IP Library Granted Patent US 11,072,770
Granted Patent B2
US 11,072,770 · App. 15/517,242 · Granted Jul 27, 2021

Compact reactor for enzymatic treatment

Inventor: Lars Aglen (Lysöysundet, NO)
Assignee: NUAS TECNOLOGY AS
C12M21/18C12M23/06C12M23/58C12M29/06C12M41/22C12M45/09C12M1/04
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Quick Facts
Patent No.
US 11,072,770
App. No.
15/517,242
Granted
Jul 27, 2021
Kind
B2
Abstract

Reactor for enzymatic hydrolysis of a raw material comprising in sequence: i)—a first heat exchanger adapted to heat the raw material supplied to the reactor to a temperature within a range that favours enzymatic hydrolysis, ii)—a reactor comprising plural in reactor chambers connected in series, separated by closable valves, iii)—a second heat exchanger adapted to heat the reaction mixture to a temperature higher than the temperature range favouring enzymatic hydrolysis, the reactor being formed with inclined tubular reactor chambers assembled to form a reactor with vertical axis, the first reactor chamber being the vertically uppermost chamber of the reactor, while at least one reactor chamber is adapted to be stirred with a through-flowing inert gas.

Claims (26)

1. A reactor for enzymatic hydrolysis of a material comprising in sequence:

a first heat exchanger (HEX 1 ) adapted to heat raw material to be supplied to the reactor to a first temperature within a range favouring enzymatic hydrolysis;

a reactor comprising a plurality of serially connected reactor chambers (R 1 -R 6 ) separated by closable airtight valves (V 1 -V 5 ), the reactor chambers being positioned at different vertical levels relative to one another;

a second heat exchanger (HEX 2 ) adapted to heat a reaction mixture to a temperature higher than the first temperature,

wherein a first reactor chamber (R 1 ) is positioned vertically above the other reactor chambers, and a last reactor chamber (R 6 ) is positioned vertically below the other reactor chambers and at least one of the reactor chambers is adapted to be stirred with a through-flowing inert gas introduced via a supply conduit ( 10 ), and wherein a return conduit ( 14 ) is configured to recycle the inert gas.

2. The reactor of claim 1 , wherein each reactor chamber has uniform size and shape and lies symmetric about a vertical axis.

3. The reactor of claim 1 , wherein said reactor chambers are tubular and inclined and connected so that the assembly is symmetrical about a vertical axis.

4. The reactor of claim 1 , wherein all of the reactor chambers are (R 1 -R 6 ) adapted to be stirred with through-flowing inert gas being supplied near a downstream end of the respective reactor chambers and discharged near the upstream end of the respective reactor chambers.

5. The reactor of claim 1 , wherein the reactor chambers (R 1 -R 6 ) are curved and assembled relative to one another to form a helix.

6. The reactor of claim 3 , wherein at least one of the first heat exchanger (HEX 1 ) and the second heat exchanger (HEX 2 ) is arranged along the vertical axis of the reactor.

7. The reactor of claim 3 , wherein the first heat exchanger (HEX 1 ) and a second heat exchanger (HEX 2 ) are arranged above each other along the vertical axis of the reactor.

8. The reactor of claim 5 , wherein the first heat exchanger (HEX 1 ) and the second heat exchanger (HEX 2 ) are arranged one above the other, concentrically within the helix.

9. The reactor of claim 1 , wherein at least one pasteurizing chamber (P 1 -P 3 ) is positioned downstream of the second heat exchanger (HEX 2 ).

10. The reactor of claim 9 , wherein the at least one pasteurizing chamber (P 1 -P 3 ) is a tubular chamber of substantially the same shape as reaction chambers (R 1 -R 6 ).

11. The reactor of claim 3 , further comprising an outer housing enclosing the reactor chambers and both heat exchangers.

12. The reactor of claim 1 , wherein the inert gas is adapted for recirculation and reuse.

13. The reactor of claim 3 , wherein the reactor chambers (R 1 -R 6 ) have an vertical/horizontal inclination of at least about 1/10.

14. The reactor of claim 1 , wherein each reactor chamber (R 101 - R 107 ) has the shape of a container having a simple, regular shape, and the reactor chambers are arranged vertically above each other with a first reactor chamber (R 101 ) vertically above the other reactor chambers and a last reactor chamber (R 107 ) vertically below the other reactor chambers.

15. The reactor of claim 14 , wherein each reactor chamber (R 101 -R 107 ) has a lowest point at a discharge point for the material in the reactor chamber.

16. The reactor of claim 14 , comprising a plurality of pasteurizing chambers (P 101 - P 103 ), wherein each pasteurizing chamber has the shape of a container with a regular shape and is arranged vertically above one other with a first pasteurizing chamber (P 101 ) being vertically above the other pasteurizing chambers and a last pasteurizing chamber (P 103 ) being vertically below the other pasteurizing chambers.

17. The reactor of claim 14 , comprising a plurality of pasteurizing chambers (P 101 - P 103 ), wherein a first heat exchanger (HEX 101 ) is connected upstream of the first reactor chamber (R 101 ) and wherein a second heat exchanger (HEX 102 ) is connected downstream of the last reactor chamber (R 107 ) and upstream of a first pasteurizing chamber (P 101 ).

18. The reactor of claim 14 , comprising a plurality of pasteurizing chambers (P 101 - P 103 ), wherein the reactor is grouped into four groups which are arranged independently of each other laterally adjacent to each other, the first heat exchanger (HEX 101 ) forming the first group, reactor chambers (R 101 -R 107 ) forming a second group, the second heat exchanger (HEX 102 ) forming the third group while the pasteurizing chambers (P 101 -P 103 ) form the fourth group.

19. The reactor of claim 1 , wherein each reactor chamber (Ri) is arranged for periodically being discharged via a supply of inert gas at an overpressure to each reactor chamber (Ri) and opening of downstream closable valve (Vi).

20. The reactor of claim 1 , wherein said first heat exchanger (HEX 1 , HEX 101 ) is configured to heat the material mixture to a temperature of about 50° C. and the second heat exchanger (HEX 2 , HEX 102 ) is configured to heat the material mixture to a temperature of at least about 90° C.

21. The reactor of claim 1 , wherein the reactor comprises or is adapted to be connected to a feed device ( 54 ) adapted to dispense a certain, adjustable amount of enzyme with a certain amount of raw material for hydrolysis.

22. The reactor of claim 1 , wherein the reactor is adapted to be stirred with nitrogen as inert gas.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE RECEIVING PARTY NAME PREVIOUSLY RECORDED ON REEL 056713 FRAME 0018. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF NAME. Recorded Sep 20, 2021
From: N OG U AS
To: NUAS TECHNOLOGY AS
Reel/Frame 057542/0794 →
CHANGE OF NAME Recorded Jun 22, 2021
From: N OG U AS
To: NUAS TECNOLOGY AS
Reel/Frame 056713/0018 →
CORRECTIVE ASSIGNMENT TO CORRECT THE RECEIVING PARTY NAME PREVIOUSLY RECORDED AT REEL: 41884 FRAME: 553. ASSIGNOR(S) HEREBY CONFIRMS THE ASSINGMENT. Recorded Jun 18, 2021
From: AGLEN, LARS
To: N OG U AS
Reel/Frame 056690/0462 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 6, 2017
From: AGLEN, LARS
To: N & U AS
Reel/Frame 041884/0653 →
Priority Claims (2)
NO 20141197 · Oct 7, 2014 · national
NO 20150943 · Jul 15, 2015 · national
Continuity (1)
Related Publication 20170306280A1 · Oct 26, 2017