IP Library Granted Patent US 10,034,486
Granted Patent B2
US 10,034,486 · App. 15/639,688 · Granted Jul 31, 2018

Liquid espresso concentrate and method for preparing same

Inventors: Joannes Hubertus Petrus Maria Smits (Utrecht, NL); Cornelis Hendricus de Vos (Utrecht, NL); Ghanshijam Bhansing (Utrecht, NL)
Assignee: Koninklijke Douwe Egberts B.V.
A23F5/243A23F5/26A23F5/285
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Quick Facts
Patent No.
US 10,034,486
App. No.
15/639,688
Granted
Jul 31, 2018
Kind
B2
Abstract

Shown is a method of making a coffee concentrate, and a coffee concentrate obtainable by the method. The method involves primary and secondary extraction, with split tapping of the primary extract into a first and second primary draw off. The extraction is conducted under such conditions as to satisfy a minimum mass transfer Fourier number, and a minimum ratio of the extraction yield of the first primary draw-off to the extraction yield obtained in all extraction sections.

Claims (36)

1. A method for preparing a coffee concentrate comprising the steps of:

(a) providing ground roasted coffee beans having an average Martin diameter minimal value of from 0.5 to 3 mm;

(b) subjecting the ground roasted coffee beans to primary extraction with water, said primary extraction comprising obtaining a first primary extract with a draw-off factor of at most 2;

(c) drawing off a second primary extract after said first primary extract;

(d) subjecting the primarily extracted ground roasted coffee beans to a secondary extraction with water, so as to obtain a secondary extract;

(e) subjecting the second primary extract and the secondary extract to evaporation and combining the extracts before or after the evaporation, so as to obtain a concentrated extract having a dry solid matter content of from 30 wt. % to 75 wt. %;

(f) combining the concentrated extract with the first primary extract; and

(g) optionally adding water;

so as to obtain a liquid coffee concentrate having a dry solid matter content of from 15 wt. % to 55 wt. %, wherein the primary extraction is conducted under such conditions as to satisfy a mass transfer Fourier number of at least 0.35; and wherein the ratio of the first primary drawn soluble solids yield (Y-PE1) to the total extraction yield for coffee solubles (Y_TE) is in a range of from 0.15 to 1.0.

2. The method according to claim 1 , wherein the Martin diameter minimal value of the ground roasted coffee beans is 0.5 to 2.0 mm.

3. The method according to claim 2 , wherein the average Martin diameter minimal value of the ground roasted coffee beans is 1.4 to 1.9 mm.

4. The method according to claim 1 , wherein the coffee beans have a roasting degree corresponding to a roasting loss of 13% to 20%.

5. The method according to claim 1 , wherein the ground roasted coffee beans of step (a) have been roasted for 7.5 minutes to 15 minutes.

6. The method according to claim 1 , wherein the total extraction yield (Y_TE) ranges from 25% to 45%.

7. The method according to claim 1 , wherein the first primary drawn soluble solids yield (Y-PE1) ranges from 7.5% to 25%.

8. The method according to claim 1 , wherein the ratio of first primary drawn soluble solids yield (Y_PE1) to total extraction yield (Y_TE) ranges from 0.20 to 0.60.

9. The method according to claim 1 , wherein the Fourier number for primary extraction ranges from 0.5 to 1.5.

10. The method according to claim 1 , wherein aroma is recovered by means of steam stripping from the second primary draw-off to obtain a recovered aroma distillate, wherein partial aroma-recovery is applied to 20% to 60% of the total amount of the second primary draw-off, and the recovered aroma distillate is added to the coffee concentrate after evaporation.

11. The method according to claim 1 , wherein the dry solid matter content of the concentrated extract of step (e) after evaporation ranges from 40% solids content to 60% solids content.

12. The method according to claim 1 , wherein the ratio of water-to-coffee bean weight of step (b) is between 2.8 and 15.

13. The method according to claim 1 , wherein the primary extraction is conducted using, as an extraction fluid, water of a temperature between 70° C. and 120° C.

14. The method according to claim 1 , wherein the dry solid matter content of the obtained liquid coffee concentrate ranges from 25 wt. % to 35 wt. %.

15. A coffee concentrate comprising 15% to 55% dry solid matter, obtainable by a method as claimed in claim 1 .

16. A coffee concentrate comprising 15% to 55% dry solid matter, characterized by comprising 1-caffeoylquinic acid lactone (1-CQL) in an amount of at least 450 mg chlorogenic acid equivalents per kg of dry solid matter.

17. The method according to claim 2 , wherein the average Martin diameter minimal value of the ground roasted coffee beans is 1.6 to 1.8 mm.

18. The method according to claim 1 , wherein the ground roasted coffee beans of step (a) have been roasted for 8 to 10 minutes.

19. The method according to claim 1 , wherein the total extraction yield (Y_TE) ranges from 30% to 35%.

20. The method according to claim 1 , wherein the first primary drawn soluble solids yield (Y_PE1) ranges from 10% to 20%.

21. The method according to claim 1 , wherein the ratio of Y_PE1 to Y_TE ranges from 0.30 to 0.40.

22. The method according to claim 1 , wherein the Fourier number for primary extraction ranges from 0.5 to 1.0.

23. The method according to claim 1 , wherein aroma is recovered by means of steam stripping from the second primary draw-off to obtain a recovered aroma distillate, wherein partial aroma-recovery is applied to 20% to 40% of the total amount of the second primary draw-off, and the recovered aroma distillate is added to the coffee concentrate after evaporation.

24. The method according to claim 1 , wherein the ratio of water-to-coffee bean weight of step (b) is between 3 and 10.

25. The method according to claim 1 , wherein the ratio of water-to-coffee bean weight of step (b) is between 4.0 and 8.0.

26. The method according to claim 1 , wherein the primary extraction is conducted using, as an extraction fluid, water of a temperature between 85° C. and 95° C.

27. The coffee concentrate of claim 16 , comprising 1-CQL in an amount of at least 510 mg chlorogenic acid equivalents per kg of dry solid matter.

28. The coffee concentrate of claim 16 , comprising 1-CQL in an amount of at least 590 mg chlorogenic acid equivalents per kg of dry solid matter.

Assignments (2)
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNMENT PREVIOUSLY RECORDED AT REEL: 044155 FRAME: 0346. ASSIGNOR(S) HEREBY CONFIRMS THE CORRECTIVE ASSIGNMENT TO CORRECT THE NAME OF INVENTOR JOANNES HUBERTUS PETRUS MARIA SMITS.. Recorded Nov 20, 2017
From: SMITS, JOANNES HUBERTUS PETRUS MARIA; DE VOS, CORNELIS HENDRICUS; BHANSING, GHANSHIJAM
To: KONINKLIJKE DOUWE EGBERTS B.V.
Reel/Frame 044792/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 16, 2017
From: SMITS, JOHANNES HUBERTUS PETRUS MARIA; DE VOS, CORNELIS HENDRICUS; BHANSING, GHANSHIJAM
To: KONINKLIJKE DOUWE EGBERTS B.V.
Reel/Frame 044155/0346 →
Priority Claims (1)
EP 15150052 · Jan 2, 2015 · regional
Continuity (2)
Continuation PCTNL2015050912 · Dec 28, 2015
Related Publication 20170295814A1 · Oct 19, 2017
Cited By (3)
US 12,557,938 US 12,672,660 US 12,721,359