Mini hot press apparatus
The present invention relates to a mini hot press apparatus, and more particularly, to an apparatus which can be used for making or annealing a polycrystalline material by pressurization and heating in various surrounding environments such as in a low vacuum, high vacuum, ultrahigh vacuum, high pressure gas, gas flow, even in air, etc.
1. A mini hot press apparatus comprising:
a chamber including an inner case, a first space formed inside the inner case, an outer case having a size larger than the inner case and connected to the inner case to be sealed, a second space configured to accommodate a cooling medium as a sealed space formed between the inner case and the outer case, a cap installed on an upper end of each of the inner case and the outer case, and a bottom plate installed on a lower end of each of the inner case and the outer case;
a hollow mold installed in the first space of the chamber to accommodate a material therein;
a first rod inserted into the hollow mold and located under the material;
a second rod inserted into the hollow mold and located on the material;
a third rod located under the first rod in the first space of the chamber;
a fourth rod located on the second rod and installed to pass through the cap of the chamber to be disposed over the first space and the outside of the chamber;
a heater installed in the first space of the chamber to surround the hollow mold;
a first press installed at the outside of the chamber and configured to press the bottom plate, and a second press installed at the outside of the chamber and configured to press the fourth rod,
a thermocouple installed between the hollow mold and the heater;
a first low thermal conductive plate installed between the third rod and the bottom plate, and a second low thermal conductive plate installed between the second rod and the fourth rod;
a gas inlet and a gas outlet installed to be connected to the first space of the chamber
wherein the hollow mold, the third rod, and the fourth rod are formed of an insulator;
a quick-disconnect coupling installed on a portion of the cap through which the fourth rod passes;
O rings each installed between the inner case, the outer case, and the bottom plate, between the inner case, the outer case, and the cap, and between the cap and the quick-disconnect coupling; and
a multi pin electrical feedthrough installed at the outside of the chamber, and connected to the heater and the thermocouple through a wire; and
a copper gasket installed at the multi pin electrical feedthrough for sealing,
wherein the heater is a cylinder heater having a hollow cylindrical shape,
wherein the thermocouple measures a temperature of the material,
wherein thermal conductivity of each of the first low thermal conductive plate and the second low thermal conductive plate is independently 0.1 to 100 W/m·K,
wherein an inner wall of the mold is coated with a graphite film layer,
wherein an upper end of the first rod is coated with the graphite film layer, and
wherein a lower end of the second rod is coated with the graphite film layer.
2. The mini hot press apparatus of claim 1 , further comprising a thermal radiation blocking material installed on an outer circumference of the heater.
3. The mini hot press apparatus of claim 1 , further comprising a cooling medium inlet and a cooling medium outlet installed to be connected to the second space of the chamber.
4. The mini hot press apparatus of claim 1 , wherein a gas is at least one of an inert gas, a high-pressure gas, and a cooling medium.
5. The mini hot press apparatus of claim 1 , wherein a vacuum pump is connected to the chamber to form a vacuum in the chamber.