IP Library › Granted Patent US 10,919,998
Granted Patent B2
US 10,919,998 · App. 15/776,257 · Granted Feb 16, 2021

Color-conversion photonic crystal structure and color-conversion photonic crystal sensor using same

Inventors: Seo Hyun Jung (Ulsan, KR); Jong Mok Park (Daejeon, KR); Ho Youl Kong (Gyeongsangnam-do, KR); Ja Young Bae (Ulsan, KR)
Assignee: KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY
C08F212/12C08F220/54G01N21/81G02F1/3615B82Y15/00B82Y20/00G02F2202/022G02F2202/32
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Quick Facts
Patent No.
US 10,919,998
App. No.
15/776,257
Granted
Feb 16, 2021
Kind
B2
Abstract

A photonic crystal structure employs such a structure that two layers having different refractive indices are laminated alternately, a polymer including a structure unit derived from a monomer that contains a fluorocarbon group being used for one of the repeated layers such that the photonic crystal structure can respond to humidity and/or organic solvent concentration. Using the photonic crystal structure, it is possible to manufacture a color-conversion photonic crystal sensor having excellent sensitivity and reproduction characteristics.

Claims (25)

1. A color-conversion photonic crystal structure, comprising:

a first refractive index layer which includes a first polymer having a first refractive index; and a second refractive index layer which includes a second polymer having a second refractive index, wherein these refractive index layers are alternately laminated,

wherein the first refractive index is higher than the second refractive index; and

the second polymer comprises a structure unit represented by Formula 3:

wherein R 3 is selected from hydrogen and C 1-3 alkyl;

X 2 is C 1-10 alkyl substituted by at least one fluorine atom; and

n is independently an integer of 1 or more.

2. The structure of claim 1 , wherein a total laminating number of the first refractive index layer and the second refractive index layer ranges from 5 to 30.

3. The structure of claim 1 , wherein the first refractive index layer has a thickness of 50 to 150 nm, and the second refractive index layer has a thickness of 5 to 80 nm.

4. The structure of claim 1 , wherein the first polymer has a structure unit represented by Formulae 1 and 2 below in a molar ratio of 100:1 to 100:20, and a number average molecular weight of 10,000 to 100,000 g/mol:

wherein R 1 and R 2 are each independently selected from hydrogen and C 1-3 alkyl;

X 1 is selected from hydroxyl, cyano, nitro, amino, sulfonic acid or salts thereof, C 1-10 alkyl and C 1-10 alkoxy;

a1 is selected from 0, 1, 2 and 3;

Y 1 is O or NH; and

n is independently an integer of 1 or more.

5. The structure of claim 4 , wherein X 1 in Formula 1 is selected from methyl, ethyl, propyl, butyl, iso-butyl, sec-butyl and tert-butyl, and a1 is 0 or 1.

6. The structure of claim 1 , wherein the second polymer has the structure unit represented by Formula 3 and a structure unit represented by Formula 4 in a molar ratio of 100:1 to 100:5, and a number average molecular weight of 10,000 to 100,000 g/mol:

wherein R 3 and R 4 are each independently selected from hydrogen and C 1-3 alkyl;

X 2 is selected from C 1-10 alkyl substituted by at least one fluorine atom;

Y 2 is O or NH; and

n is independently an integer of 1 or more.

7. The structure of claim 6 , wherein X 2 in Formula 3 is selected from fluoromethyl, difluoromethyl, trifluoromethyl, 1-fluoroethyl, 2-fluoroethyl, 1,1-difluoroethyl, 1,2-difluoroethyl, 2,2-difluoroethyl, 1,1,2-trifluoroethyl, 1,2,2-trifluoroethyl, 1,1-trifluoroethyl, 1-fluoropropyl, 2-fluoropropyl, 1,1-difluoropropyl, 1,2-difluoropropyl, 2,2-difluoropropyl, 1,1,2-trifluoropropyl, 1,2,2-trifluoropropyl, 1-fluorobutyl, 2-fluorobutyl, 1,1-difluorobutyl, 1,2-difluorobutyl, 2,2-difluorobutyl, 1,1,2-trifluorobutyl; and 1,2,2-trifluorobutyl.

8. The structure of claim 1 , wherein a reflective wavelength of the photonic crystal structure is shifted by an external stimulation.

9. The structure of claim 8 , wherein the external stimulation occurs by a change in humidity or organic solvent concentration.

10. A color-conversion photonic crystal sensor comprising the color-conversion photonic crystal structure of claim 1 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 15, 2018
From: JUNG, SEO HYUN; PARK, JONG MOK; KONG, HO YOUL; BAE, JA YOUNG
To: KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGY
Reel/Frame 045808/0436 →
Priority Claims (1)
KR 10-2015-0175283 · Dec 9, 2015 · national
Continuity (1)
Related Publication 20200255565A1 · Aug 13, 2020