IP Library Granted Patent US 10,738,392
Granted Patent B2
US 10,738,392 · App. 15/781,850 · Granted Aug 11, 2020

Method for determining and regulating a diameter of a single crystal during pulling of the single crystal

Inventors: Thomas Schroeck (Kastl, DE); Thomas Aubrunner (Tacherting, DE)
Assignee: SILTRONIC AG
C30B15/22C30B15/20C30B15/30C30B29/06
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Quick Facts
Patent No.
US 10,738,392
App. No.
15/781,850
Granted
Aug 11, 2020
Kind
B2
Abstract

The diameter (d K ) of a cylindrical section and of an end cone of a single crystal being pulled from a melt in a crucible, is determined by measuring the diameter (d K ) of the single crystal at an interface with the melt while taking into account a lowering rate (v s ) of a surface of the melt relative to the crucible, a lifting rate (v K ) with which the crystal is raised relative to the crucible, and a conservation of mass, wherein a diameter of a cylindrical section of the single crystal, determined by means of observing a bright ring on the surface of the melt, and is used for a correction, a plausibility check or a comparison of the diameter (d K ) of the single crystal.

Claims (20)

1. A method for determining a diameter (dK) of a single crystal during the pulling of a cylindrical section of the single crystal and of an end cone of the single crystal from a melt in a crucible of a device for pulling the single crystal, comprising

determining the diameter (dK) of the single crystal at an interface with the melt, from

a first lowering rate (v S ) of a surface of the melt relative to the crucible,

a first lifting rate (vK), with which the single crystal is raised relative to the crucible, and

a conservation of mass,

additionally determining a d K ′ diameter of the single crystal during the pulling of the cylindrical section of the single crystal by means of observing a bright ring on the surface of the melt,

employing the additionally determined dK diameter of the single crystal as a correction, a plausibility check, or a comparison of the determined diameter (d K ) of the single crystal, and wherein

either a variation of a height and/or of a shape of a boundary region between the melt and the solid single crystal is taken into account during the determination of the diameter (dK) of the single crystal by means of a correction factor in a transition region between a cylindrical section of the single crystal and the end cone,

or the determination of the diameter of the single crystal is interrupted in a transition region between a cylindrical section of the single crystal and the end cone, when a predetermined variation of a height and/or of a shape of a boundary region between the melt and the solid single crystal occurs.

2. The method of claim 1 , further comprising determining a second lowering rate (v*S) of the surface of the melt relative to the device, and a rate (v*T) with which the position of the crucible relative to the device is varied, in order to take into account the first lowering rate (v S ) of the surface of the melt relative to the crucible.

3. The method of claim 1 , wherein a rotation of the crucible and a variation of the rotation are taken into account during the determination of the second lowering rate (v*S).

4. The method of claim 1 , wherein a second lifting rate (v*K), with which the single crystal is raised relative to the device, and a rate (v*T) with which the position of the crucible relative to the device is varied, are determined in order to take into account the first lifting rate (vK) with which the single crystal is raised relative to the crucible.

5. The method of claim 1 , wherein a density difference between the density of the liquid material of the melt and the density of the single crystal is taken into account during the determination of the diameter (dK) of the single crystal.

6. The method of claim 1 , wherein the diameter of the crucible at the position of the surface of the melt is taken into account during the determination of the diameter (dK) of the single crystal.

7. The method of claim 1 , wherein a diameter (dT) of the crucible is taken into account during the determination of the diameter (d K ) of the single crystal during the pulling of the end cone of the single crystal ( 200 ), and the accuracy of the determination of the diameter (dK) of the single crystal is increased by correcting the diameter (dT) of the crucible by a constant offset.

8. The method of claim 1 , wherein noise suppression by means of a filter, an observer and/or an adaptive filter, is carried out during determination of the diameter (dK) of the single crystal.

9. The method of claim 1 , wherein the diameter (dK) of the single crystal which is determined is used as a variable to be regulated during the pulling of the constant diameter portion of single crystal.

10. The method of claim 1 , wherein the diameter (dK) of the single crystal which is determined is used as a variable to be regulated during the pulling of the end cone of single crystal.

11. The method of claim 9 , wherein the first lifting rate (vK) and/or the second lifting rate (v*K) of the single crystal, a rate (vT) with which the position of the crucible is varied, the power of one or more heaters for heating the melt and/or temperatures of the device, and/or a rotation rate of the single crystal and/or of the crucible are used as manipulated variables during the pulling of the single crystal.

12. The method of claim 10 , wherein the first lifting rate (vK) and/or the second lifting rate (v*K) of the single crystal, a rate (vT) with which the position of the crucible is varied, the power of one or more heaters for heating the melt and/or temperatures of the device, and/or a rotation rate of the single crystal and/or of the crucible are used as manipulated variables during the pulling of the single crystal.

Assignments (3)
CORRECTIVE ASSIGNMENT TO CORRECT THE DATE OF THE CHANGE OF ADDRESS FROM 03/12/2020 TO 12/03/2020 PREVIOUSLY RECORDED AT REEL: 056719 FRAME: 0881. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jul 1, 2021
From: SILTRONIC AG
To: SILTRONIC AG
Reel/Frame 057561/0451 →
CHANGE OF ADDRESS Recorded Jun 30, 2021
From: SILTRONIC AG
To: SILTRONIC AG
Reel/Frame 056719/0881 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 10, 2018
From: SCHROECK, THOMAS; AUBRUNNER, THOMAS
To: SILTRONIC AG
Reel/Frame 046330/0818 →