IP Library Granted Patent US 10,960,401
Granted Patent B2
US 10,960,401 · App. 15/645,001 · Granted Mar 30, 2021

Process for the decomposition of biomass material

Inventors: Ralf Hortsch (Munich, DE); Thomas Hoppe (Landshut, DE); Bjoern Huehnlein (Straubing, DE)
Assignee: Clariant International Ltd.
B02C23/00A23K10/12A23K10/32B02C23/06B02C23/08B02C23/14B09B3/00B09B3/0041B09B5/00C08B37/0057C08H8/00C12P7/08C12P7/10C08B1/00C12P7/00C12P2201/00Y02E50/10
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Quick Facts
Patent No.
US 10,960,401
App. No.
15/645,001
Granted
Mar 30, 2021
Kind
B2
Abstract

A process for the decomposition of biomass-material includes subjecting a lignocellulose-containing biomass-material to comminution, subjecting the comminuted lignocellulose-containing biomass-material to a sifting to separate from the comminuted lignocellulose-containing biomass-material a fraction of small-particles, and subjecting the remaining comminuted lignocellulose-containing biomass-material to a pretreatment. Before, during, or after the pretreatment, small particles can be added to the remaining comminuted lignocellulose-containing biomass-material. Optionally, the small particles can be added continuously during the pretreatment. The addition of small particles decreases friction of the remaining comminuted lignocellulose-containing biomass-material results in decreased process time, energy savings, and reduced production costs.

Claims (26)

1. A process for the decomposition of lignocellulose-containing biomass-material, comprising the steps:

(a) providing lignocellulose-containing biomass-material;

(b) subjecting the lignocellulose-containing biomass-material to comminution, whereby a plurality of particles of the biomass-material are formed;

(c) sifting the comminuted lignocellulose-containing biomass-material to obtain a particle-fraction having an average particle diameter of less than 2500 μm and remaining comminuted lignocellulose-containing biomass-material; and

(d) subjecting the remaining comminuted lignocellulose-containing biomass-material to a pretreatment;

wherein before, during or after the pretreatment, particles of said particle fraction or other particles are added to the remaining comminuted lignocellulose-containing biomass-material, wherein at least 70 wt.-% of the particles added have an average particle diameter of less than 1.6 mm, and wherein the particles added have a volumetric particle size distribution with a D(0.10) value of from 20 to 175 μm and a D(0.50) value from 250 to 450 μm.

2. The process of claim 1 , wherein the particles added are added continuously during the pretreatment.

3. The process of claim 1 , wherein particles are added to the remaining comminuted lignocellulose-containing biomass-material in an amount from 1 to 15 weight %, wherein the weight of the pretreated lignocellulose-containing biomass-material represents 100%.

4. The process of claim 1 , wherein the particles added comprise one or more types of particles selected from the group consisting of graphite, charcoal, activated coal, silicate and clay mineral particles.

5. The process of claim 1 , wherein the pretreatment is selected from mechanical pretreatment, biological pretreatment, chemical pretreatment, physical pretreatment and combinations thereof.

6. The process of claim 1 , wherein the particles added are obtained from the particle-fraction separated from the comminuted lignocellulose-containing biomass-material according to step c).

7. The process of claim 1 , wherein the particle-fraction separated from the comminuted lignocellulose-containing biomass-material in step c) has an average particle diameter of less than 1600 μm.

8. The process of claim 1 , wherein at least 85 wt.-% of the particles added have an average diameter of less than 1.6 mm.

9. The process of claim 2 , wherein particles are added to the remaining comminuted lignocellulose-containing biomass-material in an amount from 1 to 15 weight %, wherein the weight of the pretreated lignocellulose-containing biomass-material represents 100%.

10. A process for the decomposition of lignocellulose-containing biomass-material, comprising the steps:

(a) providing lignocellulose-containing biomass-material;

(b) subjecting the lignocellulose-containing biomass-material to comminution, whereby a plurality of particles of the biomass-material are formed;

(c) sifting the comminuted lignocellulose-containing biomass-material to obtain a particle-fraction consisting of particles having an average particle diameter of less than 2500 μm and a remaining comminuted lignocellulose-containing biomass-material;

(d) subjecting the remaining comminuted lignocellulose-containing biomass-material to a pretreatment;

wherein before, during or after pretreatment particles of said particle fraction or other particles are added to the remaining comminuted lignocellulose-containing biomass-material wherein at least 70 wt.-% of the particles added have an average particle diameter of less than 1.6 mm, wherein the particles added are characterized by a volumetric particle size distribution with a D(0.10) value from 20 to 175 μm and a D(0.50) value from 250 to 450 μm;

wherein the particles added are added continuously during the pretreatment;

wherein particles are added to the remaining comminuted lignocellulose-containing biomass-material in an amount from 1 to 15 weight %, wherein the weight of the pretreated lignocellulose-containing biomass-material represents 100%;

wherein the particles added comprise one or more types of particles selected from the group consisting of graphite, charcoal, activated coal, silicate and clay mineral particles;

wherein the pretreatment is selected from mechanical pretreatment, biological pretreatment, chemical pretreatment, physical pretreatment and combinations thereof.

11. The process of claim 10 , wherein the particle-fraction obtained from the comminuted lignocellulose-containing biomass-material in step c) has an average particle diameter of less than 1600 μm.

12. The process of claim 10 , wherein at least 85 wt.-% of the particles added have an average diameter of less than 1.6 mm.

Assignments (2)
CONFIRMATORY DEED OF ASSIGNMENT EFFECTIVE MAY 1, 2018 Recorded Nov 2, 2022
From: CLARIANT INTERNATIONAL LTD
To: CLARIANT PRODUKTE (DEUTSCHLAND) GMBH
Reel/Frame 061875/0121 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 10, 2017
From: HORTSCH, RALF; HOPPE, THOMAS; HUEHNLEIN, BJOERN
To: CLARIANT INTERNATIONAL LTD.
Reel/Frame 043136/0299 →
Priority Claims (1)
EP 15000112 · Jan 16, 2015 · regional
Continuity (2)
Continuation In Part PCTEP2015079986 · Dec 16, 2015
Related Publication 20170320970A1 · Nov 9, 2017