IP Library Granted Patent US 10,564,115
Granted Patent B2
US 10,564,115 · App. 15/586,465 · Granted Feb 18, 2020

X-ray analysis of drilling fluid

Inventor: Mark Alexander Pals (Almelo, NL)
Assignee: MALVERN PANALYTICAL B.V.
G01N23/223G01N33/2823G01N2223/076G01N2223/321G01N2223/635G01N2223/637
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Quick Facts
Patent No.
US 10,564,115
App. No.
15/586,465
Granted
Feb 18, 2020
Kind
B2
Abstract

A measurement head for making X-ray measurements on drilling fluid includes an inner pipe ( 30 ) having a outlet ( 32 ) and an outer pipe ( 34 ) around the inner pipe. Drilling fluid is pumped through the outlet refreshing the fluid at the outlet. The pump is then stopped. A height sensor ( 42 ) is then used to measuring the height of a meniscus of drilling fluid at the outlet ( 32 ). An X-ray head ( 50 ) including an X-ray source ( 52 ) and an X-ray detector ( 54 ) is then moved into a reproducible position above the meniscus of fluid above the outlet. The height sensor ( 42 ) may be fixed to a movable cover ( 40 ), to the X-ray head ( 50 ) or to some other part of the measurement head.

Claims (37)

1. A measurement head for drilling fluid, comprising:

an inner pipe having an outlet, the outlet extending horizontally for allowing stationary fluid to remain in the inner pipe at the outlet for measurement;

an outer pipe around the inner pipe for collecting material output by the outlet of the inner pipe;

a height sensor for measuring the height of fluid at the outlet;

an X-ray head including an X-ray source and an X-ray detector; and

a cover movable between a first position covering the outlet to direct fluid output by the outlet into the outer pipe and a second position in which the cover is spaced from the outlet;

wherein the X-ray head is movable in the vertical direction with the cover in the second position so that the X-ray head can be moved to a position with a fixed height above material in the outlet using measurements from the height sensor; and

wherein the height sensor is a light beam occlusion sensor having a light source and a light detector, the light source directing a light beam onto the light detector; and

wherein the X-ray head is arranged to be moved downwards until the light beam incident on the light detector is broken.

2. A measurement head according to claim 1 , wherein the height sensor comprises a camera for capturing an image of the height of fluid at the horizontal output.

3. A measurement system, comprising:

a measurement head comprising:

an inner pipe having an outlet, the outlet extending horizontally for allowing stationary fluid to remain in the pipe at the outlet for measurement;

an outer pipe around the inner pipe for collecting material output by the outlet of the inner pipe;

a height sensor for measuring the height of fluid at the outlet; and

an X-ray head including an X-ray source and an X-ray detector; and

a control means arranged to control the motion of the X-ray head and height sensor to move the X-ray head between a rest position and a measurement position, wherein in the measurement position the X-ray source and X-ray detector are positioned above the outlet at a height determined by the height of fluid at the outlet measured by the height sensor,

and wherein the height sensor is a light beam occlusion sensor having a light source and a light detector, the light source directing a light beam onto the light detector; and

wherein the X-ray head is arranged to be moved downwards until the light beam incident on the light detector is broken.

4. A method of operation of a measurement head for drilling fluid, comprising:

pumping drilling fluid through an inner pipe, out through a outlet and removing the drilling fluid from an outer pipe;

halting the pumping, leaving a meniscus of drilling fluid at the outlet;

using a height sensor to measure the height of the meniscus;

aligning an X-ray head using the measured height; and

making an X-ray measurement using the X-ray head.

5. A method of operation according to claim 4 , further comprising:

covering the outer pipe over the outlet with a movable cover during the step of pumping drilling fluid; and

moving the movable cover before the steps of using the height sensor, aligning the X-ray head and making an X-ray fluorescence measurement.

6. A method of operation according to claim 5 , wherein the height sensor is a laser height sensor mounted to the cover, wherein the movable cover is in a first position during the step of pumping drilling fluid, the method further comprising:

moving the cover to a second position in which the laser height sensor is above the outlet during the step of measuring the height of material at the outlet; and

moving the cover to a third position in which neither the cover nor the laser height sensor are above the outlet during the steps of aligning the X-ray head and making an X-ray fluorescence measurement.

7. A method of operation according to claim 6 further comprising moving the X-ray head in the vertical direction with the cover in the third position to a position with a fixed height above material in the outlet using measurements from the laser height sensor.

8. A method of operation according to claim 5 , wherein the height sensor is mounted to the X-ray head;

wherein the steps of using a height sensor and aligning the X-ray head take place at the same time by moving the X-ray head in the vertical direction until it reaches a position with a fixed height above material in the outlet using measurements from the height sensor.

9. A method of operation according to claim 8 , wherein the height sensor is a light beam occlusion sensor having a light source and a light detector, the light source directing a light beam onto the light detector;

the method comprising moving the X-ray head downwards until the light beam incident on the light detector is broken.

10. A method of operation according to claim 4 , wherein the X-ray measurements are X-ray fluorescence measurements.

Assignments (2)
CHANGE OF NAME Recorded Jan 15, 2018
From: PANALYTICAL B.V.
To: MALVERN PANALYTICAL B.V.
Reel/Frame 045765/0354 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 15, 2017
From: PALS, MARK ALEXANDER
To: PANALYTICAL B.V.
Reel/Frame 042723/0687 →
Priority Claims (1)
EP 16171494 · May 26, 2016 · regional
Continuity (1)
Related Publication 20170343495A1 · Nov 30, 2017
Cited By (1)
US 12,650,370