IP Library Granted Patent US 10,612,128
Granted Patent B2
US 10,612,128 · App. 15/517,744 · Granted Apr 7, 2020

Sputtering target comprising Al—Te—Cu—Zr-based alloy and method of manufacturing same

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Quick Facts
Patent No.
US 10,612,128
App. No.
15/517,744
Granted
Apr 7, 2020
Kind
B2
Abstract

A sputtering target containing 20 at % to 40 at % of Te, 5 at % to 20 at % of Cu, 5 at % to 15 at % of Zr, and remainder being Al, wherein a structure of the sputtering target is comprise of an Al phase, a Cu phase, a CuTeZr phase, a CuTe phase and a Zr phase. The present invention aims to provide an Al—Te—Cu—Zr-based alloy sputtering target capable of effectively suppressing the degradation of properties caused by compositional deviation, as well as a method of manufacturing the same.

Claims (12)

1. A sputtering target containing 20 at % to 40 at % of Te, 5 at % to 20 at % of Cu, 5 at % to 15 at % of Zr, and remainder being Al, wherein a structure of the sputtering target is configured from an Al phase, a Cu phase, a CuTeZr phase, a CuTe phase and a Zr phase.

2. The sputtering target according to claim 1 , wherein the sputtering target has an average grain size of 1 μm to 50 μm, and a maximum grain size of 100 μm or less.

3. The sputtering target according to claim 2 , wherein the sputtering target has a purity of 3N or higher, and an oxygen content of 3000 wtppm or less.

4. The sputtering target according to claim 3 , wherein the sputtering target contains one or more elements selected among Si, C, Ti, Hf, V, Nb, Ta, lanthanoid elements, Ge, Zn, Co, Ni, Fe, Mg, Ga, S, and Se.

5. The sputtering target according to claim 4 , wherein the sputtering target has a relative density of 90% or more.

6. A method of manufacturing a sputtering target, wherein an Al raw material powder, a Te raw material powder, a Cu raw material powder, and a Zr raw material powder are weighed to achieve an intended composition, thereafter mixed, and an obtained mixed powder is subsequently sintered at 300° C. to 380° C. to produce a sputtering target containing 20 at % to 40 at % of Te, 5 at % to 20 at % of Cu, 5 at % to 15 at % of Zr, and remainder being Al, wherein a structure of the sputtering target is configured from an Al phase, a Cu phase, a CuTeZr phase, a CuTe phase and a Zr phase.

7. The method of manufacturing a sputtering target according to claim 6 , wherein raw material powders having an average grain size of 1 μm to 50 μm and a maximum grain size of 100 μm or less are used.

8. The method of manufacturing a sputtering target according to claim 7 , wherein sintering is performed in an argon atmosphere.

9. The method of manufacturing a sputtering target according to claim 6 , wherein sintering is performed in an argon atmosphere.

10. The sputtering target according to claim 1 , wherein the sputtering target has a purity of 3N or higher, and an oxygen content of 3000 wtppm or less.

11. The sputtering target according to claim 1 , wherein the sputtering target contains one or more elements selected among Si, C, Ti, Hf, V, Nb, Ta, lanthanoid elements, Ge, Zn, Co, Ni, Fe, Mg, Ga, S, and Se.

12. The sputtering target according to claim 1 , wherein the sputtering target has a relative density of 90% or more.

Assignments (2)
CHANGE OF ADDRESS Recorded Aug 11, 2021
From: JX NIPPON MINING & METALS CORPORATION
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 057160/0114 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 17, 2017
From: KOIDO, YOSHIMASA
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 042029/0588 →