IP Library Granted Patent US 10,336,944
Granted Patent B2
US 10,336,944 · App. 15/711,634 · Granted Jul 2, 2019

Direct synthesis of hydrocarbons from co-electrolysis solid oxide cell

Inventors: Fanglin Chen (Irmo, SC); Libin Lei (Columbia, SC); Tong Liu (Columbia, SC); Shumin Fang (Columbia, SC)
Assignee: University of South Carolina
C10G2/35B01J23/10B01J23/78C10G2/332C10G2/34C10G2/40C10G2/50C25B3/04C25B9/10C25B15/02C25B15/08C07C1/10C07C1/12
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Quick Facts
Patent No.
US 10,336,944
App. No.
15/711,634
Granted
Jul 2, 2019
Kind
B2
Abstract

A hydrocarbon generation system that combines a solid oxide electrolysis cell (SOEC) and a Fischer-Tropsch unit in a single microtubular reactor is described. This system can directly synthesize hydrocarbons from carbon dioxide and water. High temperature co-electrolysis of H 2 O and CO 2 and low temperature Fischer-Tropsch (F-T) process are integrated in a single microtubular reactor by designation of a temperature gradient along the axial length of the microtubular reactor. The microtubular reactor can provide direct conversion of CO 2 to hydrocarbons for use as feedstock or energy storage.

Claims (15)

1. A hydrocarbon generation system comprising:

a plurality of microtubular reactors in an array, each microtubular reactor including

a first region including a cathode and an anode in electrical communication with one another and an oxygen ion conducting electrolyte between the cathode and the anode,

a second region including a Fischer-Tropsch reaction catalyst in fluid communication and downstream of the cathode; and

a temperature control unit configured to provide the first region at a first temperature that is greater than a second temperature of the second region, wherein each microtubular reactor defines a continuous space, such that the first region and second region are in contact producing a temperature gradient along each microtubular reactor.

2. The hydrocarbon generation system of claim 1 , wherein the outer diameter of the microtubular reactor is about 3 millimeters or less.

3. The hydrocarbon generation system of claim 1 , wherein the cathode comprises nickel-yttria stabilized zirconia, nickel-samaria doped ceria, nickel-gadolinium doped ceria, perovskites having the general formula of La 1-x M1 x M2O 3-δ in which M1 is an alkaline earth element and M2 is a transition metal element, Sr 2 Fe 2-x-y Mo x M y O 6-δ in which M is a transition metal element, and combinations there.

4. The hydrocarbon generation system of claim 1 , wherein the anode comprises lanthanum strontium cobalt iron oxide, strontium-doped lanthanum manganite, strontium-doped lanthanum manganite impregnated with ceria-based catalyst, Sr 2 Fe 2-x-y Mo x M y O 6-δ in which M is a transition metal element, La 1-x M1 x M2O 3-δ in which M1 is an alkaline earth element and M2 is a transition metal element, or combinations thereof.

5. The hydrocarbon generation system of claim 1 , wherein the electrolyte comprises yttria stabilized zirconia, scandia stabilized zirconia, lanthanum gallate-based oxide, doped ceria, or combinations thereof.

6. The hydrocarbon generation system of claim 1 , wherein the Fischer-Tropsch catalyst comprises cobalt, iron, nickel, nickel/platinum alloy, rhodium, ruthenium, palladium, osmium, vanadium, iron, manganese, or combinations thereof.

7. The hydrocarbon generation system of claim 1 , wherein the cathode and the Fischer-Tropsch catalyst are on an inner surface of the microtubular reactor.

8. The hydrocarbon generation system of claim 1 , wherein the cathode and the Fischer-Tropsch catalyst are on an outer surface of the microtubular reactor.

9. The hydrocarbon generation system of claim 1 , wherein the cathode comprises the Fischer Tropsch catalyst.

10. The hydrocarbon generation system of claim 1 , wherein the Fischer Tropsch catalyst comprises Ni and the hydrocarbon comprises methane.

11. The hydrocarbon generation system of claim 10 , wherein methane comprises about 18% to about 23% of the hydrocarbon.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 3, 2017
From: CHEN, FANGLIN; LEI, LIBIN; LIU, TONG; FANG, SHUMIN
To: UNIVERSITY OF SOUTH CAROLINA
Reel/Frame 043770/0037 →
Continuity (2)
Provisional Application 62400244 · Sep 27, 2016
Related Publication 20180086984A1 · Mar 29, 2018