IP Library Granted Patent US 10,392,394
Granted Patent B2
US 10,392,394 · App. 15/886,591 · Granted Aug 27, 2019

Antimicrobial compounds and methods

Inventor: Xiaoming Xu (Kenner, LA)
Assignee: Board of Supervisors of Louisiana State University and Agricultural and Mechanical College
C07D487/08A61K6/0047C07C229/14
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Quick Facts
Patent No.
US 10,392,394
App. No.
15/886,591
Granted
Aug 27, 2019
Kind
B2
Abstract

Antimicrobial compounds are provided that are polymerizable. The compounds include monomers with antimicrobial properties. The compounds have cross-linking properties. The compounds may be utilized in dental and/or medical applications, including dental composites, dentures, bonding agents, sealants, resins and medical devices.

Claims (29)

1. A compound having the structure:

wherein R and R′ may be the same or different; and R and R′ are independently selected from the group consisting of R1, R2, R3, R4, R5, and R6:

wherein m is an integer from 1 to 30;

wherein n is an integer from 0 to 20;

wherein A is A1:

wherein X is selected from the group consisting of F, Cl, Br, I, CF 3 SO 3 (triflate), acetate, and gluconate;

wherein Y is hydrogen or an unsubstituted aliphatic group containing 1 to 6 carbons, and wherein the various Y groups may be the same or different;

wherein Z is selected from the group consisting of one hydrogen atom, two hydrogen atoms, and an unsubstituted aliphatic group containing 1 to 6 carbons;

wherein R 1 is selected from the group consisting of hydrogen, an unsubstituted aliphatic group containing 1 to 18 carbons, benzyl, and a cyclic aliphatic or aromatic group containing 5 to 18 carbons; wherein, for clarity, it is noted that R 1 and R1 are different; and

wherein L is selected from the group consisting of L3, L4, L5, L6, L7, L8, L9, L10, and L11:

2. The compound of claim 1 , wherein R is R1, R′ is R1, each Y is methyl, and L is L7; whereby said compound has the structure:

3. The compound of claim 2 , wherein X is F or Br, m is 14, and R 1 is benzyl.

4. The compound of claim 1 , where at least one of R and R′ is acrylamide.

5. The compound of claim 1 , wherein X is selected from the group consisting of F, Cl, Br, I, CF 3 SO 3 (triflate), acetate, and gluconate.

6. The compound of claim 1 , wherein each Y is a methyl group.

7. The compound of claim 1 , wherein each Y is an ethyl group.

8. The compound of claim 1 , wherein Z is methyl or ethyl.

9. The compound of claim 1 , wherein each Y is a methyl group, and Z is hydrogen.

10. The compound of claim 1 , wherein each Y is hydrogen, and Z is a methyl or ethyl group.

11. The compound of claim 1 , wherein R 1 is benzyl, and wherein m is 2, 3, 4, 6, 8, 10, 11, 12, 14, 16, or 18.

12. The compound of claim 1 , wherein R 1 is a methyl or ethyl group, and wherein m is 6, 8, 10, 11, 12, 14, 16, or 18.

13. The compound of claim 1 , wherein R 1 is an unsubstituted aliphatic group containing 3, 4, 6, 8, 10, 11, 12, 14, 16, or 18 carbons; and wherein m is 2, 3, 4, 6, 8, 10, 11, 12, 14, 16, or 18.

14. The compound of claim 1 , wherein R and R′ are the same.

15. A dental composite containing 0.5% to 10% of the compound of claim 1 .

16. A denture base material containing 0.5% to 10% of the compound of claim 1 .

17. A dental bonding agent containing 0.5% to 5% of the compound of claim 1 .

18. A dental sealant containing 0.5% to 10% of the compound of claim 1 .

19. A dental resin cement containing 0.5% to 10% of the compound of claim 1 .

20. A medical device containing 0.5% to 10% of the compound of claim 1 .

Assignments (2)
CONFIRMATORY LICENSE Recorded Feb 6, 2023
From: LSU HEALTH SCIENCES CENTER
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 062652/0941 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 15, 2021
From: XU, XIAOMING
To: BOARD OF SUPERVISORS OF LOUISIANA STATE UNIVERSITY AND AGRICULTURAL AND MECHANICAL COLLEGE
Reel/Frame 056552/0894 →
Continuity (3)
Continuation 14782936
Provisional Application 61810136 · Apr 9, 2013
Related Publication 20180155353A1 · Jun 7, 2018