IP Library Granted Patent US 10,995,346
Granted Patent B2
US 10,995,346 · App. 15/649,806 · Granted May 4, 2021

System and process for adding pre-fermentation separated non-fermentables to a post-fermentation stream

Inventors: Michael Franko (Denver, CO); John Kwik (Bellbrook, OH); Neal Jakel (Cedar Rapids, IA)
Assignee: Fluid Quip Technologies, LLC
C12P7/14C12P7/04C12P7/08C12P7/10C12P7/40C12P7/649C12P19/02C12P7/00Y02E50/10
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Quick Facts
Patent No.
US 10,995,346
App. No.
15/649,806
Granted
May 4, 2021
Kind
B2
Abstract

A system and process is disclosed for adding pre-fermentation separated non-fermentables, e.g., fiber, germ/oil, and/or protein, to a post-fermentation stream in a corn (or similar carbohydrate-containing grain) dry milling process for making alcohol and/or other biofuels/biochemical. The process includes mixing grain particles with a liquid to produce a slurry having starch and non-fermentables. The slurry is subjected to liquefaction to convert the starch in the slurry to complex sugars and produce a liquefied stream including the complex sugars and non-fermentables. After liquefaction but prior to fermentation of simple sugars resulting from conversion of the complex sugars, the non-fermentables are separated out to define a non-fermentables portion and an aqueous solution including the complex and/or simple sugars. The simple sugars are fermented to provide a fermented stream. Then, the separated non-fermentables portion is reincorporated back into the process into a post-fermentation stream. In one example, the non-fermentables may be mainly fiber.

Claims (25)

1. A process for adding pre-fermentation separated non-fermentables to a post-fermentation stream, the process comprising:

mixing grain particles with a liquid to produce a slurry having starch and non-fermentables, including coarse fiber;

subjecting the slurry to liquefaction to convert the starch in the slurry to complex sugars and produce a liquefied stream including the complex sugars and the non-fermentables;

after liquefaction but prior to fermentation of simple sugars from conversion of the complex sugars, separating out at least a portion of the non-fermentables to define a non-fermentables portion, including the coarse fiber, and an aqueous solution including the complex and/or simple sugars;

thereafter, fermenting the simple sugars to provide a fermented stream;

reincorporating the separated non-fermentables portion, including the coarse fiber, back into the process into a post-fermentation stream including into either the fermented stream directly after fermenting the simple sugars or into a residuals stream directly after distillation of the fermented stream; and

thereafter, separating the post-fermentation stream, which includes the reincorporated non-fermentables portion and thin stillage, into a thin stillage portion and a wet cake portion, which includes the reincorporated non-fermentables portion, including the coarse fiber.

2. The process of claim 1 wherein fermenting the simple sugars to provide a fermented stream comprises fermenting the simple sugars to provide fructose, propanol, isobutanol, citric acid, succinic acid, or lactic acid.

3. The process of claim 1 wherein the grain particles are corn grain particles and the process is a dry grind corn milling process.

4. The process of claim 1 wherein the separated non-fermentables portion, including the coarse fiber, is reincorporated back into the process into the fermented stream directly after fermenting the simple sugars.

5. The process of claim 1 wherein the separated non-fermentables portion, including the coarse fiber, is reincorporated back into the process into the residuals stream directly after distillation of the fermented stream.

6. The process of claim 1 wherein after liquefaction but prior to fermentation of simple sugars resulting from conversion of the complex sugars comprises directly after liquefaction but prior to saccharification of the complex sugars, separating out the non-fermentables from the liquefied stream to define a non-fermentables portion, including the coarse fiber, and an aqueous solution, including the complex sugars, and subjecting the aqueous solution to saccharification to convert the complex sugars to simple sugars then fermenting the simple sugars provide the fermented stream.

7. The process of claim 1 further comprising subjecting the liquefied stream to saccharification to convert the complex sugars to simple sugars, and wherein after liquefaction but prior to fermentation of simple sugars resulting from conversion of the complex sugars comprises after saccharification but prior to fermentation of the simple sugars, separating out the non-fermentables to define a non-fermentables portion, including the coarse fiber, and an aqueous solution including the simple sugars.

8. The process of claim 1 further comprising vacuum distilling the fermented stream to produce alcohol and provide a residuals stream, and reincorporating the separated non-fermentables portion, including the coarse fiber, back into the residuals stream from distillation.

9. The process of claim 1 further comprising pressure distilling the fermented stream to produce alcohol and provide a residuals stream, and reincorporating the separated non-fermentables portion, including the coarse fiber, back into the fermented stream prior to distillation.

10. The process of claim 1 wherein after liquefaction but prior to fermentation of simple sugars resulting from conversion of the complex sugars, separating out the coarse fiber of the non-fermentables to define a non-fermentables coarse fiber portion and an aqueous solution including the complex and/or simple sugars, and reincorporating the separated non-fermentables coarse fiber portion back into the process into a post-fermentation stream.

11. A process for adding pre-fermentation separated non-fermentables to a post-fermentation stream, the process comprising:

mixing corn grain particles with a liquid to produce a slurry having starch and non-fermentables, including coarse fiber;

subjecting the slurry to liquefaction to convert the starch in the slurry to complex sugars and produce a liquefied stream including the complex sugars and the non-fermentables;

separating out at least a portion of the non-fermentables from the liquefied stream to define a non-fermentables portion, including the coarse fiber, and an aqueous solution including the complex sugars;

subjecting the aqueous solution to saccharification to convert the complex sugars to simple sugars;

thereafter, fermenting the simple sugars to provide a fermented stream;

reincorporating the separated non-fermentables portion, including the coarse fiber, back into the process into a post-fermentation stream including into either the fermented stream directly after fermenting the simple sugars or into a residuals stream directly after distillation of the fermented stream; and

thereafter, separating the post-fermentation stream, which includes the reincorporated non-fermentables portion and thin stillage, into a thin stillage portion and a wet cake portion, which includes the reincorporated non-fermentables portion, including the coarse fiber.

12. The process of claim 11 wherein, after subjecting the slurry to liquefaction to convert the starch in the slurry to complex sugars and produce the liquefied stream including the complex sugars and the non-fermentables, separating out the coarse fiber of the non-fermentables from the liquefied stream to define a non-fermentables coarse fiber portion and an aqueous solution including the complex sugars, and reincorporating the separated non-fermentables coarse fiber portion back into the process into a post-fermentation stream.

Assignments (2)
CHANGE OF NAME Recorded Jun 14, 2019
From: FLUID QUIP PROCESS TECHNOLOGIES, LLC
To: FLUID QUIP TECHNOLOGIES, LLC
Reel/Frame 049476/0914 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 15, 2017
From: FRANKO, MICHAEL; JAKEL, NEAL; KWIK, JOHN
To: FLUID QUIP PROCESS TECHNOLOGIES, LLC
Reel/Frame 043293/0741 →
Continuity (2)
Provisional Application 62362334 · Jul 14, 2016
Related Publication 20180016602A1 · Jan 18, 2018