IP Library › Granted Patent US 10,118,174
Granted Patent B2
US 10,118,174 · App. 15/825,689 · Granted Nov 6, 2018

Device and method for pressure-driven plug transport and reaction

Inventors: Rustem F. Ismagilov (Chicago, IL); Joshua David Tice (Chicago, IL); Helen Song Baca (Antioch, IL); Lewis Spencer Roach (Chicago, IL)
Assignee: The University of Chicago
B01L3/502784B01F3/0861B01F5/0646B01F5/0647B01F13/0071B01J19/0046B01J19/0093B01L3/502746B01L3/502761B01L7/52C12P19/34C12Q1/44G01N35/08G01N35/085B01F5/0403B01F2215/0037B01J2219/0059B01J2219/0074B01J2219/0086B01J2219/00286B01J2219/00576B01J2219/00585B01J2219/00599B01J2219/00722B01J2219/00725B01J2219/00736B01J2219/00756B01J2219/00783B01J2219/00837B01J2219/00867B01J2219/00869B01J2219/00889B01J2219/00891B01J2219/00975B01J2219/00977B01L2200/0647B01L2200/0668B01L2200/0673B01L2200/10B01L2300/0867B01L2300/0883B01L2400/0424B01L2400/0448B01L2400/0454B01L2400/0487B82Y30/00G01N15/1484G01N2015/1409Y02A90/26Y10T436/118339Y10T436/12Y10T436/2575
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Quick Facts
Patent No.
US 10,118,174
App. No.
15/825,689
Granted
Nov 6, 2018
Kind
B2
Abstract

The present invention provides microfabricated substrates and methods of conducting reactions within these substrates. The reactions occur in plugs transported in the flow of a carrier-fluid.

Claims (33)

1. A method of conducting an autocatalytic reaction comprising forming a plurality of plugs and conducting the autocatalytic reaction in at least one plug, wherein:

each plug comprises an aqueous fluid surrounded by a hydrophobic fluid;

the aqueous fluid of at least one plug comprises a biological reagent;

the hydrophobic fluid of each plug comprises a fluorosurfactant; and

the fluorosurfactant is linked to an oligoethylene glycol (OEG).

2. The method of claim 1 , wherein the plugs are formed in a microchannel.

3. The method of claim 1 , further comprising sorting the plugs.

4. The method of claim 1 , wherein the autocatalytic reaction is a polymerase-chain reaction (PCR).

5. The method of claim 1 , wherein at least one plug comprises a single biological reagent.

6. The method of claim 5 , wherein the single biological reagent is DNA or RNA.

7. The method of claim 1 , wherein the fluorosurfactant comprises an oligoethylene glycol terminal.

8. The method of claim 7 , wherein the fluorosurfactant is of the formula:

wherein m is 0, 3, 4, 5, or 6; and n is an integer of no less than 16.

9. The method of claim 7 , where the oligoethylene glycol is linked to a terminal end of the fluorosurfactant.

10. The method of claim 1 , wherein the fluorosurfactant is linked to the oligoethylene glycol (OEG).

11. A method of preparing a composition comprising a plurality of plugs, the method comprising:

flowing an aqueous fluid in a first microchannel toward a junction, the aqueous fluid comprising a biological reagent;

flowing a hydrophobic fluid that is immiscible with the aqueous fluid in a second microchannel toward the junction, the hydrophobic fluid comprising a fluorosurfactant is linked to an oligoethylene glycol (OEG); and

contacting the aqueous fluid with the hydrophobic fluid at the junction and forming a plurality of plugs at the junction, wherein each plug comprises a subvolume of the aqueous fluid surrounded by the hydrophobic fluid and the subvolume of the aqueous fluid of at least one plug comprises a biological reagent.

12. The method of claim 11 , wherein pressure is applied in the first and second microchannels to induce fluid flow.

13. The method of claim 12 , wherein continuous flow of the hydrophobic fluid is provided in the microchannel after the contacting.

14. The method of claim 11 , wherein the biological reagent is at least one of a cell, a virion, an enzyme, a protein, and a nucleic acid.

15. The method of claim 11 , wherein the fluorosurfactant comprises a hydrophilic head.

16. The method of claim 11 , wherein the fluorosurfactant comprises an oligoethylene glycol terminal.

17. The method of claim 16 , wherein the fluorosurfactant is of the formula:

wherein m is 0, 3, 4, 5, or 6; and n is an integer of no less than 16.

18. The method of claim 16 , where the oligoethylene glycol is linked to a terminal end of the fluorosurfactant.

19. The method of claim 11 , wherein the fluorosurfactant is linked to the oligoethylene glycol (OEG).

20. A method of conducting an enzymatic reaction comprising forming a plurality of plugs and conducting the enzymatic reaction in at least one plug, wherein:

each plug comprises an aqueous fluid surrounded by a hydrophobic fluid;

the aqueous fluid of at least one plug comprises an enzyme;

the hydrophobic fluid of each plug comprises a fluorosurfactant; and

the fluorosurfactant is linked to an oligoethylene glycol (OEG).

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 28, 2018
From: ISMAGILOV, RUSTEM F.; TICE, JOSHUA DAVID; SONG BACA, HELEN; ROACH, LEWIS SPENCER
To: THE UNIVERSITY OF CHICAGO
Reel/Frame 047002/0719 →
Continuity (7)
Division 14836432 · Aug 26, 2015
Continuation 14507938 · Oct 7, 2014
Continuation 11589700 · Oct 30, 2006
Division 10434970 · May 9, 2003
Provisional Application 60394544 · Jul 8, 2002
Provisional Application 60379927 · May 9, 2002
Related Publication 20180154362A1 · Jun 7, 2018
Cited By (7)
US 12,233,407 US 12,239,973 US 12,311,353 US 12,339,078 US 12,370,538 US 12,503,723 US 12,606,747