IP Library › Granted Patent US 10,357,913
Granted Patent B2
US 10,357,913 · App. 15/882,745 · Granted Jul 23, 2019

Transparent oriented polypropylene film with high moisture vapor and oxygen barrier properties

Inventors: Shichen Dou (Warwick, RI); Tracy A. Paolilli (East Greenwich, RI); Keunsuk P. Chang (North Kingstown, RI)
Assignee: TORAY PLASTICS (AMERICA), INC.
B29C48/91B29C48/08B29C48/154B29C48/21B29C48/22B32B7/12B32B27/08B32B27/28B32B27/32B32B27/322B29K2023/00B29K2023/12B29K2995/0026B29K2995/0067B29L2007/008B29L2009/00B29L2009/005B32B2250/24B32B2255/10B32B2255/26B32B2270/00B32B2307/31B32B2307/412B32B2307/514B32B2307/7242B32B2307/7244B32B2307/7246B32B2307/7265B32B2307/732B32B2307/746B32B2439/70B32B2553/00
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Quick Facts
Patent No.
US 10,357,913
App. No.
15/882,745
Granted
Jul 23, 2019
Kind
B2
Abstract

Described are transparent oriented polypropylene films with improved barrier properties and methods of making these films. The films and methods include a core layer comprising polypropylene, hydrocarbon resin, and polyethylene wax to improve moisture vapor barrier properties, an optional barrier layer comprising polar polymers to improve oxygen barrier properties, and optional skin layers to improve heat sealing, winding, printing, and/or adhesion.

Claims (13)

1. A method of making a film comprising:

coextruding a core layer comprising high crystalline polypropylene, hydrocarbon resin, and 0.5 wt. % polyethylene wax with a skin layer comprising polyolefin; and

adding a barrier layer comprising crosslinked polar polymers on a surface of the core layer opposite the skin layer.

2. The method of claim 1 , wherein the barrier layer is coextruded on the surface of the core layer opposite the skin layer.

3. The method of claim 1 , wherein the barrier layer is coated on the surface of the core layer opposite the skin layer.

4. The method of claim 3 , wherein the film is oriented in the machine direction prior to coating of the barrier layer.

5. The method of claim 4 , wherein the film is oriented in the transverse direction after coating the film with the barrier layer.

6. The method of claim 1 , further comprising coextruding a tie-layer comprising polyolefin on a surface of the core layer opposite the skin layer.

7. The method of claim 6 , wherein the barrier layer is inline or offline coated on the surface of the tie-layer opposite the core layer.

8. The method of claim 6 , wherein the barrier layer is coextruded on the surface of the tie-layer opposite the core layer.

9. The method of claim 1 , further comprising heat aging the film.

10. The method of claim 9 , wherein the aging temperature is lower than a Tg of the hydrocarbon resin and a melting temperature of the polyethylene wax.

11. The method of claim 9 , wherein the aging temperature is from 40-70° C. and the aging time is from 12 to 48 hours.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 29, 2018
From: DOU, SHICHEN; PAOLILLI, TRACY; CHANG, KEUNSUK P.
To: TORAY PLASTICS (AMERICA), INC.
Reel/Frame 044759/0162 →
Continuity (2)
Division 14798192 · Jul 13, 2015
Related Publication 20180162035A1 · Jun 14, 2018
Cited By (2)
US 12,202,232 US 12,741,260