IP Library Granted Patent US 10,208,020
Granted Patent B2
US 10,208,020 · App. 15/908,249 · Granted Feb 19, 2019

Substituted amino triazoles useful as human chitinase inhibitors

Inventors: Marzena Mazur (Łódź, PL); Robert Koralewski (Łódź, PL); Bartlomiej Borek (Łódź, PL); Sylwia Olejniczak (Łódź, PL); Wojciech J. Czestkowski (Pabianice, PL); Michal C. Piotrowicz (Łódź, PL); Jacek P. Olczak (Łódź, PL); Adam A. Golebiowski (Warsaw, PL); Agnieszka Bartoszewicz (Warsaw, PL); Elżbieta Maziarz (Kamień, PL); Michal Łukasz Kowalski (Godziszka, PL)
Assignee: OncoArendi Therapeutics S.A.
C07D401/14C07D413/14C07D417/14C07D487/04C07D498/04
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Quick Facts
Patent No.
US 10,208,020
App. No.
15/908,249
Granted
Feb 19, 2019
Kind
B2
Abstract

Disclosed are amino triazole compounds substituted with a piperidinyl ring that is itself substituted with a heterocyclic ring. These compounds are inhibitors of acidic mammalian chitinase and chitotriosidase. Also disclosed are methods of using the compounds to treat asthma reactions caused by allergens, as well as acute and chronic inflammatory diseases, autoimmune diseases, dental diseases, neurologic diseases, metabolic diseases, liver diseases, polycystic ovary syndrome, endometriosis, and cancer.

Claims (77)

1. A method for the therapeutic treatment of a disease, disorder, or condition associated with aberrant expression or activity of acidic mammalian chitinase, comprising administering to a human in need thereof a therapeutically effective amount of a compound, wherein said compound is represented by formula (I):

wherein:

W is halo, (C 1 -C 3 )alkyl, (C 1 -C 3 )alkoxy-, or (C 1 -C 3 )alkylthio-;

X is a single bond, —CH 2 —, —CH 2 CH 2 —, —CH═CH—, or —C(O)—;

Y is a single bond, —CH—, —CHCH 2 —, —CH 2 CH—, —C═CH—, —CH═C—, —N—, —O—, —S(O)—, or —S(O) 2 —;

if Y is a single bond, —O—, —S(O)—, or —S(O) 2 —, then R 1 is absent;

R 1 is H, (C 1 -C 6 )alkyl, (C 1 -C 6 )haloalkyl, (C 1 -C 6 )alkoxy, (C 1 -C 6 )hydroxyalkyl, (C 1 -C 6 )alkoxy(C 1 -C 6 )alkyl, aryl(C 1 -C 6 )alkyl, heteroaryl(C 1 -C 6 )alkyl, —C(O)(C 1 -C 6 )alkyl, —C(O)aryl, —C(O)heteroaryl, —C(O)aryl(C 1 -C 6 )alkyl, —C(O)heteroaryl(C 1 -C 6 )alkyl, —S(O) 2 (C 1 -C 6 )alkyl, —S(O) 2 aryl, —S(O) 2 heteroaryl, —S(O) 2 aryl(C 1 -C 6 )alkyl, —S(O) 2 heteroaryl(C 1 -C 6 )alkyl, —CO 2 H, —C(O)O(C 1 -C 6 )alkyl, —C(O)O(aryl), —C(O)O(heteroaryl), —C(O)O(aryl(C 1 -C 6 )alkyl), —C(O)O(heteroaryl(C 1 -C 6 )alkyl), —C(O)NH 2 , —C(O)NHOH, —C(O)NHCN, —C(O)NH((C 1 -C 6 )alkyl), —C(O)N((C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl(C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl), —C(O)N(aryl)((C 1 -C 6 )alkyl), —C(O)N(aryl) 2 , —C(O)N(C 1 -C 6 )alkyl)(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl)(aryl(C 1 -C 6 )alkyl), —C(O)NH((C 1 -C 6 )haloalkyl), —C(O)N((C 1 -C 6 )haloalkyl) 2 , —S(O) 2 NH 2 , —S(O) 2 NH((C 1 -C 6 )alkyl), —S(O) 2 NH((C 1 -C 6 )haloalkyl), —S(O) 2 NH(aryl), —S(O) 2 NH(heteroaryl(C 1 -C 6 )alkyl), —S(O) 2 NH(heteroaryl), —S(O) 2 N((C 1 -C 6 )alkyl) 2 , —S(O) 2 NHC(O)(C 1 -C 6 )alkyl, —S(O) 2 NHC(O)(C 1 -C 6 )haloalkyl, —S(O) 2 NHC(O)aryl, —S(O) 2 NHC(O)aryl(C 1 -C 6 )alkyl, —S(O) 2 NHC(O)heteroaryl, —S(O) 2 NHC(O)heteroaryl(C 1 -C 6 )alkyl, —NHS(O) 2 (C 1 -C 6 )alkyl, —NHS(O) 2 aryl, —NHS(O) 2 (C 1 -C 6 )haloalkyl, —NHS(O) 2 aryl(C 1 -C 6 )alkyl, —NHS(O) 2 heteroaryl, —NHS(O) 2 heteroaryl(C 1 -C 6 )alkyl, —NHC(O)((C 1 -C 6 )alkyl), —NHC(O)((C 1 -C 6 )haloalkyl), —NHC(O)(aryl), —NHC(O)(aryl(C 1 -C 6 )alkyl), —NHC(O)(heteroaryl), —NHC(O)(heteroaryl(C 1 -C 6 )alkyl), —NHC(O)NH(C 1 -C 6 )alkyl, —NHC(O)NH(aryl), —NHC(O)NH(aryl(C 1 -C 6 )alkyl), —NHC(O)NH(heteroaryl), —NHC(O)NH(heteroaryl(C 1 -C 6 )alkyl), —C(O)NHS(O) 2 (C 1 -C 6 )alkyl, —C(O)NHS(O) 2 aryl, C(O)NHS(O) 2 ((C 1 -C 6 )haloalkyl), —C(O)NHS(O) 2 (aryl(C 1 -C 6 )alkyl), —C(O)NHS(O) 2 heteroaryl, —C(O)NHS(O) 2 (heteroaryl(C 1 -C 6 )alkyl), —P(O)(OH) 2 , —((C 1 -C 6 )alkylene)C(O)OH, ((C 1 -C 6 )alkylene)C(O)O(C 1 -C 6 )alkyl, —NH 2 , —NH(C 1 -C 6 )alkyl, —N((C 1 -C 6 )alkyl) 2 , —NC, —CN, —C(S)NH 2 , —NHC(O)NH 2 , (C 1 -C 6 )alkylthio-, (C 1 -C 6 )mercaptoalkyl-, or —C(O)heterocyclyl;

Z is —CH—, —C(O)—, or —C((C 1 -C 3 )alkyl)-;

if Z is —C(O)—, then R 2 is absent,

R 2 is H, halo, (C 1 -C 6 )alkyl, (C 1 -C 6 )alkoxy, (C 1 -C 6 )hydroxyalkyl, (C 1 -C 6 )alkoxy(C 1 -C 6 )alkyl, —CO 2 H, —C(O)O(C 1 -C 6 )alkyl, —C(O)O(aryl), —C(O)O(heteroaryl), —C(O)O(aryl(C 1 -C 6 )alkyl), —C(O)O(heteroaryl(C 1 -C 6 )alkyl), —C(O)NHOH, —C(O)NHCN, —C(O)NH 2 , —C(O)NH((C 1 -C 6 )alkyl), —C(O)N((C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl(C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl), —C(O)N(aryl)((C 1 -C 6 )alkyl), —C(O)N(aryl) 2 , —C(O)N(C 1 -C 6 )alkyl)(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl)(aryl(C 1 -C 6 )alkyl), —C(O)NH((C 1 -C 6 )haloalkyl), —C(O)N((C 1 -C 6 )haloalkyl) 2 , —S(O) 2 NH 2 , —S(O) 2 NH((C 1 -C 6 )alkyl), —S(O) 2 NH((C 1 -C 6 )haloalkyl), —S(O) 2 NH(aryl), —S(O) 2 NH(heteroaryl(C 1 -C 6 )alkyl), —S(O) 2 NH(heteroaryl), —S(O) 2 NH(heteroaryl(C 1 -C 6 )alkyl), —S(O) 2 N((C 1 -C 6 )alkyl) 2 , —S(O) 2 NHC(O)(C 1 -C 6 )alkyl, —S(O) 2 NHC(O)(C 1 -C 6 )haloalkyl, —S(O) 2 NHC(O)aryl, —S(O) 2 NHC(O)aryl(C 1 -C 6 )alkyl, —S(O) 2 NHC(O)heteroaryl, —S(O) 2 NHC(O)heteroaryl(C 1 -C 6 )alkyl, —NHS(O) 2 (C 1 -C 6 )alkyl, —NHS(O) 2 aryl, NHS(O) 2 (C 1 -C 6 )haloalkyl, —NHS(O) 2 aryl(C 1 -C 6 )alkyl, —NHS(O) 2 heteroaryl, —NHS(O) 2 heteroaryl(C 1 -C 6 )alkyl, —NHC(O)((C 1 -C 6 )alkyl), —NHC(O)((C 1 -C 6 )haloalkyl), —NHC(O)(aryl), —NHC(O)(aryl(C 1 -C 6 )alkyl), —NHC(O)(heteroaryl), —NHC(O)(heteroaryl(C 1 -C 6 )alkyl), —NHC(O)NH(C 1 -C 6 )alkyl, —NHC(O)NHaryl, —NHC(O)NH(aryl(C 1 -C 6 )alkyl), —NHC(O)NH(heteroaryl), —NHC(O)NH(heteroaryl(C 1 -C 6 )alkyl), —C(O)NHS(O) 2 (C 1 -C 6 )alkyl, —C(O)NHS(O) 2 aryl, C(O)NHS(O) 2 ((C 1 -C 6 )haloalkyl), —C(O)NHS(O) 2 (aryl(C 1 -C 6 )alkyl), —C(O)NHS(O) 2 heteroaryl, —C(O)NHS(O) 2 (heteroaryl(C 1 -C 6 )alkyl), —P(O)(OH) 2 , aryl(C 1 -C 6 )alkyl, (C 3 -C 7 )cycloalkyl(C 1 -C 6 )alkyl-, —NC, —CN, —C(S)NH 2 , —NHC(O)NH 2 , (C 1 -C 6 )alkylthio-, (C 1 -C 6 )mercaptoalkyl-, or —C(O)heterocyclyl;

R 3 is H, (C 1 -C 3 )alkyl, (C 1 -C 3 )alkoxy(C 1 -C 3 )alkyl, (C 1 -C 3 )alkylthio(C 1 -C 3 )alkyl, (C 1 -C 6 )haloalkyl, —NC, —CN, —C(S)NH 2 , —NHC(O)NH 2 , or —C≡CH;

R 4 is H, (C 1 -C 3 )alkyl, (C 1 -C 3 )alkylthio(C 1 -C 3 )alkyl, (C 1 -C 6 )haloalkyl, (C 1 -C 3 )alkoxy(C 1 -C 3 )alkyl-, or (C 1 -C 4 )hydroxyalkyl;

R 5 is H, halo, —NO 2 , —CN, (C 1 -C 6 )alkyl, (C 1 -C 6 )haloalkyl, —NH 2 , —NH((C 1 -C 6 )alkyl), —N((C 1 -C 6 )alkyl) 2 , —OH, (C 1 -C 6 )alkoxy, hydroxy(C 1 -C 6 )alkyl, (C 1 -C 6 )alkoxy(C 1 -C 6 )alkyl, (C 1 -C 6 )haloalkoxy, —SH, (C 1 -C 3 )alkylthio(C 1 -C 3 )alkyl, —NC, —C(S)NH 2 , —NHC(O)NH 2 , or —C≡CH; and

R 6 is H, halo, —OH, —NH 2 , or —SH; or

R 6 , taken together with the carbon atom bearing it, represents —C(O)—;

wherein:

any occurrence of alkyl, aryl, arylalkyl, heteroaryl, heteroarylalkyl, alkylene, heterocyclyl, cycloalkyl, alkoxy, alkylthio, haloalkyl, or hydroxyalkyl is optionally substituted with one or more substituents independently selected from the group consisting of —OH, halo, —NH 2 , —NH((C 1 -C 6 )alkyl), —N((C 1 -C 6 )alkyl) 2 , —CN, —NO 2 , (C 1 -C 6 )alkyl, (C 1 -C 6 )haloalkyl, (C 1 -C 6 )alkoxy, aryl, heteroaryl, aryl(C 1 -C 6 )alkyl, heteroaryl(C 1 -C 6 )alkyl, (C 3 -C 7 )cycloalkyl, heterocyclyl, —C(O)OH, —C(O)O(C 1 -C 6 )alkyl, —C(O)NH 2 , —C(O)NH(C 1 -C 6 )alkyl, and —C(O)N((C 1 -C 6 )alkyl) 2 ;

or a pharmaceutically acceptable salt, solvate, tautomer, stereoisomer, or polymorph thereof.

2. The method of claim 1 , wherein the disease, disorder, or condition is selected from the group consisting of allergic diseases, acute and chronic inflammatory diseases, autoimmune diseases, dental diseases, neurologic diseases, metabolic diseases, liver diseases, kidney diseases, skin diseases, polycystic ovary syndrome, endometriosis, fibrotic disorders, storage diseases, and cancer.

3. The method of claim 1 , wherein W is fluoro, chloro, bromo, methyl, or methoxy.

4. The method of claim 1 , wherein R 6 is H or —OH.

5. The method of claim 1 , wherein X is a single bond, —CH 2 —, or —C(O)—.

6. The method of claim 1 , wherein Y is a single bond, —CH—, —N—, —O—, or —S(O) 2 —.

7. The method of claim 1 , wherein Y is —CH— or —N—.

8. The method of claim 7 , wherein R 1 is H or (C 1 -C 6 )alkyl.

9. The method of claim 7 , wherein R 1 is —C(O)heterocyclyl selected from the group consisting of

10. The method of claim 7 , wherein R 1 is —CH 2 CO 2 H or —CH 2 C(O)O(C 1 -C 6 )alkyl.

11. The method of claim 1 , wherein Z is —CH—.

12. The method of claim 11 , wherein R 2 is H, halo, (C 1 -C 6 )alkyl, (C 1 -C 6 )alkoxy, (C 1 -C 6 )hydroxyalkyl, (C 1 -C 6 )alkoxy(C 1 -C 6 )alkyl, —CO 2 H, —C(O)O(C 1 -C 6 )alkyl, —C(O)O(aryl), —C(O)O(heteroaryl), —C(O)O(aryl(C 1 -C 6 )alkyl), —C(O)O(heteroaryl(C 1 -C 6 )alkyl), —C(O)NH 2 , —C(O)NH((C 1 -C 6 )alkyl), —C(O)N((C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl(C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl), —C(O)N(aryl)((C 1 -C 6 )alkyl), —C(O)N(aryl) 2 , —C(O)N(C 1 -C 6 )alkyl)(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl)(aryl(C 1 -C 6 )alkyl), —C(O)NH((C 1 -C 6 )haloalkyl), —C(O)N((C 1 -C 6 )haloalkyl) 2 , aryl(C 1 -C 6 )alkyl, (C 3 -C 7 )cycloalkyl(C 1 -C 6 )alkyl-, or —C(O)heterocyclyl.

13. The method of claim 11 , wherein R 2 is H, (C 1 -C 6 )alkyl, or (C 1 -C 6 )alkoxy(C 1 -C 6 )alkyl.

14. The method of claim 11 , wherein R 2 is —C(O)heterocyclyl selected from the group consisting of

15. The method of claim 1 , wherein:

W is bromo or chloro;

X is a single bond, —CH 2 —, or —C(O)—;

Y is a single bond, —CH—, —N—, —O—, or —S(O) 2 —;

if Y is a single bond, —O—, or —S(O) 2 —, then R 1 is absent;

R 1 is H, methyl, isobutyl, methoxy, acetyl, methoxycarbonyl, methanesulfonyl, p-toluenesulfonyl, methoxycarbonylmethyl, or carboxymethyl;

Z is —CH—, —C(O)—, or —C(CH 3 )—;

if Z is —C(O)—, then R 2 is absent;

R 2 is H, methyl, ethyl, isopropyl, isobutyl, —C(O)NH 2 , —C(O)NHMe, —CH 2 OH, —CH 2 OCH 3 , —CH 2 OCH 2 CH 3 , —C(CH 3 ) 2 OH, —C(CH 3 ) 2 OCH 3 , —CO 2 H, —CO 2 CH 2 CH 3 , —OCH 3 , —F, —CH 2 -(p-chlorophenyl), or —CH 2 -cyclohexyl;

R 3 , R 4 , and R 5 are each H; and

R 6 is H or OH.

16. The method of claim 1 , wherein said compound is selected from the group consisting of:

17. The method of claim 16 , wherein the disease, disorder, or condition is selected from the group consisting of allergic diseases, acute and chronic inflammatory diseases, autoimmune diseases, dental diseases, neurologic diseases, metabolic diseases, liver diseases, kidney diseases, skin diseases, polycystic ovary syndrome, endometriosis, fibrotic disorders, storage diseases, and cancer.

18. The method of claim 1 , wherein said compound is represented by:

19. The method of claim 18 , wherein the disease, disorder, or condition is selected from the group consisting of allergic diseases, acute and chronic inflammatory diseases, autoimmune diseases, dental diseases, neurologic diseases, metabolic diseases, liver diseases, kidney diseases, skin diseases, polycystic ovary syndrome, endometriosis, fibrotic disorders, storage diseases, and cancer.

20. A method for the therapeutic treatment of a disease, disorder, or condition associated with aberrant expression or activity of chitotriosidase, comprising administering to a human in need thereof a therapeutically effective amount of a compound, wherein said compound is represented by formula (I):

wherein:

W is halo, (C 1 -C 3 )alkyl, (C 1 -C 3 )alkoxy-, or (C 1 -C 3 )alkylthio-;

X is a single bond, —CH 2 —, —CH 2 CH 2 —, —CH═CH—, or —C(O)—;

Y is a single bond, —CH—, —CHCH 2 —, —CH 2 CH—, —C═CH—, —CH═C—, —N—, —O—, —S(O)—, or —S(O) 2 —;

if Y is a single bond, —O—, —S(O)—, or —S(O) 2 —, then R 1 is absent;

R 1 is H, (C 1 -C 6 )alkyl, (C 1 -C 6 )haloalkyl, (C 1 -C 6 )alkoxy, (C 1 -C 6 )hydroxyalkyl, (C 1 -C 6 )alkoxy(C 1 -C 6 )alkyl, aryl(C 1 -C 6 )alkyl, heteroaryl(C 1 -C 6 )alkyl, —C(O)(C 1 -C 6 )alkyl, —C(O)aryl, —C(O)heteroaryl, —C(O)aryl(C 1 -C 6 )alkyl, —C(O)heteroaryl(C 1 -C 6 )alkyl, —S(O) 2 (C 1 -C 6 )alkyl, —S(O) 2 aryl, —S(O) 2 heteroaryl, —S(O) 2 aryl(C 1 -C 6 )alkyl, —S(O) 2 heteroaryl(C 1 -C 6 )alkyl, —CO 2 H, —C(O)O(C 1 -C 6 )alkyl, —C(O)O(aryl), —C(O)O(heteroaryl), —C(O)O(aryl(C 1 -C 6 )alkyl), —C(O)O(heteroaryl(C 1 -C 6 )alkyl), —C(O)NH 2 , —C(O)NHOH, —C(O)NHCN, —C(O)NH((C 1 -C 6 )alkyl), —C(O)N((C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl(C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl), —C(O)N(aryl)((C 1 -C 6 )alkyl), —C(O)N(aryl) 2 , —C(O)N(C 1 -C 6 )alkyl)(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl)(aryl(C 1 -C 6 )alkyl), —C(O)NH((C 1 -C 6 )haloalkyl), —C(O)N((C 1 -C 6 )haloalkyl) 2 , —S(O) 2 NH 2 , —S(O) 2 NH((C 1 -C 6 )alkyl), —S(O) 2 NH((C 1 -C 6 )haloalkyl), —S(O) 2 NH(aryl), —S(O) 2 NH(heteroaryl(C 1 -C 6 )alkyl), —S(O) 2 NH(heteroaryl), —S(O) 2 N((C 1 -C 6 )alkyl) 2 , —S(O) 2 NHC(O)(C 1 -C 6 )alkyl, —S(O) 2 NHC(O)(C 1 -C 6 )haloalkyl, —S(O) 2 NHC(O)aryl, —S(O) 2 NHC(O)aryl(C 1 -C 6 )alkyl, —S(O) 2 NHC(O)heteroaryl, —S(O) 2 NHC(O)heteroaryl(C 1 -C 6 )alkyl, —NHS(O) 2 (C 1 -C 6 )alkyl, —NHS(O) 2 aryl, —NHS(O) 2 (C 1 -C 6 )haloalkyl, —NHS(O) 2 aryl(C 1 -C 6 )alkyl, —NHS(O) 2 heteroaryl, —NHS(O) 2 heteroaryl(C 1 -C 6 )alkyl, —NHC(O)((C 1 -C 6 )alkyl), —NHC(O)((C 1 -C 6 )haloalkyl), —NHC(O)(aryl), —NHC(O)(aryl(C 1 -C 6 )alkyl), —NHC(O)(heteroaryl), —NHC(O)(heteroaryl(C 1 -C 6 )alkyl), —NHC(O)NH(C 1 -C 6 )alkyl, —NHC(O)NH(aryl), —NHC(O)NH(aryl(C 1 -C 6 )alkyl), —NHC(O)NH(heteroaryl), —NHC(O)NH(heteroaryl(C 1 -C 6 )alkyl), —C(O)NHS(O) 2 (C 1 -C 6 )alkyl, —C(O)NHS(O) 2 aryl, C(O)NHS(O) 2 ((C 1 -C 6 )haloalkyl), —C(O)NHS(O) 2 (aryl(C 1 -C 6 )alkyl), —C(O)NHS(O) 2 heteroaryl, —C(O)NHS(O) 2 (heteroaryl(C 1 -C 6 )alkyl), —P(O)(OH) 2 , —((C 1 -C 6 )alkylene)C(O)OH, ((C 1 -C 6 )alkylene)C(O)O(C 1 -C 6 )alkyl, —NH 2 , —NH(C 1 -C 6 )alkyl, —N((C 1 -C 6 )alkyl) 2 , —NC, —CN, —C(S)NH 2 , —NHC(O)NH 2 , (C 1 -C 6 )alkylthio-, (C 1 -C 6 )mercaptoalkyl-, or —C(O)heterocyclyl;

Z is —CH—, —C(O)—, or —C((C 1 -C 3 )alkyl)-;

if Z is —C(O)—, then R 2 is absent,

R 2 is H, halo, (C 1 -C 6 )alkyl, (C 1 -C 6 )alkoxy, (C 1 -C 6 )hydroxyalkyl, (C 1 -C 6 )alkoxy(C 1 -C 6 )alkyl, —CO 2 H, —C(O)O(C 1 -C 6 )alkyl, —C(O)O(aryl), —C(O)O(heteroaryl), —C(O)O(aryl(C 1 -C 6 )alkyl), —C(O)O(heteroaryl(C 1 -C 6 )alkyl), —C(O)NHOH, —C(O)NHCN, —C(O)NH 2 , —C(O)NH((C 1 -C 6 )alkyl), —C(O)N((C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl(C 1 -C 6 )alkyl) 2 , —C(O)NH(aryl), —C(O)N(aryl)((C 1 -C 6 )alkyl), —C(O)N(aryl) 2 , —C(O)N(C 1 -C 6 )alkyl)(aryl(C 1 -C 6 )alkyl), —C(O)N(aryl)(aryl(C 1 -C 6 )alkyl), —C(O)NH((C 1 -C 6 )haloalkyl), —C(O)N((C 1 -C 6 )haloalkyl) 2 , —S(O) 2 NH 2 , —S(O) 2 NH((C 1 -C 6 )alkyl), —S(O) 2 NH((C 1 -C 6 )haloalkyl), —S(O) 2 NH(aryl), —S(O) 2 NH(heteroaryl(C 1 -C 6 )alkyl), —S(O) 2 NH(heteroaryl), —S(O) 2 NH(heteroaryl(C 1 -C 6 )alkyl), —S(O) 2 N((C 1 -C 6 )alkyl) 2 , —S(O) 2 NHC(O)(C 1 -C 6 )alkyl, —S(O) 2 NHC(O)(C 1 -C 6 )haloalkyl, —S(O) 2 NHC(O)aryl, —S(O) 2 NHC(O)aryl(C 1 -C 6 )alkyl, —S(O) 2 NHC(O)heteroaryl, —S(O) 2 NHC(O)heteroaryl(C 1 -C 6 )alkyl, —NHS(O) 2 (C 1 -C 6 )alkyl, —NHS(O) 2 aryl, NHS(O) 2 (C 1 -C 6 )haloalkyl, —NHS(O) 2 aryl(C 1 -C 6 )alkyl, —NHS(O) 2 heteroaryl, —NHS(O) 2 heteroaryl(C 1 -C 6 )alkyl, —NHC(O)((C 1 -C 6 )alkyl), —NHC(O)((C 1 -C 6 )haloalkyl), —NHC(O)(aryl), —NHC(O)(aryl(C 1 -C 6 )alkyl), —NHC(O)(heteroaryl), —NHC(O)(heteroaryl(C 1 -C 6 )alkyl), —NHC(O)NH(C 1 -C 6 )alkyl, —NHC(O)NHaryl, —NHC(O)NH(aryl(C 1 -C 6 )alkyl), —NHC(O)NH(heteroaryl), —NHC(O)NH(heteroaryl(C 1 -C 6 )alkyl), —C(O)NHS(O) 2 (C 1 -C 6 )alkyl, —C(O)NHS(O) 2 aryl, C(O)NHS(O) 2 ((C 1 -C 6 )haloalkyl), —C(O)NHS(O) 2 (aryl(C 1 -C 6 )alkyl), —C(O)NHS(O) 2 heteroaryl, —C(O)NHS(O) 2 (heteroaryl(C 1 -C 6 )alkyl), —P(O)(OH) 2 , aryl(C 1 -C 6 )alkyl, (C 3 -C 7 )cycloalkyl(C 1 -C 6 )alkyl-, —NC, —CN, —C(S)NH 2 , —NHC(O)NH 2 , (C 1 -C 6 )alkylthio-, (C 1 -C 6 )mercaptoalkyl-, or —C(O)heterocyclyl;

R 3 is H, (C 1 -C 3 )alkyl, (C 1 -C 3 )alkoxy(C 1 -C 3 )alkyl, (C 1 -C 3 )alkylthio(C 1 -C 3 )alkyl, (C 1 -C 6 )haloalkyl, —NC, —CN, —C(S)NH 2 , —NHC(O)NH 2 , or —C≡CH;

R 4 is H, (C 1 -C 3 )alkyl, (C 1 -C 3 )alkylthio(C 1 -C 3 )alkyl, (C 1 -C 6 )haloalkyl, (C 1 -C 3 )alkoxy(C 1 -C 3 )alkyl-, or (C 1 -C 4 )hydroxyalkyl;

R 5 is H, halo, —NO 2 , —CN, (C 1 -C 6 )alkyl, (C 1 -C 6 )haloalkyl, —NH 2 , —NH((C 1 -C 6 )alkyl), —N((C 1 -C 6 )alkyl) 2 , —OH, (C 1 -C 6 )alkoxy, hydroxy(C 1 -C 6 )alkyl, (C 1 -C 6 )alkoxy(C 1 -C 6 )alkyl, (C 1 -C 6 )haloalkoxy, —SH, (C 1 -C 3 )alkylthio(C 1 -C 3 )alkyl, —NC, —C(S)NH 2 , —NHC(O)NH 2 , or —C≡CH; and

R 6 is H, halo, —OH, —NH 2 , or —SH; or

R 6 , taken together with the carbon atom bearing it, represents —C(O)—;

wherein:

any occurrence of alkyl, aryl, arylalkyl, heteroaryl, heteroarylalkyl, alkylene, heterocyclyl, cycloalkyl, alkoxy, alkylthio, haloalkyl, or hydroxyalkyl is optionally substituted with one or more substituents independently selected from the group consisting of —OH, halo, —NH 2 , —NH((C 1 -C 6 )alkyl), —N((C 1 -C 6 )alkyl) 2 , —CN, —NO 2 , (C 1 -C 6 )alkyl, (C 1 -C 6 )haloalkyl, (C 1 -C 6 )alkoxy, aryl, heteroaryl, aryl(C 1 -C 6 )alkyl, heteroaryl(C 1 -C 6 )alkyl, (C 3 -C 7 )cycloalkyl, heterocyclyl, —C(O)OH, —C(O)O(C 1 -C 6 )alkyl, —C(O)NH 2 , —C(O)NH(C 1 -C 6 )alkyl, and —C(O)N((C 1 -C 6 )alkyl) 2 ;

or a pharmaceutically acceptable salt, solvate, tautomer, stereoisomer, or polymorph thereof.

21. The method of claim 20 , wherein:

W is bromo or chloro;

X is a single bond, —CH 2 —, or —C(O)—;

Y is a single bond, —CH—, —N—, —O—, or —S(O) 2 —;

if Y is a single bond, —O—, or —S(O) 2 —, then R 1 is absent;

R 1 is H, methyl, isobutyl, methoxy, acetyl, methoxycarbonyl, methanesulfonyl, p-toluenesulfonyl, methoxycarbonylmethyl, or carboxymethyl;

Z is —CH—, —C(O)—, or —C(CH 3 )—;

if Z is —C(O)—, then R 2 is absent;

R 2 is H, methyl, ethyl, isopropyl, isobutyl, —C(O)NH 2 , —C(O)NHMe, —CH 2 OH, —CH 2 OCH 3 , —CH 2 OCH 2 CH 3 , —C(CH 3 ) 2 OH, —C(CH 3 ) 2 OCH 3 , —CO 2 H, —CO 2 CH 2 CH 3 , —OCH 3 , —F, —CH 2 -(p-chlorophenyl), or —CH 2 -cyclohexyl;

R 3 , R 4 , and R 5 are each H; and

R 6 is H or OH.

22. The method of claim 20 , wherein said compound is selected from the group consisting of:

23. The method of claim 20 , wherein said compound is represented by:

Assignments (5)
RELEASE OF SECURITY INTEREST Recorded Feb 17, 2023
From: GILEAD SCIENCES, INC.
To: GALAPAGOS NV
Reel/Frame 062733/0145 →
CHANGE OF NAME Recorded Aug 4, 2022
From: ONCOARENDI THERAPEUTICS S.A.
To: MOLECURE S.A.
Reel/Frame 061072/0709 →
SECURITY INTEREST Recorded Feb 15, 2022
From: GALAPAGOS NV
To: GILEAD SCIENCES, INC
Reel/Frame 059020/0896 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 12, 2018
From: MAZUR, MARZENA; KORALEWSKI, ROBERT; BOREK, BARTLOMIEJ; OLEJNICZAK, SYLWIA; CZESTKOWSKI, WOJCIECH; PIOTROWICZ, MICHAL C.; OLCZAK, JACEK; GOLEBIOWSKI, ADAM A.; BARTOSZEWICZ, AGNIESZKA; MAZIARZ, ELZBIETA; KOWALSKI, MICHAL L.
To: ONCOARENDI THERAPEUTICS SP Z O.O.
Reel/Frame 046334/0514 →
CHANGE OF NAME Recorded Jul 12, 2018
From: ONCOARENDI THERAPEUTICS SP Z O.O.
To: ONCOARENDI THERAPEUTICS S.A.
Reel/Frame 046570/0525 →
Continuity (3)
Continuation 15255226 · Sep 2, 2016
Continuation 62214299 · Sep 4, 2015
Related Publication 20180258071A1 · Sep 13, 2018
Cited By (1)
US 12,319,677