IP Library Granted Patent US 10,093,635
Granted Patent B2
US 10,093,635 · App. 15/814,322 · Granted Oct 9, 2018

MAGL inhibitors

Inventors: Cheryl A. Grice (Encinitas, CA); Daniel J. Buzard (San Diego, CA); Michael B. Shaghafi (San Diego, CA)
Assignee: ABIDE THERAPEUTICS, INC.
C07D295/195
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Quick Facts
Patent No.
US 10,093,635
App. No.
15/814,322
Granted
Oct 9, 2018
Kind
B2
Abstract

Provided herein are piperazine carbamates and pharmaceutical compositions comprising said compounds. The subject compounds and compositions are useful as modulators of MAGL. Furthermore, the subject compounds and compositions are useful for the treatment of pain.

Claims (49)

1. A compound having the structure of Formula (I):

wherein:

R 1 is —R 14 , —OR 3 , —SR 4 , —S(O) 2 R 4 , or —C≡C—(CR 6 R 7 )—R 8 ;

each R 2 is independently selected from C 1-6 alkyl, halogen, —CN, C 1-6 haloalkyl, —C 1-6 alkyl(heterocycloalkyl), —OR 17 , and —C(O)NR 18 R 19 ;

R 3 is —(CR 6 R 7 ) m —R 8 , —(CR 6 R 7 ) p —Y—(CR 6 R 7 ) q —R 8 , or —(CR 6 R 7 ) t —C 3-6 cycloalkyl-R 8 ;

R 4 is —(CR 6 R 7 ) m —R 8′ , —(CR 6 R 7 ) v —C(O)OH, or —(CR 6 R 7 ) p —Y—(CR 6 R 7 ) q —R 8 ;

Y is —O— or —N(R 22 )—;

each R 6 and R 7 is each independently selected from H, F, and C 1-6 alkyl; or R 6 and R 7 , together with the carbon to which they are attached, form a C 3-6 cycloalkyl ring;

R 8 is —C(O)OR 9 , —C(O)R 10 , or —C(O)O—(CR 12 R 13 )—OC(O)R 11 ;

R 8′ is —C(O)OR 9′ , —C(O)R 10′ , or —C(O)O—(CR 12 R 13 )—OC(O)R 11 ;

R 9 is H or C 1-6 alkyl;

R 9′ is C 1-6 alkyl;

R 10 is C 1-6 alkyl or —NHSO 2 R 21 ;

R 10′ is C 2-6 alkyl or —NHSO 2 R 21 ;

R 11 is C 1-6 alkyl or C 1-6 alkoxy;

R 12 and R 13 is each independently H or C 1-6 alkyl;

R 14 is —(CR 15 R 16 ) m —R 8 or —(CR 6 R 7 ) p —Y—(CR 6 R 7 ) q —R 8 ;

each R 15 and R 16 is each independently selected from H, F, and C 1-6 alkyl;

each R 17 is independently selected from H, C 1-6 alkyl, C 1-6 haloalkyl, and C 3-6 cycloalkyl;

each R 18 and R 19 is each independently selected from H, C 1-6 alkyl, C 3-6 cycloalkyl, aryl, and heteroaryl; or R 18 and R 19 , together with the nitrogen to which they are attached, form a heterocycloalkyl ring optionally substituted with one, two, or three R 20 ;

each R 20 is independently selected from halogen, C 1-6 alkyl, C 1-6 haloalkyl, oxo, —CN, and C 3-6 cycloalkyl;

R 21 is C 1-6 alkyl or C 3-6 cycloalkyl;

R 22 is H, C 1-6 alkyl, or —SO 2 R 23 ;

R 23 is C 1-6 alkyl;

m is 1, 2, 3 or 4;

n is 0, 1, 2, 3, or 4;

p is 2, 3, or 4;

q is 1, 2, or 3;

t is 0, 1, or 2; and

v is 3 or 4;

or a pharmaceutically acceptable salt or solvate thereof.

2. The compound of claim 1 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 1 is —OR 3 .

3. The compound of claim 2 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 3 is —(CR 6 R 7 ) m —R 8 .

4. The compound of claim 3 , or a pharmaceutically acceptable salt or solvate thereof, wherein m is 1, 2, or 3.

5. The compound of claim 4 , or a pharmaceutically acceptable salt or solvate thereof, wherein each R 6 and R 7 is each independently selected from H and C 1-6 alkyl, or R 6 and R 7 , together with the carbon to which they are attached, form a C 3-6 cycloalkyl ring.

6. The compound of claim 5 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 8 is —C(O)OR 9 .

7. The compound of claim 6 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 9 is H.

8. The compound of claim 6 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 9 is C 1-6 alkyl.

9. The compound of claim 5 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 8 is —C(O)R 10 .

10. The compound of claim 9 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 10 is —NHSO 2 R 21 .

11. The compound of claim 10 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 21 is C 1-6 alkyl.

12. The compound of claim 10 , or a pharmaceutically acceptable salt or solvate thereof, wherein R 21 is C 3-6 cycloalkyl.

13. The compound of claim 7 , or a pharmaceutically acceptable salt or solvate thereof, wherein each R 2 is independently selected from C 1-6 alkyl, halogen, and C 1-6 haloalkyl.

14. The compound of claim 13 , or a pharmaceutically acceptable salt or solvate thereof, wherein n is 2.

15. The compound of claim 13 , or a pharmaceutically acceptable salt or solvate thereof, wherein n is 1.

16. The compound of claim 1 having the structure selected from:

or a pharmaceutically acceptable salt or solvate thereof.

17. A pharmaceutical composition comprising a compound of claim 1 , or a pharmaceutically acceptable salt or solvate thereof, and at least one pharmaceutically acceptable excipient.

18. A pharmaceutical composition comprising a compound of claim 16 , or a pharmaceutically acceptable salt or solvate thereof, and at least one pharmaceutically acceptable excipient.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE THE RECEIVING PARTY NAME PREVIOUSLY RECORDED AT REEL: 055679 FRAME: 0885. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 11, 2021
From: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
To: H. LUNDBECK A/S
Reel/Frame 056544/0697 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 23, 2021
From: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
To: H. LUNDBECK A/S.
Reel/Frame 055679/0885 →
MERGER Recorded Mar 23, 2021
From: ABIDE THERAPEUTICS, INC.
To: LUNDBECK LA JOLLA RESEARCH CENTER, INC.
Reel/Frame 057434/0784 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 20, 2017
From: GRICE, CHERYL A.; BUZARD, DANIEL J.; SHAGHAFI, MICHAEL B.
To: ABIDE THERAPEUTICS, INC.
Reel/Frame 044454/0495 →
Continuity (2)
Provisional Application 62423099 · Nov 16, 2016
Related Publication 20180134674A1 · May 17, 2018
Cited By (1)
US 12,286,421