyester fiber, and preparation method therefor

Inventors: Sung Jin Oh (Anyang-si, KR); Min Suk Lee (Anyang-si, KR)
Assignee: HYOSUNG TNC CORPORATION
D01F1/02C08K3/2279D01F1/10D01F6/62
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Quick Facts
Patent No.
US 10,240,258
App. No.
15/509,918
Granted
Mar 26, 2019
Kind
B2
Abstract

The present invention is directed to a method for preparing a polyester fiber, the method including: mixing 5-50 wt % of composite metal oxide particles, including a tungsten-based oxide, a cesium-based oxide, an antimony-based oxide, an indium-based oxide, and a tin-based oxide, with 40-90 wt % of one or two types of organic solvents selected from among alcohol, ketone, and acetates, 0.4-20 wt % of polyvinyl butyral, i.e., polymer, and 2-30 wt % of calcium stearate or magnesium stearate to obtain a mixture, and stirring and grinding the mixture to prepare a dispersion liquid; drying the dispersion liquid to prepare a powdered additive; mixing 1-30 wt % of the additive with polyester chips to obtain a mixture and melting this mixture to prepare master batch chips; and mixing 1-10 wt % of the master batch chips with general polyester chips to obtain a mixture, and melting and spinning this mixture.

Claims (14)

1. A polyester fiber comprising 0.01-2 wt % of composite metal oxide particles in which a tungsten-based oxide, a cesium-based oxide, an antimony-based oxide, an indium-based oxide, and a tin-based oxide are mixed.

2. The polyester fiber of claim 1 , wherein the composite metal oxide particles comprise, based on 100 parts by weight of WO 3 , 3-20 parts by weight of Cs 2 O, 1-10 parts by weight of Sb 2 O 3 , 0.5-5 parts by weight of In 2 O 3 , and 0.1-1 part by weight of SnO 2 .

3. The polyester fiber of claim 1 , wherein the polyester fiber has a single-fiber fineness of 0.5-3 denier.

4. A fabric product using a polyester fiber, wherein the polyester fiber is the polyester fiber set forth in claim 1 .

5. A method for preparing a polyester fiber, the method comprising:

mixing 5-50 wt % of composite metal oxide particles, including a tungsten-based oxide, a cesium-based oxide, an antimony-based oxide, an indium-based oxide, and a tin-based oxide, with 40-90 wt % of one or two types of organic solvents selected from among alcohol, ketone, and acetates, 0.4-20 wt % of polyvinyl butyral, i.e., polymer, and 2-30 wt % of calcium stearate or magnesium stearate to obtain a mixture, and stirring and grinding the mixture to prepare a dispersion liquid;

drying the dispersion liquid to prepare a powdered additive;

mixing 1-30 wt % of the additive with polyester chips to obtain a mixture and melting this mixture to prepare master batch chips; and

mixing 1-10 wt % of the master batch chips with general polyester chips to obtain a mixture, and melting and spinning this mixture.

6. The method of claim 5 , wherein the composite metal oxide particles comprise, based on 100 parts by weight of WO 3 , 3-20 parts by weight of Cs 2 O, 1-10 parts by weight of Sb 2 O 3 , 0.5-5 parts by weight of In 2 O 3 , and 0.1-1 part by weight of SnO 2 .

7. The method of claim 5 , wherein the polyester chips used in the preparation of the master batch chips have an intrinsic viscosity of 0.60-0.70 dl/g.

8. The method of claim 5 , wherein the additive included in the master batch chips has an average particle size of 2 μm or less.

9. The method of claim 5 , wherein the organic solvents are a mixture of one or two types of materials selected from among alcohol, ketone, and acetone.

10. The method of claim 5 , wherein the spinning of the mixture is performed using a spinning nozzle having a C-shaped cross section.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 17, 2020
From: RAI, DEVNDRA; DIAZ-SAN SEGUNDO, FAYNA
To: THE UNIVERSITY OF CONNECTICUT
Reel/Frame 053513/0487 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2018
From: HYOSUNG CORPORATION
To: HYOSUNG TNC CORPORATION
Reel/Frame 047841/0033 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2017
From: OH, SUNG JIN; LEE, MIN SUK
To: HYOSUNG CORPORATION
Reel/Frame 041925/0650 →
Priority Claims (1)
KR 10-2014-0129230 · Sep 26, 2014 · national
Continuity (1)
Related Publication 20170306530A1 · Oct 26, 2017