IP Library Granted Patent US 10,431,419
Granted Patent B2
US 10,431,419 · App. 15/643,862 · Granted Oct 1, 2019

Sparse sampling methods and probe systems for analytical instruments

Inventors: Libor Kovarik (West Richland, WA); Andrew J. Stevens (Richland, WA); Andrey V. Liyu (Pasco, WA); Nigel D. Browning (Richland, WA)
Assignee: Battelle Memorial Institute
H01J37/222H01J37/28H01J2237/226H01J2237/2802H01J2237/2809
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Quick Facts
Patent No.
US 10,431,419
App. No.
15/643,862
Granted
Oct 1, 2019
Kind
B2
Abstract

Sparse sampling approaches and probe systems for analytical instruments are disclosed providing for effective sub-sampling of a specimen and inpainting to reconstruct representations of actual information. The sub-sampling involves serial acquisition of contiguous measured values lying at positions along a scan path extending in a line toward a first direction and having random perturbations in a second direction. The perturbations are limited within a predetermined distance from the line. Inpainting techniques are utilized among the measured values to reconstruct a representation of actual information regarding the specimen.

Claims (31)

1. A method for sparse sampling with an analytical probe, the method comprising:

a) acquiring in a serial mode a plurality of contiguous measured values lying at positions along a scan path extending in a line toward a first direction and having random perturbations in a second direction, wherein the random perturbations are limited within a predetermined distance from the line; and

b) inpainting among the measured values and reconstructing a representation of actual information.

2. The method of claim 1 , further comprising repeating said acquiring step at different portions of a sample region, thereby acquiring measured values over substantially the entire sample region.

3. The method of claim 2 , wherein a plurality of the lines are adjacent and resemble a serpentine line form or a sawtooth line form.

4. The method of claim 1 , wherein the line has a curved form.

5. The method of claim 1 , wherein said acquiring further comprises moving an analytical probe and a sample from which the measured values are acquired relative to one another.

6. The method of claim 1 , wherein said acquiring further comprises holding an analytical probe at each of the positions from which measured values are acquired for a dwell time, the dwell time being less than a rise time associated with positional uncertainty of the analytical probe.

7. The method of claim 6 , wherein the dwell time is greater than or equal to 50% of the rise time.

8. The method of claim 6 , wherein the dwell time is between 70% and 90% of the rise time.

9. The method of claim 1 , wherein said acquiring further comprises sensing a sample with a physical tip.

10. The method of claim 1 , wherein said acquiring further comprises illuminating a sample with a charged particle beam, a neutral particle beam, an electromagnetic beam, or an optical beam.

11. The method of claim 10 , wherein said illuminating comprises illuminating with a substantially constant illumination intensity.

12. A sparse sampling analytical probe system comprising:

a) a scanner configured to move a sample and an analytical probe relative to one another and to scan the analytical probe over the sample along a scan path extending in a line toward a first direction and having random perturbations in a second direction, wherein the random perturbations are limited within a predetermined distance from the line;

b) a detector configured to acquire in a serial mode a plurality of contiguous measured values lying at positions along the scan path; and

c) a processor configured to apply inpainting techniques based on the measured values and to reconstruct a representation of actual information.

13. The system of claim 12 , wherein the analytical probe comprises a charged particle beam, a neutral particle beam, an electromagnetic beam, or an optical beam.

14. The system of claim 13 , wherein the analytical probe has a substantially constant illumination intensity at every position at which a measured value is acquired.

15. The system of claim 13 , wherein the scanner comprises electromagnetic deflectors.

16. The system of claim 15 , wherein the electromagnetic deflectors comprise scan coils.

17. The system of claim 13 , wherein the scanner comprises electrostatic deflectors.

18. The system of claim 12 , wherein the analytical probe comprises a physical tip.

19. The system of claim 18 , wherein the scanner comprises piezoelectric manipulators, optical elements, or a combination thereof.

20. The system of claim 13 , wherein the processor is configured to execute computer readable instructions including an inpainting solver stored in a memory device, the inpainting solver applying Bayesian dictionary learning techniques, beta-process factor analysis techniques, or combinations thereof.

21. The system of claim 13 , wherein the representation of actual information comprises an image having N pixels, and the plurality of measured values is fewer than or equal to 1%, 2%, 3%, 5%, 10%, 15%, 20%, 25%, 30%, 33%, 40%, 50%, 60%, 70%, 80%, or 90% of the N pixels.

22. The system of claim 12 , wherein the line comprises a continuous portion of a serpentine form or a sawtooth form.

23. The system of claim 12 , wherein the line has a curved line form.

24. The system of claim 12 , the scanner further configured to hold the analytical probe at each of the positions from which measured values are acquired for a dwell time, the dwell time being less than a rise time associated with positional uncertainty of the analytical probe.

25. The system of claim 24 , wherein the dwell time is greater than or equal to 50% of the rise time.

26. The system of claim 25 , wherein the dwell time is between 70% and 90% of the rise time.

Assignments (2)
CONFIRMATORY LICENSE Recorded Aug 2, 2017
From: BATTELLE MEMORIAL INSTITUTE, PACIFIC NORTHWEST DIVISION
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 043166/0945 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 12, 2017
From: KOVARIK, LIBOR; STEVENS, ANDREW J.; LIYU, ANDREY V.; BROWNING, NIGEL D.
To: BATTELLE MEMORIAL INSTITUTE
Reel/Frame 042985/0742 →
Continuity (2)
Provisional Application 62364176 · Jul 19, 2016
Related Publication 20180025887A1 · Jan 25, 2018
Cited By (3)
US 12,289,507 US 12,532,085 US 12,627,902