IP Library Granted Patent US 10,680,234
Granted Patent B2
US 10,680,234 · App. 15/938,026 · Granted Jun 9, 2020

Lithium-sulfur battery with polyanthraquinone binder

Inventors: Chen Liao (Westmont, IL); Ka-Cheong Lau (Chicago, IL)
Assignee: UCHICAGO ARGONNE, LLC
H01M4/136H01M4/583H01M4/623H01M4/661
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Quick Facts
Patent No.
US 10,680,234
App. No.
15/938,026
Granted
Jun 9, 2020
Kind
B2
Abstract

A cathode for a lithium-sulfur (Li—S) battery is described herein, which comprises elemental sulfur (e.g., S 8 ) and an electroactive polyanthraquinone-containing binder. In some embodiments, the cathode also includes a conductive carbon material in addition to the sulfur and binder. Also described herein is a Li—S battery comprising the cathode, in combination with a metallic lithium-containing anode, a lithium conductive separator membrane between the anode and the cathode, and a liquid electrolyte comprising a lithium salt dissolved in a non-aqueous organic solvent.

Claims (24)

1. A lithium-sulfur (Li—S) battery cathode comprising elemental sulfur dispersed in a binder comprising 2,6-polyanthraquinone.

2. The cathode of claim 1 , further comprising a current collector contacting the sulfur and the binder.

3. The cathode of claim 1 , wherein the elemental sulfur and the binder are coated on an aluminum current collector.

4. The cathode of claim 1 , wherein the cathode further comprises a carbon material dispersed in the binder.

5. The cathode of claim 1 , wherein the 2,6-polyanthraquinone has a number average molecular weight of about 60 kDa to 80 kDa and a polydispersity index of about 2 to about 2.2, as determined by reduction of the 2,6-polyanthraquinone with about 2 equivalents of lithium naphthalenide per anthraquinone unit thereof, followed by gel permeation size exclusion chromatography using a chromatography medium comprising a highly cross-linked polystyrene-divinylbenzene gel and narrow dispersity polystyrene standards with tetrahydrofuran as eluent.

6. The cathode of claim 1 , wherein the 2,6-polyanthraquinone comprises about 50 to about 66 percent by weight (wt %) of the binder.

7. The cathode of claim 1 , wherein the 2,6-polyanthraquinone comprises about 50 wt % of the binder.

8. The cathode of claim 1 , wherein the binder further comprises at least one other binder compound in combination with the 2,6-polyanthraquinone.

9. The cathode of claim 8 , wherein the at least one other binder compound comprises polyvinylidene difluoride.

10. The cathode of claim 1 , wherein the cathode comprises about 50 wt % of S 8 , about 20 to about 40 wt % of a carbon material, and about 10 to about 30 wt % of the binder.

11. A lithium-sulfur (Li—S) battery comprising:

(a) an anode comprising metallic lithium;

(b) a cathode comprising elemental sulfur dispersed in a binder comprising 2,6-polyanthraquinone;

(c) a porous separator membrane between the anode and the cathode; and

(d) a liquid electrolyte composition comprising a lithium salt dissolved in a non-aqueous organic solvent contacting the anode, the cathode, and the membrane.

12. The battery of claim 11 , wherein the cathode further comprises a current collector contacting the sulfur and the binder.

13. The battery of claim 11 , wherein the elemental sulfur and the 2,6-polyanthraquinone are coated on an aluminum current collector.

14. The battery of claim 11 , wherein the cathode further comprises a carbon material dispersed in the binder.

15. The battery of claim 11 , wherein the 2,6-polyanthraquinone has a number average molecular weight of about 60 kDa to 80 kDa and a polydispersity index of about 2 to about 2.2, as determined by reduction of the 2,6-polyanthraquinone with about 2 equivalents of lithium naphthalenide per anthraquinone unit thereof, followed by gel permeation size exclusion chromatography using a chromatography medium comprising a highly cross-linked polystyrene-divinylbenzene gel and narrow dispersity polystyrene standards with tetrahydrofuran as eluent.

16. The battery of claim 11 , wherein the 2,6-polyanthraquinone comprises about 50 to about 66 wt % of the binder.

17. The battery of claim 11 , wherein the 2,6-polyanthraquinone comprises about 50 wt % of the binder.

18. The battery of claim 11 , wherein the binder comprises at least one other binder compound in combination with the 2,6-polyanthraquinone.

19. The battery of claim 18 , wherein the at least one other binder compound comprises polyvinylidene difluoride.

20. The battery of claim 11 , wherein the cathode comprises about 50 wt % of S 8 , about 20 to about 40 wt % of a carbon material, and about 10 to about 30 wt % of the binder.

Assignments (2)
CONFIRMATORY LICENSE Recorded Nov 22, 2019
From: UCHICAGO ARGONNE, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 051097/0430 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 19, 2018
From: LIAO, CHEN; LAU, KA-CHEONG
To: UCHICAGO ARGONNE, LLC
Reel/Frame 046397/0427 →
Continuity (1)
Related Publication 20190305296A1 · Oct 3, 2019