IP Library Granted Patent US 10,241,058
Granted Patent B2
US 10,241,058 · App. 15/641,724 · Granted Mar 26, 2019

Systems and methods for quality control of a periodic structure

Inventors: Alexei Maznev (Allston, MA); Keith A. Nelson (Newton, MA); Abdelhak Bensaoula (Houston, TX); Jateen S. Gandhi (Houston, TX); Donna Washington Stokes (Friendswood, TX); Rebecca Lynne Forrest (Houston, TX); Hyun Doug Shin (Cambridge, MA)
Assignee: Massachusetts Institute of Technology
G01N21/9515G01N21/1717G01N21/8422G01N21/9501G01N29/2418G01N29/38G01N29/46G10K11/002G01N2021/8438G01N2291/0231G01N2291/0237G01N2291/02854G01N2291/2697
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Quick Facts
Patent No.
US 10,241,058
App. No.
15/641,724
Granted
Mar 26, 2019
Kind
B2
Abstract

Quality control of a periodic structure is performed using the damping rate of acoustic waves generated in the periodic structure. In this technique, an excitation light beam illuminates the first layer in the periodic structure to excite an acoustic wave. Possible irregularities in the periodic structure can scatter the acoustic wave, thereby increasing the damping rate of the acoustic wave. A sequence of probe light beams illuminates the periodic structure to measure the acoustic wave as a function of time to generated a temporal signal representing the damping rate of the acoustic signal. The acquired damping rate is employed to evaluate the quality of the periodic structure.

Claims (44)

1. A method of quality control of a periodic structure comprising a stack of layers, the method comprising:

illuminating the periodic structure through a first layer in the stack of layers with at least one excitation light beam, the at least one excitation light beam exciting an acoustic wave in the periodic structure;

illuminating the periodic structure with at least one probe light beam;

detecting the at least one probe light beam, using a photodetector, after interaction with the periodic structure, the photodetector being configured to generate a signal representing a damping rate of the acoustic wave; and

estimating, with a processor, non-uniformity of the periodic structure based at least in part on the damping rate of the acoustic wave in the periodic structure,

wherein estimating the non-uniformity of the periodic structure comprises estimating a period variation of the periodic structure, and

wherein estimating the period variation of the periodic structure comprises detecting a deviation in a period of the periodic structure substantially equal to or less than 5 nm from an expected period of the periodic structure.

2. The method of claim 1 , further comprising:

generating the excitation light beam with a pulse duration substantially equal to or less than 1 ns.

3. The method of claim 1 , wherein the at least one probe light beam comprises a sequence of probe light pulses, each probe light pulse in the sequence of probe light pulses having a distinct time delay with respect to the at least one excitation light beam, and wherein detecting the at least one probe light beam comprises detecting each probe light pulse as a function of the distinct time delay.

4. The method of claim 1 , wherein the at least one excitation light beam comprises a sequence of excitation light pulses and the at least one probe light beam comprises a sequence of probe light pulses, each probe light pulse in the sequence of probe light pulses having a distinct time delay with respect to a corresponding excitation light pulse in the sequence of excitation light pulses.

5. The method of claim 1 , wherein detecting the probe light beam comprises detecting the probe light beam transmitted through the periodic structure.

6. The method of claim 1 , wherein detecting the probe light beam comprises detecting the probe light beam reflected from the periodic structure.

7. The method of claim 1 , wherein the periodic structure comprises a semiconductor superlattice.

8. A method of quality control of a periodic structure comprising a stack of layers, the method comprising:

illuminating the periodic structure through a first layer in the stack of layers with at least one excitation light beam, the at least one excitation light beam exciting an acoustic wave in the periodic structure;

illuminating the periodic structure with at least one probe light beam;

detecting the at least one probe light beam, using a photodetector, after interaction with the periodic structure, the photodetector being configured to generate a signal representing a damping rate of the acoustic wave;

estimating, with a processor, non-uniformity of the periodic structure based at least in part on the damping rate of the acoustic wave in the periodic structure,

wherein estimating the non-uniformity of the periodic structure comprises estimating a flatness of interfaces between adjacent layers in the stack of layers, and

wherein estimating the flatness of the interfaces comprises detecting a deviation from an expected flatness substantially equal to or less than 5 nm.

9. A method of quality control of a periodic structure comprising a stack of layers, the method comprising:

illuminating the periodic structure through a first layer in the stack of layers with at least one excitation light beam, the at least one excitation light beam exciting an acoustic wave in the periodic structure;

illuminating the periodic structure with at least one probe light beam;

detecting the at least one probe light beam, using a photodetector, after interaction with the periodic structure, the photodetector being configured to generate a signal representing a damping rate of the acoustic wave;

estimating, with a processor, non-uniformity of the periodic structure based at least in part on the damping rate of the acoustic wave in the periodic structure, wherein estimating the non-uniformity of the periodic structure comprises comparing the damping rate of the acoustic signal with a reference damping rate of a reference acoustic signal in a reference periodic structure;

measuring a dimension of the reference periodic structure; and

measuring the reference damping rate of the reference acoustic signal in the reference periodic structure.

10. The method of claim 9 , wherein measuring the dimension of the reference periodic structure comprises measuring the dimension using an electron microscope.

11. A method of quality control of a periodic structure comprising a stack of layers, the method comprising:

illuminating the periodic structure through a first layer in the stack of layers with at least one excitation light beam, the at least one excitation light beam exciting an acoustic wave in the periodic structure;

illuminating the periodic structure with at least one probe light beam;

detecting the at least one probe light beam, using a photodetector, after interaction with the periodic structure, the photodetector being configured to generate a signal representing a damping rate of the acoustic wave; and

estimating, with a processor, non-uniformity of the periodic structure based at least in part on the damping rate of the acoustic wave in the periodic structure,

wherein estimating the non-uniformity of the periodic structure comprises comparing the damping rate with a threshold damping rate, and the method further comprises:

in response to determining that the damping rate is greater than the threshold damping rate, generating a message indicating that the periodic structure is defective.

12. An apparatus for evaluating non-uniformity of a periodic structure comprising a stack of layers, the apparatus comprising:

at least one light source configured to illuminate the periodic structure through a first layer in the stack of layers with an excitation light beam, the excitation light beam exciting an acoustic wave in the periodic structure, the at least one light source further configured to illuminate the periodic structure with a probe light beam;

a detection system, in optical communication with the periodic structure, configured to detect the probe light beam after interaction with the periodic structure, the detection system further configured to generate a signal representing a damping rate of the acoustic wave in the periodic structure, the damping rate of the acoustic wave representing the non-uniformity of the periodic structure; and

a processor, operably coupled to the detection system, to estimate the non-uniformity of the periodic structure based on the damping rate of the acoustic wave, wherein the processor is configured to estimate the non-uniformity of the periodic structure by estimating a period variation of the periodic structure and configured to estimate the period variation of the periodic structure by detecting a deviation in a period of the periodic structure substantially equal to or less than 5 nm from an expected period of the periodic structure.

13. The apparatus of claim 12 , wherein the at least one light source is configured to emit the excitation light beam with a pulse duration substantially equal to or less than 1 ns.

14. The apparatus of claim 12 , wherein the at least one light source is configured to emit the probe light beam with a pulse duration substantially equal to or less than 1 ns and the probe light beam is variably delayed with respect to the excitation light beam.

15. The apparatus of claim 12 , wherein the detection system is configured to measure the probe light beam transmitted through the periodic structure.

16. The apparatus of claim 12 , wherein the detection system is configured to measure the probe light beam reflected from the periodic structure.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 31, 2019
From: MAZNEV, ALEXEI; NELSON, KEITH A.; SHIN, HYUN DOUG
To: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Reel/Frame 048200/0444 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 31, 2019
From: BENSAOULA, ABDELHAK; GANDHI, JATEEN S.; STOKES, DONNA WASHINGTON; FORREST, REBECCA LYNNE
To: UNIVERSITY OF HOUSTON
Reel/Frame 048207/0686 →
CONFIRMATORY LICENSE Recorded Sep 5, 2018
From: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 047015/0507 →
Continuity (2)
Provisional Application 62358219 · Jul 5, 2016
Related Publication 20180011031A1 · Jan 11, 2018