IP Library Granted Patent US 11,825,863
Granted Patent B2
US 11,825,863 · App. 15/558,153 · Granted Nov 28, 2023

Method for removing glucosinolates from oilseed meals

Inventors: Mark Hetherington (Saskatoon, CA); Travis Hoffman (Saskatoon, CA); Michael Lindenbaum (Beaconsfield, CA)
Assignees: AGRISOMA BIOSCIENCES INC.; NUSEED GLOBAL INNOVATION LTD.
A23K10/14A23K10/10A23K10/30A23K40/00A23K50/10A23L5/25A23N17/001A23N17/004A23N17/005A23N17/007C12N9/24
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Quick Facts
Patent No.
US 11,825,863
App. No.
15/558,153
Granted
Nov 28, 2023
Kind
B2
Abstract

A process to remove the glucosinolates of oilseed meals, such as Brassica carinata oilseed meals, is provided. In one embodiment, exogenous myrosinase is used to convert the glucosinolates to volatile isothiocyanate compounds, which can then be removed under conditions of mild heat and negative pressure. In another embodiment, heat and pressure are used to remove glucosinolates from Brassica carinata oilseed. The processed meals may contain less than 80% of their starting levels of glucosinolates and may be suitable for use in various applications, including as animal feeds.

Claims (17)

1. A process for producing a meal fraction of Brassica carinata oilseed having reduced sinigrin content, the method comprising:

a. pressing seeds of Brassica carinata oilseed to produce oilseed flakes;

b. cooking the oilseed flakes at a temperature in the range of 105° C. to 180° C.;

c. pressing the cooked oilseed flakes to remove oil from the oilseed flakes, thereby producing an oil fraction and a meal fraction;

d. treating the meal fraction with hexane to extract residual oil;

e. desolventizing-toasting the hexane-extracted meal fraction to remove residual hexane for a period of greater than 1 hour but less than 5 hours; and

f. drying the meal fraction to a moisture content of 12% or less, and

g. recovering a meal fraction of Brassica carinata having a sinigrin content of less than 20 μmol per gram of meal.

2. The process of claim 1 , wherein the sinigrin content of the meal fraction of Brassica carinata oilseed is less than 15 μmol per g of meal.

3. The process of claim 1 , comprising cooking the oilseed flakes at a temperature in the range of 105° C. to 150° C.

4. The process of claim 1 , comprising pressing the cooked oilseed flakes with an expeller or screw press.

5. The process of claim 1 , comprising desolventizing-toasting the hexane-extracted meal fraction at a temperature in the range of 95° C. to 115° C.

6. A meal fraction of Brassica carinata oilseed produced by the process of claim 1 .

7. A meal fraction of Brassica carinata oilseed produced by the process of claim 2 .

8. A meal fraction of Brassica carinata oilseed produced by the process of claim 3 .

9. A meal fraction of Brassica carinata oilseed produced by the process of claim 4 .

10. A meal fraction of Brassica carinata oilseed produced by the process of claim 5 .

Assignments (22)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 20, 2020
From: AGRISOMA BIOSCIENCES INC.
To: NUSEED GLOBAL INNOVATION LTD.
Reel/Frame 054109/0196 →
SECURITY INTEREST Recorded Sep 17, 2019
From: AGRISOMA BIOSCIENCES INC.
To: BDC CAPITAL INC.
Reel/Frame 050395/0072 →
SECURITY INTEREST Recorded Sep 17, 2019
From: AGRISOMA BIOSCIENCES INC.
To: PLAZA, JOHN
Reel/Frame 050395/0872 →
SECURITY INTEREST Recorded Sep 17, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CAPITAL REGIONAL ET COOPERATIF DESJARDINS
Reel/Frame 050395/0143 →
SECURITY INTEREST Recorded Sep 17, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CYCLE CAPITAL FUND III, L.P.
Reel/Frame 050395/0518 →
SECURITY INTEREST Recorded Sep 17, 2019
From: AGRISOMA BIOSCIENCES INC.
To: GESTION MANUIA INC.
Reel/Frame 050395/0432 →
SECURITY INTEREST Recorded Sep 17, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CAPITAL REGIONAL ET COOPERATIF DESJARDINS
Reel/Frame 050395/0355 →
SECURITY INTEREST Recorded Sep 17, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CYCLE CAPITAL FUND III, L.P.
Reel/Frame 050395/0646 →
SECURITY INTEREST Recorded Jan 31, 2019
From: AGRISOMA BIOSCIENCES INC.
To: BDC CAPITAL INC.
Reel/Frame 048199/0227 →
SECURITY INTEREST Recorded Jan 31, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CAPITAL RÉGIONAL ET COOPÉRATIF DESJARDINS
Reel/Frame 048199/0246 →
SECURITY INTEREST Recorded Jan 31, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CYCLE CAPITAL FUND III, L.P.
Reel/Frame 048199/0285 →
SECURITY INTEREST Recorded Jan 29, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CAPITAL RÉGIONAL ET COOPÉRATIF DESJARDINS
Reel/Frame 048162/0518 →
SECURITY INTEREST Recorded Jan 29, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CYCLE CAPITAL FUND III, L.P.
Reel/Frame 048162/0491 →
SECURITY INTEREST Recorded Jan 29, 2019
From: AGRISOMA BIOSCIENCES INC.
To: GESTION MANUIA INC.
Reel/Frame 048162/0529 →
SECURITY INTEREST Recorded Jan 25, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CAPITAL RÉGIONAL ET COOPÉRATIF DESJARDINS
Reel/Frame 048132/0551 →
SECURITY INTEREST Recorded Jan 25, 2019
From: AGRISOMA BIOSCIENCES INC.
To: CYCLE CAPITAL FUND III, L.P.
Reel/Frame 048132/0194 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 22, 2018
From: AGRISOMA BIOSCIENCES INC.
To: JOHN PLAZA
Reel/Frame 045668/0909 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 22, 2018
From: AGRISOMA BIOSCIENCES INC.
To: BDC CAPITAL INC.
Reel/Frame 045668/0948 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 22, 2018
From: AGRISOMA BIOSCIENCES INC.
To: CAPITAL REGIONAL ET COOPERATIF DESJARDINS
Reel/Frame 045669/0435 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 22, 2018
From: AGRISOMA BIOSCIENCES INC.
To: GESTION MANUIA INC.
Reel/Frame 045669/0529 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 22, 2018
From: AGRISOMA BIOSCIENCES INC.
To: CYCLE CAPITAL FUND III, L.P.
Reel/Frame 045540/0689 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 31, 2017
From: HETHERINGTON, MARK; HOFFMANN, TRAVIS; LINDENBAUM, MICHAEL
To: AGRISOMA BIOSCIENCES INC.
Reel/Frame 043989/0488 →
Continuity (2)
Provisional Application 62262032 · Dec 2, 2015
Related Publication 20180042266A1 · Feb 15, 2018