IP Library Granted Patent US 10,801,108
Granted Patent B2
US 10,801,108 · App. 15/687,625 · Granted Oct 13, 2020

Method for fabricating ceramic matrix composite components

Inventors: Ying She (Hartford, CT); Rajiv Ranjan (South Windsor, CT); Zissis A. Dardas (Worcester, MA); Gajawalli V. Srinivasan (South Windsor, CT); Lesia V. Protsailo (Bolton, CT)
Assignee: Raytheon Technologies Corporation
C23C16/45544C04B35/565C04B35/62868C04B35/806C23C16/045H01L21/02529C01B32/956C04B2235/614
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Quick Facts
Patent No.
US 10,801,108
App. No.
15/687,625
Granted
Oct 13, 2020
Kind
B2
Abstract

A method for fabricating a component according to an example of the present disclosure includes the steps of depositing a stoichiometric precursor layer onto a preform, and densifying the preform by depositing a matrix material onto the stoichiometric precursor layer. An alternate method and a component are also disclosed.

Claims (15)

1. A method of fabricating a component, the method comprising:

arranging one or more preforms in a reactor;

providing a silicon-containing precursor to the reactor such that the silicon-containing precursor adsorbs onto the one or more preforms;

providing a carbon-containing precursor to the reactor such that the carbon-containing precursor reacts with the silicon-containing precursor to form a stoichiometric precursor layer, wherein the ratio of silicon atoms to carbon atoms in the stoichiometric precursor layer is approximately one; and

providing at least one silicon carbide precursor to the reactor to densify the one or more preforms by depositing a silicon carbide matrix onto the stoichiometric precursor layer.

2. The method of claim 1 , wherein the silicon carbide matrix has a ratio of silicon atoms to carbon atoms, and the ratio is approximately one.

3. The method of claim 1 , wherein the silicon-containing precursor includes one of Cl 2 SiH 2 , SiH 4 , ClSiH 3 , and Si 2 H 6 and the carbon-containing precursor includes one of CH 4 (methane), C 2 H 6 (ethane), C 3 H 8 (propane), C 2 H 2 (acetylene), and C 2 H 4 (ethylene).

4. The method of claim 1 , wherein the at least one silicon carbide precursor includes a first precursor and a second precursor, and the first precursor is methyltrichlorosilane (MTS) and the second precursor is hydrogen (H 2 ).

5. The method of claim 1 , further comprising the step of vacuuming the reactor after the step of providing the silicon-containing precursor to the reactor to remove excess silicon-containing precursor from the reactor.

6. The method of claim 1 , further comprising the step of vacuuming the reactor after the step of providing the carbon-containing precursor to the reactor to remove excess carbon-containing precursor from the reactor.

7. The method of claim 1 , wherein the reactor includes an exhaust valve, and wherein the exhaust valve is closed during the step of providing the silicon-containing precursor to the reactor and the step of providing the carbon-containing precursor to the reactor, and the exhaust valve is open during the step of providing at least one silicon-carbide precursor to the reactor.

8. The method of claim 1 , wherein the one or more preforms comprise silicon carbide fibers.

9. The method of claim 8 , wherein the silicon carbide fibers are coated with a boron nitride interfacial coating.

10. The method of claim 8 , wherein the silicon carbon fibers have a unidirectional orientation with respect to one another.

11. The method of claim 8 , further comprising determining the ratio of silicon atoms to carbon atoms in the silicon carbide matrix, and comparing the ratio to one.

Assignments (4)
CHANGE OF NAME Recorded Jul 27, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064714/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE AND REMOVE PATENT APPLICATION NUMBER 11886281 AND ADD PATENT APPLICATION NUMBER 14846874. TO CORRECT THE RECEIVING PARTY ADDRESS PREVIOUSLY RECORDED AT REEL: 054062 FRAME: 0001. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF ADDRESS. Recorded Mar 4, 2021
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 055659/0001 →
CHANGE OF NAME Recorded Sep 4, 2020
From: UNITED TECHNOLOGIES CORPORATION
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 054062/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2017
From: SHE, YING; RANJAN, RAJIV; DARDAS, ZISSIS A.; SRINIVASAN, GAJAWALLI V.; PROTSAILO, LESIA V.
To: UNITED TECHNOLOGIES CORPORATION
Reel/Frame 043419/0087 →
Continuity (1)
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