Fully water-soluble granule enriched in humic acid
View Patent ↗Disclosed is a process for making a water-soluble granule enriched in humic acid. Disclosed also is a water-soluble granule enriched in humic acid. Such a granule is useful as an organic aid to crop growth, particularly in applications where solubility is desirable or necessary.
1. A fully water-soluble granule comprising:
a homogenous powder comprising a hydrolyzed humic acid with a moisture content of about 9% to about 15% and a loose bulk density between about 28 and 49 pounds per cubic feet,
wherein the hydrolyzed humic acid is extracted from leonardite or humalite with an alkaline mixture; and
wherein the homogenous powder is granulated via compaction to form the fully water-soluble granule,
wherein the fully water-soluble granule is between about 0.5 mm and about 4.5 mm in diameter, and
wherein at least 95% of the fully water-soluble granule dissolves within five minutes when the fully water-soluble granule is submerged in one liter of water at a temperature of 25 degrees Celsius.
2. The fully water-soluble granule of claim 1 , wherein the granule is between about 0.8 mm and about 2.0 mm in diameter.
3. The fully water-soluble granule of claim 1 , wherein the granule is between about 2.1 mm and about 4.0 mm in diameter.
4. The fully water-soluble granule of claim 1 , wherein at least 99% of the granule dissolves within five minutes when the granule is submerged in one liter of water at a temperature of 25 degrees Celsius.
5. The fully water-soluble granule of claim 1 , wherein at least 95% of the granule dissolves within one minute when the granule is submerged in one liter of water at a temperature of 25 degrees Celsius.
6. The fully water-soluble granule of claim 1 , wherein at least 99% of the granule dissolves within one minute when the fully-water soluble granule is submerged in one liter of water at a temperature of 25 degrees Celsius.
7. The fully water-soluble granule of claim 1 , wherein the homogenous powder is granulated via compaction with a roller compactor at a speed of about 8 rpm and wherein the roller compactor exerts a pressure of about 1700 psi and does not exceed a temperature of about 130 degrees Fahrenheit.
8. A fully water-soluble granule enriched in humic acid, the granule made by a process comprising:
obtaining a sample of a carbonaceous substance comprising humic acid and one or more other substances;
contacting the sample with an amount of an alkaline mixture, thereby forming an extraction mixture, the extraction mixture consisting essentially of a sludge component, the sludge component comprising, predominantly, the sample, and an extraction component, the extraction component comprising, predominantly, the alkaline mixture;
maintaining the sludge component in contact with the extraction component for a period of time sufficient for the extraction component to become relatively enriched in humic acid and the sludge component to become relatively depleted of humic acid;
separating the sludge component from the extraction component;
spray drying the extraction component, thereby forming a plurality of powder particles; and
compacting, via a roll compactor, at least a portion of the plurality of powder particles,
wherein the at least a portion of the plurality of powder particles, as a result of the compacting, are made into a form of a fully water-soluble granule with a diameter between about 0.5 mm and about 4.5 mm
wherein at least 95% of the fully water-soluble granule dissolves within five minutes when the fully water-soluble granule is submerged in one liter of water at a temperature of 25 degrees Celsius.
9. The fully water-soluble granule of claim 8 , wherein the roll compactor operates at a speed of about 8 rpm and exerts a pressure of about 1700 psi.
10. The fully water-soluble granule of claim 8 , wherein the process further comprises:
rehydrating the fully water-soluble granule, thereby forming a rehydrated solution; and
applying the rehydrated solution to a desired location.