IP Library Granted Patent US 11,724,310
Granted Patent B2
US 11,724,310 · App. 15/883,416 · Granted Aug 15, 2023

Titanium-group nano-whiskers and method of production

Inventors: Paul A. Menchhofer (Clinton, TN); Roland D. Seals (Oak Ridge, TN); James O. Kiggans, Jr. (Oak Ridge, TN)
Assignees: Consolidated Nuclear Security, LLC; UT-Battelle, LLC
B22F1/16C01B32/914C01B32/921C22C32/0052C22C47/00C22C49/04C22C49/14C23C16/0218C23C16/32C23C16/4417C30B25/005C30B29/36C30B29/62H01B1/02B22F1/054B22F2301/205B22F2302/10
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Quick Facts
Patent No.
US 11,724,310
App. No.
15/883,416
Granted
Aug 15, 2023
Kind
B2
Abstract

Disclosed herein are structures comprising a titanium, zirconium, or hafnium powder particle with titanium carbide, zirconium carbide, or hafnium carbide (respectively) nano-whiskers grown directly from and anchored to the powder particle. Also disclosed are methods for fabrication of such structures, involving heating the powder particles and exposing the particles to an organic gas.

Claims (21)

1. A titanium-group structure comprising:

a titanium-group powder particle having a plurality of titanium-group nano-whiskers jointlessly extending from the titanium-group powder particle by being grown directly from the titanium-group powder particle.

2. The titanium-group structure of claim 1 wherein the titanium-group powder particle has a maximum dimension of about 500 microns and the plurality of titanium group nano-whiskers have a maximum diameter of about one hundred nanometers and a length that is at least about one hundred nanometers.

3. The titanium-group structure of claim 1 wherein the titanium-group powder particle comprises titanium and the plurality of titanium group nano-whiskers comprise titanium carbide.

4. The titanium-group structure of claim 1 wherein the titanium-group powder particle comprises zirconium and the plurality of titanium-group nano-whiskers comprise zirconium carbide.

5. The titanium-group structure of claim 1 wherein the titanium-group powder particle comprises hafnium and the plurality of titanium-group nano-whiskers comprise hafnium carbide.

6. The titanium-group structure of claim 1 wherein the titanium-group powder particle comprises any combination of titanium, zirconium, and hafnium.

7. The titanium-group structure of claim 6 wherein the titanium group nano-whiskers comprise any combination of titanium carbide, zirconium carbide, and hafnium carbide.

8. The titanium-group structure of claim 1 wherein the plurality of titanium-group nano-whiskers each have a tapered structure.

9. The titanium-group structure of claim 1 wherein the titanium-group powder particle has a dimension that is at least one micron.

10. The titanium-group structure of claim 1 wherein the plurality of titanium-group nano-whiskers each have a maximum diameter of about ten nanometers and a length that is in a range from about five hundred nanometers to about one thousand nanometers.

11. The titanium-group structure of claim 1 wherein the plurality of titanium-group nano-whiskers include face-centered cubic crystalline titanium-group nano-whiskers.

12. A titanium-group structure consisting of a titanium-group powder particle having a plurality of titanium-group nano-whiskers jointlessly extending from the titanium-group powder particle.

13. The titanium-group structure of claim 12 wherein the titanium-group powder particle has a maximum dimension of about 500 microns and the plurality of titanium group nano-whiskers have a maximum diameter of about one hundred nanometers and a length that is at least about one hundred nanometers.

14. The titanium-group structure of claim 12 wherein the titanium-group powder particle comprises titanium and the plurality of titanium group nano-whiskers comprise titanium carbide.

15. The titanium-group structure of claim 12 wherein the titanium-group powder particle comprises zirconium and the plurality of titanium-group nano-whiskers comprise zirconium carbide.

16. The titanium-group structure of claim 12 wherein the titanium-group powder particle comprises hafnium and the plurality of titanium-group nano-whiskers comprise hafnium carbide.

17. The titanium-group structure of claim 12 wherein the titanium-group powder particle comprises any combination of titanium, zirconium, and hafnium and the titanium group nano-whiskers comprise any combination of titanium carbide, zirconium carbide, and hafnium carbide.

18. The titanium-group structure of claim 12 wherein the plurality of titanium-group nano-whiskers each have a tapered structure.

19. The titanium-group structure of claim 12 wherein the titanium-group powder particle has a dimension that is at least one micron.

20. The titanium-group structure of claim 12 wherein the plurality of titanium-group nano-whiskers each have a maximum diameter of about ten nanometers and a length that is in a range from about five hundred nanometers to about one thousand nanometers.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 4, 2020
From: MENCHHOFER, PAUL A.; KIGGANS, JAMES O., JR.
To: UT-BATTELLE, LLC
Reel/Frame 052834/0912 →
CONFIRMATORY LICENSE Recorded Jun 18, 2019
From: UT-BATTELLE, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 049500/0657 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 2, 2018
From: SEALS, ROLAND D.
To: CONSOLIDATED NUCLEAR SECURITY, LLC
Reel/Frame 045090/0867 →
CONFIRMATORY LICENSE Recorded Feb 2, 2018
From: CONSOLIDATED NUCELAR SECURITY, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 044812/0143 →
Continuity (2)
Continuation In Part 13162866 · Jun 17, 2011
Related Publication 20180154435A1 · Jun 7, 2018