IP Library › Granted Patent US 10,150,142
Granted Patent B2
US 10,150,142 · App. 15/545,803 · Granted Dec 11, 2018

Coating method for forming flame retardant substrate

Inventors: Jaime C. Grunlan (College Station, TX); Marcus Leistner (College Station, TX); Merid M. Haile (College Station, TX)
Assignee: The Texas A&M University System
B05D7/54B05D5/00B05D7/52B05D7/58C09D5/18C09D5/185C09D7/40C09D179/02C09D201/00C09D201/005C09K21/04C09K21/10C09K21/12D06M11/72D06M15/61B05D2505/00D06M2101/06D06M2200/30
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Quick Facts
Patent No.
US 10,150,142
App. No.
15/545,803
Granted
Dec 11, 2018
Kind
B2
Abstract

A method includes coating a substrate to provide a flame resistant substrate. In an embodiment, the method includes preparing an aqueous solution. The aqueous solution comprises a phosphate material, a cationic material, and a water. The method further includes exposing the substrate to the aqueous solution to produce a coating on the substrate. The coating includes the cationic material and the phosphate material. The method also includes exposing the coating on the substrate to a melamine solution.

Claims (23)

1. A method for coating a substrate to provide a flame resistant, coated substrate, comprising:

(A) preparing an aqueous solution, wherein the aqueous solution comprises a phosphate material, a cationic material, and a water;

(B) exposing the substrate to the aqueous solution to produce a coating on the substrate, wherein the coating comprises the cationic material and the phosphate material; and

(C) exposing the coating on the substrate to a solution comprising an amine, amide, or combinations thereof.

2. The method of claim 1 , wherein the aqueous solution comprises from about 0.01 wt. % cationic materials to about 30.0 wt. % cationic materials.

3. The method of claim 1 , wherein the aqueous solution comprises from about 0.01 wt. % phosphate materials to about 30.0 wt. % phosphate materials.

4. The method of claim 1 , wherein the substrate is exposed to the aqueous solution from about 1 second to about 24 hours.

5. The method of claim 1 , wherein the coated substrate has between about 5.0 wt. % coating and about 25 wt. % coating.

6. The method of claim 1 , wherein the coating is between about 10 nanometers and about 1,000 nanometers thick.

7. The method of claim 1 , wherein the substrate comprises foam, fabric, leather, vinyl compounds, plastic, glass, ceramic, metal, wood, carpet, hook and loop fasteners, non-foam padding, lapis, ducts, or any combinations thereof.

8. The method of claim 1 , wherein the aqueous solution further comprises an anionic material.

9. The method of claim 8 , wherein the anionic material comprises an anionic polymer, a colloidal particle, a sulfated molecule, a boronic acid, a boron containing acid, or any combinations thereof.

10. The method of claim 1 , wherein the phosphate material comprises polysodium phosphate, ammonium phosphate, ammonium polyphosphate, sodium hexametaphosphate, or any combinations thereof.

11. The method of claim 10 , wherein the phosphate material comprises polysodium phosphate.

12. The method of claim 1 , wherein the cationic material comprises a polymer, a colloidal particle, a nanoparticle, a nitrogen-rich molecule, or any combinations thereof.

13. The method of claim 12 , wherein the polymer comprises a cationic polymer, a polymer with hydrogen bonding, or any combinations thereof.

14. The method of claim 13 , wherein the cationic polymer comprises branched polyethylenimine, cationic polyacrylamide, cationic poly diallyldimethylammonium chloride, poly (melamine-co-formaldehyde), polymelamine, a copolymer of polymelamine, polyvinylpyridine, a copolymer of polyvinylpyridine, or any combinations thereof.

15. The method of claim 1 , wherein (C) comprises exposing the coating on the substrate to the solution comprising an amine, amide, or combinations thereof, exposing the coating on the substrate to a buffer solution, or both.

16. The method of claim 1 , further comprising (D) exposing the coating on the substrate to a buffer solution.

17. The method of claim 16 , further comprising (E) curing the coating on the substrate.

18. The method of claim 1 , wherein the coating further comprises an additive.

19. The method of claim 18 , wherein the additive comprises a crosslinker.

20. The method of claim 1 , wherein the solution comprising an amine, amide, or combinations thereof is a buffer solution.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 26, 2018
From: GRUNLAN, JAIME C.; LEISTNER, MARCUS; HAILE, MERID
To: THE TEXAS A&M UNIVERSITY SYSTEM
Reel/Frame 046979/0800 →
Continuity (2)
Provisional Application 62108893 · Jan 28, 2015
Related Publication 20180022939A1 · Jan 25, 2018
Cited By (1)
US 12,286,579