IP Library Granted Patent US 10,377,742
Granted Patent B2
US 10,377,742 · App. 15/603,023 · Granted Aug 13, 2019

AMPK-activating heterocyclic compounds and methods for using the same

Inventors: Dane Goff (Redwood City, CA); Donald Payan (Hillsborough, CA); Rajinder Singh (Belmont, CA); Simon Shaw (Oakland, CA); David Carroll (San Francisco, CA); Yasumichi Hitoshi (Brisbane, CA)
Assignee: Rigel Pharmaceuticals, Inc.
C07D401/14C07D213/56C07D213/81C07D213/82C07D401/04C07D401/06C07D401/12C07D405/12C07D405/14C07D409/12C07D409/14C07D413/14C07D417/14C07D451/06C07D471/10C07D487/04C07D495/04C07B2200/07
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Quick Facts
Patent No.
US 10,377,742
App. No.
15/603,023
Granted
Aug 13, 2019
Kind
B2
Abstract

Disclosed are substituted pyridine compounds as well as pharmaceutical compositions and methods of use. One embodiment is a compound having the structure wherein E, J, T, the ring system denoted by “B”, T, R 3 , R 4 , w and x are as described herein. In certain embodiments, a compound disclosed herein activates the AMPK pathway, and can be used to treat metabolism-related disorders and conditions.

Claims (50)

1. A compound having the structural formula:

or a pharmaceutically acceptable salt or N-oxide thereof, wherein

one of X 1 and X 2 is N, and the others are CH or C substituted by one of the w R 3 ;

Y is N or CH;

R 1 is H;

G is —CH 2 —, —C(O)— or S(O) 2 —;

R 17 is phenyl substituted with 0, 1 or 2 substituents each independently selected from methyl, ethyl, n-propyl, isopropyl, trifluoromethyl, pentafluoroethyl, acetyl, —NH 2 , —OH, methoxy, ethoxy, trifluoromethoxy, —SO 2 Me, -halogen, —NO 2 , N 3 , —SF 5 , and —CN;

w is 0, 1 or 2;

each R 3 is independently selected from methyl, ethyl, n-propyl, isopropyl, trifluoromethyl, pentafluoroethyl, acetyl, —NH 2 , —OH, methoxy, ethoxy, trifluoromethoxy, —SO 2 Me, -halogen, —NO 2 and —CN;

Q is a single bond, —CH 2 —, —O—, —C(O)— or —S(O) 2 —;

the ring system denoted by “A” is phenyl;

each R 5 is independently selected from methyl, trifluoromethyl, acetyl, methoxy, trifluoromethoxy, -halogen, —NO 2 , N 3 , —SF 5 , and —CN; and

y is 0, 1 or 2.

2. The compound according to claim 1 , wherein Y is N.

3. The compound according to claim 1 , wherein Y is CH.

4. The compound according to claim 3 , wherein Q is —O—.

5. The compound according to claim 1 , wherein Q is —C(O)— or —S(O) 2 —.

6. The compound according to claim 1 , wherein Q is —CH 2 —.

7. The compound according to claim 1 , wherein Q is a single bond.

8. The compound according to claim 1 , wherein y is other than zero and at least one R 5 is halogen, CN, trifluoromethyl, pentafluoroethyl, trifluoromethoxy, —N 3 , —SF 5 or NO 2 .

9. The compound according to claim 1 , wherein w is 0.

10. The compound according to claim 1 , having the structural formula:

11. The compound according to claim 1 having the structural formula:

12. The compound according to claim 1 , wherein the

13. The compound according to claim 1 , wherein the

14. A compound according to claim 1 , wherein G is —CH 2 —.

15. A compound according to claim 1 , wherein G is —C(O)—.

16. A compound according to claim 1 , wherein the compound is

N-(cis-1-(4-cyanobenzyl)-3-fluoropiperidin-4-yl)-5-(4-(4-fluorobenzyl)piperazine-1-carbonyl)picolinamide;

N-(cis-1-(4-chlorobenzyl)-3-fluoropiperidin-4-yl)-5-(4-(4-fluorobenzyl)piperazine-1-carbonyl)picolinamide;

N-((trans)-1-(4-cyanobenzyl)-3-fluoropiperidin-4-yl)-5-(4-(4-(methylsulfonyl)benzoyl)piperidine-1-carbonyl)picolinamide;

N-((trans)-3-fluoro-1-(4-(trifluoromethoxy)benzyl)piperidin-4-yl)-5-(4-(4-(methylsulfonyl)benzoyl)piperidine-1-carbonyl)picolinamide;

N-((trans)-1-(4-cyanobenzyl)-3-fluoropiperidin-4-yl)-5-(4-(4-(methylsulfonyl)phenoxy)piperidine-1-carbonyl)picolinamide;

N-((trans)-3-fluoro-1-(4-(trifluoromethoxy)benzyl)piperidin-4-yl)-5-(4-(4-(methylsulfonyl)phenoxy)piperidine-1-carbonyl)picolinamide;

N-((trans)-1-(4-cyanobenzyl)-3-fluoropiperidin-4-yl)-6-(4-(4-methoxybenzoyl)piperidine-1-carbonyl)nicotinamide;

N-((trans)-3-fluoro-1-(4-(trifluoromethoxy)benzyl)piperidin-4-yl)-6-(4-(4-methoxybenzoyl)piperidine-1-carbonyl)nicotinamide;

N-((trans)-3-fluoro-1-(4-isopropoxybenzyl)piperidin-4-yl)-6-(4-(4-methoxybenzoyl)piperidine-1-carbonyl)nicotinamide;

N-((trans)-1-(4-cyano-3-fluorobenzyl)-3-fluoropiperidin-4-yl)-6-(4-(4-methoxybenzoyl)piperidine-1-carbonyl)nicotinamide;

N-((3R,4R)-1-(4-cyanobenzyl)-3-fluoropiperidin-4-yl)-6-(4-(4-methoxybenzoyl)piperidine-1-carbonyl)nicotinamide;

N-((3S,4S)-1-(4-cyanobenzyl)-3-fluoropiperidin-4-yl)-6-(4-(4-methoxybenzoyl)piperidine-1-carbonyl)nicotinamide;

N-((cis)-1-(4-cyanobenzyl)-3-fluoropiperidin-4-yl)-6-(4-(4-methoxybenzoyl)piperidine-1-carbonyl)nicotinamide; or

N-((cis)-3-fluoro-1-(4-(trifluoromethoxy)benzyl)piperidin-4-yl)-6-(4-(4-methoxybenzoyl)piperidine-1-carbonyl)nicotinamide;

or a pharmaceutically acceptable salt or N-oxide thereof.

17. A pharmaceutical composition comprising:

at least one pharmaceutically acceptable carrier, diluent or excipient; and

a compound according to claim 1 or a pharmaceutically acceptable salt or N-oxide thereof.

18. A method for treating type II diabetes in a subject, the method comprising administering to the subject an effective amount of a compound according to claim 1 or a pharmaceutically acceptable salt or N-oxide thereof.

19. A method for treating atherosclerosis in a subject, the method comprising administering to the subject an effective amount of a compound according to claim 1 or a pharmaceutically acceptable salt or N-oxide thereof.

20. A method for improving exercise efficiency in a subject, the method comprising administering to the subject an effective amount of a compound according to claim 1 or a pharmaceutically acceptable salt or N-oxide thereof.

21. A method for treating intermittent claudication, the method comprising administering to the subject an effective amount of a compound according to claim 1 or a pharmaceutically acceptable salt or N-oxide thereof.

Assignments (3)
SECURITY INTEREST Recorded May 8, 2026
From: RIGEL PHARMACEUTICALS, INC.
To: MIDCAP FUNDING IV TRUST
Reel/Frame 075576/0880 →
SECURITY INTEREST Recorded Aug 25, 2022
From: RIGEL PHARMACEUTICALS, INC.
To: MIDCAP FINANCIAL TRUST
Reel/Frame 061327/0712 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 25, 2017
From: GOFF, DANE; PAYAN, DONALD; SINGH, RAJINDER; SHAW, SIMON; CARROLL, DAVID; HITOSHI, YASUMICHI
To: RIGEL PHARMACEUTICALS, INC.
Reel/Frame 042506/0654 →
Continuity (6)
Division 14993936 · Jan 12, 2016
Division 14325766 · Jul 8, 2014
Division 13194810 · Jul 29, 2011
Division 13800986 · Mar 13, 2013
Provisional Application 61368928 · Jul 29, 2010
Related Publication 20180057478A1 · Mar 1, 2018
Cited By (8)
US 12,233,062 US 12,264,149 US 12,285,429 US 12,441,707 US 12,509,460 US 12,522,597 US 12,612,397 US 12,708,623