IP Library Granted Patent US 10,030,020
Granted Patent B2
US 10,030,020 · App. 15/593,239 · Granted Jul 24, 2018

Spirocycle compounds and methods of making and using same

Inventors: Justin S. Cisar (San Diego, CA); Cheryl A. Grice (Encinitas, CA); Todd K. Jones (Solana Beach, CA); Olivia D. Weber (San Diego, CA); Daniel J. Buzard (San Diego, CA); Michael B. Shaghafi (San Diego, CA)
Assignee: ABIDE THERAPEUTICS, INC.
C07D471/10C07D519/00
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Quick Facts
Patent No.
US 10,030,020
App. No.
15/593,239
Granted
Jul 24, 2018
Kind
B2
Abstract

Provided herein are spirocycle compounds and pharmaceutical compositions comprising said compounds. The subject compounds and compositions are useful as modulators of MAGL and/or ABHD6. Furthermore, the subject compounds and compositions are useful for the treatment of pain.

Claims (33)

1. A compound of Formula (Ia):

wherein:

R 1 is H or C 1-6 alkyl;

R 2 is H or C 1-6 alkyl;

each R 3 is independently selected from C 2-6 alkenyl, C 2-6 alkynyl, C 1-6 alkynyl, halogen, —CN, C 1-6 haloalkyl, C 1-6 aminoalkyl, heterocycloalkyl, —C 1-6 alkyl(heterocycloalkyl), heteroaryl, —SF 5 , —NR 5 R 6 , —OR 7 , —CO 2 R 8 , —C(O)R 8 , and —C(O)NR 8 R 9 , wherein heterocycloalkyl and —C 1-6 alkyl(heterocycloalkyl) are optionally substituted with one or two R 4 ; or two adjacent R 3 form a heterocycloalkyl ring optionally substituted with one, two, or three R 4 ;

each R 4 is independently selected from C 1-6 alkyl, C 1-6 haloalkyl, C 3-8 cycloalkyl, halogen, oxo, —CN, —CO 2 R 8 , —C(O)R 8 , —C(O)NR 8 R 9 , —SO 2 R 8 , —NR 9 C(O)R 8 , and —NR 9 SO 2 R 8 ;

each R 5 and R 6 is independently selected from H, C 1-6 alkyl, C 1-6 haloalkyl, C 1-6 aminoalkyl, C 3-8 cycloalkyl, —C 1-6 alkyl(heterocycloalkyl), —C 1-6 alkyl-C(O)(heterocycloalkyl), heterocycloalkyl, aryl, and heteroaryl; or R 5 and R 6 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring optionally substituted with one, two, or three R 10 ;

each R 7 is independently selected from H, C 1-6 alkyl, C 1-6 haloalkyl, C 1-6 aminoalkyl, C 3-8 cycloalkyl, —C 1-6 alkyl(heterocycloalkyl), —C 1-6 alkyl-C(O)(heterocycloalkyl), heterocycloalkyl, aryl, and heteroaryl, wherein heterocycloalkyl, aryl, and heteroaryl are optionally substituted with one or two groups selected from oxo, C 1-6 alkyl, C 1-6 haloalkyl, CO 2 H, and C(O)NH 2 ;

each R 8 and R 9 is independently selected from H, C 1-6 alkyl, C 1-6 haloalkyl, C 3-8 cycloalkyl, aryl, and heteroaryl; or R 8 and R 9 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring optionally substituted with one or two groups selected from C 1-6 alkyl, C 1-6 haloalkyl, CO 2 H, and C(O)NH 2 ;

each R 10 is independently selected from C 1-6 alkyl, C 3-8 cycloalkyl, C 1-6 haloalkyl, halogen, oxo, —CN, —CO 2 R 8 , —C(O)R 8 , —C(O)NR 8 R 9 , —SO 2 R 8 , —NR 9 C(O)R 8 , and —NR 9 SO 2 R 8 ;

p is 0, 1, 2, 3, 4, or 5;

n is 0 or 1; and

m is 1 or 2; provided that when n is 0, then m is 2; and when n is 1, then m is 1;

or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof.

2. The compound of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein each R 3 is independently selected from C 1-6 alkyl, C 2-6 alkynyl, halogen, —CN, C 1-6 haloalkyl, heterocycloalkyl, —C 1-6 alkyl(heterocycloalkyl), heteroaryl, —SF 5 , —NR 5 R 6 , —OR′, —CO 2 R 8 , and —C(O)NR 8 R 9 .

3. The compound of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 1 and R 2 are both H.

4. The compound of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 1 and R 2 are both —CH 3 .

5. The compound of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein each R 3 is independently selected from C 1-6 alkyl, halogen, C 1-6 haloalkyl, —C 1-6 alkyl(heterocycloalkyl), —NR 5 R 6 , —OR 7 , —CO 2 R 8 , and —C(O)NR 8 R 9 .

6. The compound of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein each R 3 is independently selected from halogen, C 1-6 haloalkyl, —NR 5 R 6 , and —OR 7 .

7. The compound of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 5 and R 6 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring substituted with one or two R 10 independently selected from C 1-6 alkyl, C 3-8 cycloalkyl, C 1-6 haloalkyl, halogen, —CO 2 R 8 , —C(O)R 8 , —C(O)NR 8 R 9 , —SO 2 R 8 , —NR 9 C(O)R 8 , and —NR 9 SO 2 R 8 .

8. The compound of claim 7 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 5 and R 6 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring substituted with one or two R 10 independently selected from C 1-6 alkyl and —CO 2 H.

9. The compound of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 5 and R 6 , together with the nitrogen to which they are attached, form an unsubstituted heterocycloalkyl ring.

10. The compound of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 5 and R 6 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring optionally substituted with one, two, or three R 10 selected from:

11. The compound of claim 5 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein R 7 is independently selected from C 1-6 alkyl, C 1-6 haloalkyl, C 1-6 aminoalkyl, —C 1-6 alkyl(heterocycloalkyl), —C 1-6 alkyl-C(O)(heterocycloalkyl), heterocycloalkyl, and heteroaryl.

12. The compound of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or pharmaceutically acceptable salt thereof, wherein two adjacent R 3 form a heterocycloalkyl ring optionally substituted with one or two R 4 .

13. The compound of claim 1 , wherein p is 2.

14. The compound of claim 1 , wherein p is 1.

15. The compound of claim 1 , wherein n is 0 and m is 2.

16. The compound of claim 1 , wherein n is 1 and m is 1.

17. A compound selected from:

or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or a pharmaceutically acceptable salt thereof.

18. A pharmaceutical composition comprising a compound of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or a pharmaceutically acceptable salt thereof, and at least one pharmaceutically acceptable excipient.

19. A method of treating pain, epilepsy/seizure disorder, multiple sclerosis, neuromyelitis optica (NMO), Tourette syndrome, Alzheimer's disease, or abdominal pain associated with irritable bowel syndrome in a patient, comprising administering to the patient in need thereof a therapeutically effective amount of a compound of claim 1 , or a solvate, hydrate, tautomer, N-oxide, stereoisomer, or a pharmaceutically acceptable salt thereof.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE THE RECEIVING PARTY NAME PREVIOUSLY RECORDED AT REEL: 055679 FRAME: 0885. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 11, 2021
From: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
To: H. LUNDBECK A/S
Reel/Frame 056544/0697 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2021
From: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
To: H. LUNDBECK A/S.
Reel/Frame 055679/0885 →
MERGER Recorded Mar 23, 2021
From: ABIDE THERAPEUTICS, INC.
To: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
Reel/Frame 057434/0784 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 15, 2017
From: CISAR, JUSTIN S.; GRICE, CHERYL A.; JONES, TODD K.; WEBER, OLIVIA D.; BUZARD, DANIEL J.; SHAGHAFI, MICHAEL B.
To: ABIDE THERAPEUTICS, INC.
Reel/Frame 042726/0678 →
Continuity (2)
Provisional Application 62335597 · May 12, 2016
Related Publication 20170327500A1 · Nov 16, 2017
Cited By (1)
US 12,378,219