IP Library Granted Patent US 10,060,032
Granted Patent B2
US 10,060,032 · App. 15/802,496 · Granted Aug 28, 2018

PECVD process

Inventors: Nagarajan Rajagopalan (Santa Clara, CA); Xinhai Han (Santa Clara, CA); Michael Wenyoung Tsiang (Fremont, CA); Masaki Ogata (San Jose, CA); Zhijun Jiang (Sunnyvale, CA); Juan Carlos Rocha-Alvarez (San Carlos, CA); Thomas Nowak (Cupertino, CA); Jianhua Zhou (Campbell, CA); Ramprakash Sankarakrishnan (Santa Clara, CA); Amit Kumar Bansal (Milpitas, CA); Jeongmin Lee (Sunnyvale, CA); Todd Egan (Fremont, CA); Edward Budiarto (Fremont, CA); Dmitriy Panasyuk (Santa Clara, CA); Terrance Y. Lee (Oakland, CA); Jian J. Chen (Fremont, CA); Mohamad A. Ayoub (Los Gatos, CA); Heung Lak Park (San Jose, CA); Patrick Reilly (Pleasanton, CA); Shahid Shaikh (Santa Clara, CA); Bok Hoen Kim (San Jose, CA); Sergey Starik (Kiev, UA); Ganesh Balasubramanian (Sunnyvale, CA)
Assignee: APPLIED MATERIALS, INC.
C23C16/52C23C16/458C23C16/4557C23C16/45565C23C16/46C23C16/50C23C16/505C23C16/509C23C16/5096G01B11/0625G01B11/0683G01N21/55G01N21/658H01L21/00H01L21/67248H01L21/67253H01L21/687G01N2201/1222
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Quick Facts
Patent No.
US 10,060,032
App. No.
15/802,496
Granted
Aug 28, 2018
Kind
B2
Abstract

A method of processing a substrate according to a PECVD process is described. Temperature profile of the substrate is adjusted to change deposition rate profile across the substrate. Plasma density profile is adjusted to change deposition rate profile across the substrate. Chamber surfaces exposed to the plasma are heated to improve plasma density uniformity and reduce formation of low quality deposits on chamber surfaces. In situ metrology may be used to monitor progress of a deposition process and trigger control actions involving substrate temperature profile, plasma density profile, pressure, temperature, and flow of reactants.

Claims (48)

1. A method, comprising:

disposing a substrate on a substrate support in a chamber;

establishing a temperature profile in the substrate;

controlling a temperature of a face plate of the chamber, wherein the face plate faces the substrate support, and wherein a processing region is between the face plate and the substrate support;

flowing a precursor gas mixture into the chamber;

forming a plasma in the chamber;

adjusting a density profile of the plasma; and

forming a layer of uniform thickness on the substrate.

2. The method of claim 1 , wherein the layer is of uniform composition.

3. The method of claim 1 , wherein controlling the temperature of the face plate promotes temperature uniformity in the processing region.

4. The method of claim 1 , wherein flowing the precursor gas mixture comprises providing the precursor gas mixture to the processing region through the face plate.

5. The method of claim 1 , wherein adjusting the density profile of the plasma comprises biasing an electrode coupled to at least one of:

a side wall of the chamber, and

the substrate support.

6. The method of claim 1 , further comprising:

flowing a second precursor gas mixture into the chamber; and

forming a second layer of uniform thickness to form a stack.

7. The method of claim 6 , wherein a structure of the stack is substantially planar, laminar, and parallel.

8. The method of claim 1 , wherein the uniform thickness varies from an average value by no more than 2%.

9. The method of claim 1 , further comprising sequentially forming multiple layers on the substrate in the chamber.

10. The method of claim 9 , wherein the multiple layers comprise at least 130 layers.

11. The method of claim 1 , further comprising controlling a temperature of at least one side wall of the chamber.

12. A method, comprising:

disposing a substrate on a substrate support in a chamber;

detecting a reflectivity of the substrate;

establishing a temperature profile in the substrate;

controlling a temperature of a face plate of the chamber, wherein the face plate faces the substrate support, and wherein a processing region is between the face plate and the substrate support;

flowing a precursor gas mixture into the chamber at a flow rate;

forming a plasma in the chamber from the precursor gas mixture;

adjusting a density profile of the plasma;

forming a layer on the substrate;

while forming the layer on the substrate, monitoring the reflectivity of the substrate to detect a thickness uniformity of the layer; and

based on the thickness uniformity, adjusting at least one of:

the density profile of the plasma;

the temperature profile in the substrate; and

the flow rate of the precursor gas mixture.

13. The method of claim 12 , further comprising detecting an end point based on the reflectivity of the substrate.

14. The method of claim 12 , wherein detecting the reflectivity comprises:

shining a light on the substrate; and

measuring a spectrum of light reflected by the substrate.

15. The method of claim 12 , wherein controlling the temperature of the face plate promotes temperature uniformity in the processing region.

16. The method of claim 12 , wherein flowing the precursor gas mixture comprises providing the precursor gas mixture to the processing region through the face plate.

17. The method of claim 12 , wherein adjusting the density profile of the plasma comprises biasing an electrode coupled to at least one of:

a side wall of the chamber, and

the substrate support.

18. The method of claim 12 , wherein monitoring the reflectivity of the substrate comprises monitoring a local reflectivity of multiple locations on the substrate to detect a local thickness at each of the multiple locations.

19. The method of claim 18 , wherein the local thicknesses at the multiple locations is compared to determine the thickness uniformity.

20. The method of claim 12 , further comprising sequentially forming multiple layers on the substrate in the chamber.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 30, 2017
From: RAJAGOPALAN, NAGARAJAN; HAN, XINHAI; TSIANG, MICHAEL WENYOUNG; OGATA, MASAKI; JIANG, ZHIJUN; ROCHA-ALVAREZ, JUAN CARLOS; NOWAK, THOMAS; ZHOU, JIANHUA; SANKARAKRISHNAN, RAMPRAKASH; BANSAL, AMIT KUMAR; LEE, JEONGMIN; EGAN, TODD; BUDIARTO, EDWARD; PANASYUK, DMITRIY; LEE, TERRANCE Y.; CHEN, JIAN J.; AYOUB, MOHAMAD A.; PARK, HEUNG LAK; REILLY, PATRICK; SHAIKH, SHAHID; KIM, BOK HOEN; STARIK, SERGEY; BALASUBRAMANIAN, GANESH
To: APPLIED MATERIALS, INC.
Reel/Frame 044554/0011 →
Continuity (7)
Continuation 15278455 · Sep 28, 2016
Continuation 14869371 · Sep 29, 2015
Continuation 14056203 · Oct 17, 2013
Provisional Application 61761515 · Feb 6, 2013
Provisional Application 61738247 · Dec 17, 2012
Provisional Application 61719319 · Oct 26, 2012
Related Publication 20180066364A1 · Mar 8, 2018