IP Library › Granted Patent US 10,738,263
Granted Patent B2
US 10,738,263 · App. 15/774,641 · Granted Aug 11, 2020

Zinc-free lubricating composition

Inventors: Michael R. Sutton (Matlock, GB); Paul R. Vincent (Belper, GB)
Assignee: The Lubrizol Corporation
C10M169/044C10M141/10C10M161/00C10M2203/1025C10M2205/0206C10M2205/028C10M2205/0285C10M2205/04C10M2205/06C10M2207/023C10M2207/026C10M2207/028C10M2207/04C10M2207/046C10M2207/28C10M2207/34C10M2209/04C10M2209/084C10M2209/104C10M2209/105C10M2209/106C10M2209/108C10M2209/109C10M2215/042C10M2215/064C10M2215/086C10M2215/28C10M2219/022C10M2219/046C10M2219/087C10M2223/04C10M2223/043C10M2223/049C10M2223/06C10N2220/021C10N2220/022C10N2230/02C10N2230/04C10N2230/06C10N2230/10C10N2230/40C10N2230/42C10N2230/44C10N2230/45C10N2240/10C10N2240/104
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Quick Facts
Patent No.
US 10,738,263
App. No.
15/774,641
Granted
Aug 11, 2020
Kind
B2
Abstract

The invention is directed to a zinc-free lubricating composition for an internal combustion engine containing a phosphorus anti-wear agent, an ashless antioxidant, and an oxyalkylated phenol compound. The lubricating composition provides wear protection, deposit control, and improved acid control with reduced levels of metal-containing additives.

Claims (21)

1. A zinc-free lubricating composition comprising:

(a) an oil of lubricating viscosity;

(b) a zinc-free phosphorus-containing antiwear agent;

(c) at least one oxyalkylated hydrocarbyl phenol substituted with at least one aliphatic hydrocarbyl group of 1 to 250 carbon atoms; and

(d) a sulfurized phenol or sulfur-substituted phenol ashless antioxidant.

2. The lubricating composition of claim 1 , wherein the zinc-free phosphorus-containing antiwear agent is selected from phosphites, phosphonates, organic phosphate esters, amine or ammonium phosphate salts, and combinations thereof.

3. The lubricating composition of claim 1 , wherein the oxyalkylated hydrocarbyl phenol is represented by the formula:

wherein each R 2 is independently hydrogen or a hydrocarbyl group of 1 to 6 carbon atoms;

R 3 is hydrogen, a hydrocarbyl group of 1 to 24 carbon atoms, or an acyl group represented by —C(═O)R 5 ,

R 5 is a hydrocarbyl group of 1 to 24 carbon atoms;

each R 4 is independently a hydrocarbyl group of 1 to 250 carbon atoms (typically wherein at least one R 4 contains 20 to 220, or 30 to 150, 35 to 140, or 40 to 96 carbon atoms);

n=1 to 20; and m=1 to 3.

4. The lubricating composition of claim 1 , further comprising further comprises at least one other additive selected from an ashless dispersant, a phosphorus-free ashless anti-wear additive, a friction modifier, a polymeric viscosity modifier, a corrosion inhibitor, and a metal-containing detergent.

5. The lubricating composition of claim 1 , wherein the zinc-free phosphorus antiwear agent is present in an amount to deliver 0.01 weight % to 0.15 weight % phosphorus to the lubricating composition.

6. The lubricating composition of claim 1 , wherein the ashless antioxidant is present in an amount 0.1 weight % to 10 weight % in the lubricating composition.

7. The lubricating composition of claim 1 , further comprising a functionalized polymer compound in an amount 0.2 to 8 percent by weight of the composition, wherein the polymer has a number averaged molecular weight of at least 5000, and the polymer is selected from polyolefins, poly(meth)acrylates, styrene-diene copolymers, copolymers of maleic anhydride and one or more of alpha-olefins and vinyl-aromatic monomers, and combinations thereof.

8. The lubricating composition of claim 1 , further comprising a polyalkenyl succinimide dispersant in an amount from 0.1 to 2.0 weight % of the composition.

9. The lubricating composition of claim 1 , wherein the lubricant composition comprises less than 35 weight % of Group IV base oil.

10. A method of lubricating an internal combustion engine comprising lubricating the engine with a lubricant composition comprising (a) an oil of lubricating viscosity, (b) a zinc-free phosphorus-containing antiwear agent, (c) at least one oxyalkylated hydrocarbyl phenol that is substituted with at least one aliphatic hydrocarbyl group of 1 to 250 carbon atoms, and (d) a sulfurized phenol or sulfur-substituted phenol ashless antioxidant.

11. The method of claim 9 , wherein the engine is fueled with a liquid hydrocarbon fuel, a liquid nonhydrocarbon fuel, or mixtures thereof.

12. The method of claim 9 , wherein the engine is fueled by natural gas, liquefied petroleum gas (LPG), compressed natural gas (CNG), or mixtures thereof.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 8, 2018
From: SUTTON, MICHAEL R.; VINCENT, PAUL R.
To: THE LUBRIZOL CORPORATION
Reel/Frame 046023/0722 →
Continuity (2)
Provisional Application 62253871 · Nov 11, 2015
Related Publication 20190225911A1 · Jul 25, 2019
Cited By (2)
US 12,460,150 US 12,565,625