IP Library › Granted Patent US 10,547,056
Granted Patent B2
US 10,547,056 · App. 15/763,141 · Granted Jan 28, 2020

Precursors for lithium transition metal oxide cathode materials for rechargeable batteries

Inventors: Liang Zhu (Cheonan, KR); Randy De Palma (Kessel-Lo, BE); Hyo Sun Ahn (Cheonan, KR); Sung Jun Cho (SuWon, KR); Daniël Nelis (Peer, BE); Kris Driesen (Hasselt, BE)
Assignees: UMICORE; UMICORE KOREA, LTD.
H01M4/525C01G53/006C01G53/40C01G53/44C01G53/50H01B1/08H01M4/505H01M10/0525C01P2002/52C01P2002/54C01P2004/51C01P2006/12C01P2006/40C01P2006/80H01M2004/028
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Quick Facts
Patent No.
US 10,547,056
App. No.
15/763,141
Granted
Jan 28, 2020
Kind
B2
Abstract

A particulate precursor compound for manufacturing a lithium transition metal (M)-oxide powder for use as an active positive electrode material in lithium-ion batteries, wherein (M) is Ni x Mn y Co z A v , A being a dopant, wherein 0.33≤x≤0.60, 0.20≤y≤0.33, and 0.20≤z≤0.33, v≤0.05, and x+y+z+v=1, the precursor comprising Ni, Mn and Co in a molar ratio x:y:z and having a specific surface area BET in m 2 /g and a sulfur content S expressed in wt %, wherein formula (I).

Claims (34)

1. A particulate precursor compound for manufacturing a lithium transition metal (M)-oxide powder for use as an active positive electrode material in lithium-ion batteries, wherein (M) is Ni x Mn y Co z A v , A being a dopant, and wherein

0.33≤x≤0.50, 0.20≤y≤0.33, and 0.20≤z≤0.33, v≤0.05, and x+y+z+v=1, and the precursor comprises Ni, Mn and Co in a molar ratio x:y:z and has a specific surface area BET in m 2 /g and a sulfur content S expressed in wt %, and

(

BET

-

25

18

-

6

⁢

x

)

2

+

(

S

-

0.15

0.25

-

0.05

⁢

x

)

2

≤

0.75

.

2. The particulate precursor compound of claim 1 , wherein the precursor comprises a hydroxide M-OH or an oxyhydroxide M-OOH compound.

3. A method for preparing a lithium transition metal (M)-oxide powder for use as an active positive electrode material in lithium-ion batteries, comprising:

providing the M-precursor according to claim 1 ,

providing a Li precursor compound,

mixing the M-precursor and the Li precursor, and

firing the mixture at a temperature between 600 and 1100° C. for at least 1 hr.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 1, 2018
From: ZHU, LIANG; DEPALMA, RANDY; AHN, HYO SUN; CHO, SUNG JUN; NELIS, DANIËL; DRIESEN, KRIS
To: UMICORE; UMICORE KOREA, LTD.
Reel/Frame 045960/0001 →
Priority Claims (1)
EP 15187642 · Sep 30, 2015 · regional
Continuity (1)
Related Publication 20180269477A1 · Sep 20, 2018