IP Library Granted Patent US 10,730,756
Granted Patent B2
US 10,730,756 · App. 15/877,168 · Granted Aug 4, 2020

Colloidal compositions and methods of preparing same

Inventors: Brian T. Holland (Oak Park, IL); Francois Batllo (Burr Ridge, IL); Carmen Y. Ortiz (Woodridge, IL); Dennis L. MacDonald (Wheaton, IL)
Assignee: ECOLAB USA INC.
C01B33/20A61K8/042A61K8/19A61K8/25A61K8/416A61Q19/00B01J13/0008B82Y30/00C01B33/141C01B33/26C01B37/02C01B39/02A61K2800/10C01P2004/62C01P2004/64C01P2006/12
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Quick Facts
Patent No.
US 10,730,756
App. No.
15/877,168
Granted
Aug 4, 2020
Kind
B2
Abstract

Colloidal compositions and methods of preparing same are provided. The colloidal compositions include a silicate and a metal dispersed therein. The colloidal compositions can further include a stabilizer, such as a quaternary amine, to enhance the and dispersion of the metal loading within the silicate. The colloidal compositions can be made such that the metal is dispersed within the silicate in a controlled manner.

Claims (16)

1. A method of producing a silica colloid, comprising:

providing an alkaline solution having a stabilizing component,

adding a silicic acid solution to the alkaline solution, and

forming a colloid of silica particles, wherein the stabilizing component is dispersed throughout each silica particle,

wherein the alkaline solution comprises a cationic metal component.

2. The method of claim 1 , wherein the metal component is dispersed within one or more of the silica particles.

3. The method of claim 2 , wherein the stabilizing component and/or the metal component is dispersed in a homogenous manner.

4. The method of claim 1 , wherein the stabilizer is a quaternary compound.

5. The method of claim 4 , wherein the stabilizer is a quaternary amine.

6. The method of claim 5 , wherein the quaternary amine is quaternary ammonium hydroxide.

7. A method of preparing a metal-containing silica colloid, comprising:

adding a silicic acid solution to an alkaline solution to form a mixture;

adding a metal-silicate solution to the mixture,

forming a colloid of metal silicate particles.

8. The method of claim 7 , wherein the colloid is further processed to form a crystalline structure.

9. The method of claim 8 , wherein the further processing comprises heating.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 31, 2018
From: HOLLAND, BRIAN T.; BATLLO, FRANCOIS; ORTIZ, CARMEN Y.; MACDONALD, DENNIS L.
To: NALCO COMPANY
Reel/Frame 044789/0561 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 31, 2018
From: NALCO COMPANY LLC
To: ECOLAB USA INC.
Reel/Frame 044789/0841 →
CHANGE OF NAME Recorded Jan 31, 2018
From: NALCO COMPANY
To: NALCO COMPANY LLC
Reel/Frame 045210/0156 →
Continuity (2)
Continuation 10827214 · Apr 19, 2004
Related Publication 20180141822A1 · May 24, 2018