IP Library Granted Patent US 10,626,347
Granted Patent B2
US 10,626,347 · App. 15/906,602 · Granted Apr 21, 2020

Free polyunsaturated fatty acid-containing composition and manufacturing method therefor

Inventors: Yuhei Kosuge (Tokyo, JP); Hideaki Yamaguchi (Tokyo, JP); Nobushige Doisaki (Tokyo, JP)
Assignee: NIPPON SUISAN KAISHA, LTD.
C11C3/00A23D9/007A23L33/12A61K31/201A61K31/202C07C57/12C07C69/58A23V2002/00
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Quick Facts
Patent No.
US 10,626,347
App. No.
15/906,602
Granted
Apr 21, 2020
Kind
B2
Abstract

The present disclosure is: a free polyunsaturated fatty acid-containing composition, which comprises at least one free polyunsaturated fatty acid having 20 or more carbon atoms, the content being at least 80.0% of the fatty acids in the composition, and satisfies at least one selected from a group consisting of conditions (1) and (2): (1) the content of conjugated unsaturated fatty acid is 1.0% or less of the fatty acids in the composition, and (2) the Gardner color is less than 3+; and a manufacturing method for the free polyunsaturated fatty acid-containing composition comprising the preparation of a raw material composition containing at least one polyunsaturated fatty acid having 20 or more carbon atoms, and hydrolysis of a reaction solution containing the prepared raw material composition, a lower alcohol, water and an alkali catalyst at a temperature of 10° C. or lower.

Claims (9)

1. A free polyunsaturated fatty acid-containing composition, comprising at least one free polyunsaturated fatty acid having 20 or more carbons in an amount that a content thereof is 80.0% or greater of fatty acids in the composition, wherein the free polyunsaturated fatty acid-containing composition satisfies at least one selected from the group consisting of conditions (1) and (2):

(1) a content of a conjugated unsaturated fatty acid being from 0.001% to 1.0% of the fatty acids in the composition; and

(2) the Gardner color being less than 3+.

2. The free polyunsaturated fatty acid-containing composition according to claim 1 , wherein the free polyunsaturated fatty acid-containing composition has an anisidine value of 5.0 or less.

3. The free polyunsaturated fatty acid-containing composition according to claim 1 , wherein a content of the fatty acid alkyl ester is 0.2% or less of the fatty acids in the composition.

4. The free polyunsaturated fatty acid-containing composition according to claim 1 , wherein the content of the conjugated unsaturated fatty acid is from 0.01% to 0.8% of the fatty acids in the composition.

5. The free polyunsaturated fatty acid-containing composition according to claim 1 , wherein the polyunsaturated fatty acid is at least one selected from the group consisting of eicosadienoic acid, dihomo-y-linolenic acid, Mead acid, eicosatetraenoic acid, arachidonic acid, eicosapentaenoic acid, docosatetraenoic acid, docosapentaenoic acid, and docosahexaenoic acid.

6. The free polyunsaturated fatty acid-containing composition according to claim 1 , wherein a total content of a residual organic solvent in the composition is 5000 ppm or less.

7. The free polyunsaturated fatty acid-containing composition according to claim 1 , wherein a content of a di- or higher-valent polyunsaturated fatty acid having 18 carbons in the composition is 2.0% or less of the fatty acids in the composition.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 27, 2018
From: KOSUGE, YUHEI; YAMAGUCHI, HIDEAKI; DOISAKI, NOBUSHIGE
To: NIPPON SUISAN KAISHA, LTD.
Reel/Frame 045053/0373 →
Priority Claims (1)
JP 2015-170856 · Aug 31, 2015 · national
Continuity (2)
Continuation PCTJP2016075444 · Aug 31, 2016
Related Publication 20180195021A1 · Jul 12, 2018