IP Library Granted Patent US 10,898,609
Granted Patent B2
US 10,898,609 · App. 15/744,942 · Granted Jan 26, 2021

Tissue decellularization methods

Inventors: Christine E. Schmidt (Gainesville, FL); Rebecca Ann Wachs (Lincoln, NE); Robert Chase Cornelison (Charlottesville, VA)
Assignee: University of Florida Research Foundation, Inc.
A61L27/3633A61K35/30A61K35/32A61K35/42A61L27/3687A61L27/54C12N5/0619A61L2430/40C12N2533/90
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Quick Facts
Patent No.
US 10,898,609
App. No.
15/744,942
Granted
Jan 26, 2021
Kind
B2
Abstract

Provided herein are methods of producing an acellular tissue product wherein the method can include the step of inducing apoptosis and washing the tissue after induction of apoptosis with a tonic solution. Also provided herein are acellular tissue products produced by the methods provided herein and methods of administering the acellular tissue products to a subject in need thereof.

Claims (16)

1. A tissue decellularization method comprising:

obtaining a tissue sample from a subject to generate an ex vivo tissue sample;

exposing the ex vivo tissue sample to an apoptotic agent so as to produce apoptotic bodies; and

washing the ex vivo tissue sample in a hypertonic solution so as to remove the apoptotic bodies and produce decellularized tissue.

2. The method of claim 1 , wherein the tissue sample is a peripheral nerve, a nucleus pulposus, or a combination thereof or lung tissue.

3. The method of claim 1 , wherein the apoptotic agent is camptothecin, staurosporine, doxorubicin, or an analog thereof.

4. The method of claim 1 , wherein the concentration of the apoptotic agent ranges from about 1 nM to about 1 mM.

5. The method of claim 4 , wherein the apoptotic agent is camptothecin, staurosporine, doxorubicin, or an analog thereof.

6. The method of claim 1 , wherein the ex vivo tissue sample is exposed to the apoptotic agent for about 1-3 days.

7. The method of claim 1 , further comprising the step of treating the ex vivo tissue sample with DNAse for a period of time ranging from about 30 minutes to about 24 hours.

8. The method of claim 1 , wherein the step of washing produces an acellular tissue product.

9. The method of claim 8 , further comprising the step of adding an active agent to the acellular tissue product.

10. The method of claim 9 , wherein the active agent is selected from the group consisting of: a stem cell, a nucleic acid, an amino acid, a peptide, a polypeptide, an antibody, an aptamer, a ribozyme, a guide sequence for a ribozyme that inhibits translation or transcription of essential tumor proteins or genes, a hormone, an immunomodulator, an antipyretic, an anxiolytic, an antipsychotic, an analgesic, an antispasmodic, an anti-inflammatory, an antioxidant, an anti-histamine, an anti-infective, a chemotherapeutic, or a combination thereof.

11. The method of claim 9 , further comprising administering the acellular tissue product to a subject in need thereof.

12. The method of claim 8 , further comprising administering the acellular tissue product to a subject in need thereof.

13. The method of claim 12 , wherein the subject in need thereof has a spinal injury, a spinal disease, intervertebral disc degeneration, disease or trauma of the lungs, disease or trauma of the liver, volumetric muscle loss, peripheral nerve injury, amputation, spinal degradation, osteoarthritis of the hip, osteoarthritis of the knee, volumetric muscle loss, liver cirrhosis, or otherwise requires partial or total organ replacement, an antispasmodic, an anti-inflammatory, an anti-histamine, an anti-infective, a chemotherapeutic, or a combination thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 8, 2018
From: SCHMIDT, CHRISTINE E.; WACHS, REBECCA ANN; CORNELISON, ROBERT CHASE
To: UNIVERSITY OF FLORIDA RESEARCH FOUNDATION, INC.
Reel/Frame 046583/0581 →
CONFIRMATORY LICENSE Recorded Feb 12, 2018
From: UNIVERSITY OF FLORIDA
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 045308/0488 →
Continuity (2)
Provisional Application 62192823 · Jul 15, 2015
Related Publication 20180207318A1 · Jul 26, 2018