IP Library Granted Patent US 11,505,838
Granted Patent B2
US 11,505,838 · App. 15/945,773 · Granted Nov 22, 2022

Method for producing a sugar stream

Inventors: Neal Jakel (Cedar Rapids, IA); Albert Pollmeier (Cedar Rapids, IA)
Assignee: Fluid Quip Technologies, LLC
C13K13/00A23L7/104A23L7/107A23L29/35C12M21/00C12P7/06C12P7/16C12P19/02C12P19/14C13K1/06
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Quick Facts
Patent No.
US 11,505,838
App. No.
15/945,773
Granted
Nov 22, 2022
Kind
B2
Abstract

An improved dry grind system and method for producing a sugar stream from grains or similar carbohydrate sources and/or residues, such as for biochemical production. In particular, after saccharification and prior to a sugar conversion process, a sugar/carbohydrate stream is removed from a saccharified stream. The sugar/carbohydrate stream includes a desired Dextrose Equivalent (DE) where DE describes the degree of conversion of starch to dextrose can be produced, with the such sugar stream being available for biochemical production, e.g., alcohol production, or other processes. In addition, the systems and methods also can involve the removal of certain grain components, e.g., corn kernel components, including protein and/or fiber. Sugar stream production occurs on the front end of the system and method.

Claims (31)

1. A method for producing a sugar stream from a grain feedstock, comprising:

mixing ground grain particles derived from an initial feedstock of grain and/or grain components with a liquid to produce a slurry that comprises starch;

subjecting the slurry to liquefaction to provide a liquified starch solution, which includes solids;

prior to saccharification, separating a first portion of the liquefied starch solution, via a paddle screen, into a solids portion and a liquid portion, wherein the liquid portion includes starch, and subjecting a second portion of the liquefied starch solution, which comprises the remaining portion of the solids, directly to an ethanol fermentation process;

thereafter, subjecting the liquid portion to saccharification to convert the starch to simple sugars and produce a saccharified stream that comprises the simple sugars;

after saccharification but prior to further processing of the simple sugars, directly separating the entire saccharified stream, via microfiltration, into a first solids portion and a first liquid portion that comprises the simple sugars, wherein the first liquid portion comprises a sugar stream having a dextrose equivalent of at least 20 DE and a total unfermentable solids fraction that is less than or equal to 30% of a total solids content and;

thereafter, rejoining the solids portion, obtained by subjecting the first portion of the liquefied starch solution to the separation via the paddle screen, with the first solids portion, obtained by subjecting the saccharified stream to the microfiltration, to provide a rejoined solids portion, and separately subjecting the rejoined solids portion, which comprises residual sugars, directly to the ethanol fermentation process along with the second portion of the liquefied starch solution, which includes the remaining portion of the solids, whereby the residual sugars are fermented.

2. The method of claim 1 further comprising, after mixing the grain particles with the liquid to produce the slurry and prior to subjecting the slurry to liquefaction, separating the slurry into a slurry solids portion and a slurry liquid portion that comprises the starch, grinding the slurry solids portion to produce a ground slurry solids portion, and rejoining the slurry liquid portion with the ground slurry solids portion to reconstitute the slurry prior to subjecting the slurry to liquefaction.

3. The method of claim 1 further comprising subjecting at least a portion of the sugar stream to at least one of carbon filtration, ion exchange, or evaporation.

4. The method of claim 1 further comprising subjecting at least a portion of the sugar stream to at least one of carbon filtration, ion exchange, or evaporation followed by a sugar conversion process to produce a biochemical.

5. The method of claim 4 wherein the sugar conversion process is fermentation.

6. The method of claim 4 wherein the sugar conversion process includes a catalytic or chemical reaction.

7. The method of claim 1 further comprising subjecting at least a portion of the sugar stream to carbon filtration, followed by ion exchange, and followed by evaporation.

8. The method of claim 1 further comprising subjecting at least a portion of the sugar stream to a sugar conversion process to produce a biochemical.

9. A method for producing a sugar stream from a grain feedstock, comprising:

mixing ground grain particles derived from an initial feedstock of grain and/or grain components with a liquid to produce a slurry that comprises starch;

subjecting the slurry to liquefaction to provide a liquefied starch solution;

prior to saccharification, mechanically separating a first portion of the liquefied starch solution into a solids portion and a liquid portion, wherein the liquid portion includes starch, and subjecting a second portion of the liquefied starch solution, which comprises the remaining portion of the solids, directly to an ethanol fermentation process;

thereafter, subjecting the liquid portion to saccharification to convert the starch to simple sugars and produce a saccharified stream that comprises the simple sugars;

after saccharification but prior to further processing of the simple sugars, directly separating the entire saccharified stream into a first solids portion and a first liquid portion that comprises the simple sugars, wherein the first liquid portion comprises a sugar stream having a dextrose equivalent of at least 20 DE and a total unfermentable solids fraction that is less than or equal to 30% of a total solids content; and

thereafter, rejoining the solids portion, obtained by mechanically separating the first portion of the liquefied starch solution, with the separated first solids portion to provide a rejoined solids portion, and separately subjecting the rejoined solids portion, which comprises residual sugars, directly to the ethanol fermentation process along with the second portion of the liquefied starch solution, which includes the remaining portion of the solids, whereby the residual sugars are fermented.

10. The method of claim 9 further comprising subjecting at least a portion of the sugar stream to a sugar conversion process to produce a biochemical.

11. The method of claim 9 further comprising subjecting at least a portion of the sugar stream to at least one of carbon filtration, ion exchange, or evaporation followed by a sugar conversion process to produce a biochemical.

12. The method of claim 11 wherein subjecting at least a portion of the sugar stream to at least one of carbon filtration, ion exchange, or evaporation comprises subjecting at least a portion of the sugar stream to carbon filtration, followed by ion exchange, followed by evaporation, and then followed by the sugar conversion process to produce a biochemical.

13. The method of claim 9 wherein after saccharification but prior to further processing of the simple sugars, the saccharified stream is separated, via filtration, into a first solids portion and a first liquid portion that comprises the simple sugars.

14. The method of claim 13 wherein the filtration is microfiltration.

15. The method of claim 9 wherein mechanically separating the first portion of the liquefied starch solution comprises mechanically separating the first portion of the liquefied starch solution, via a paddle screen, into a solids portion and a liquid portion, wherein the liquid portion includes starch.

16. The method of claim 9 further comprising, after mixing the grain particles with the liquid to produce the slurry and prior to subjecting the slurry to liquefaction, separating the slurry into a slurry solids portion and a slurry liquid portion that comprises the starch, grinding the slurry solids portion to produce a ground slurry solids portion, and rejoining the slurry liquid portion with the ground slurry solids portion prior to subjecting the slurry to liquefaction.

17. The method of claim 10 wherein the sugar conversion process is fermentation.

18. The method of claim 10 wherein the sugar conversion process includes a catalytic or chemical reaction.

19. The method of claim 9 further comprising subjecting at least a portion of the sugar stream to at least one of carbon filtration, ion exchange, or evaporation.

Assignments (2)
CHANGE OF NAME Recorded Jun 14, 2019
From: FLUID QUIP PROCESS TECHNOLOGIES, LLC
To: FLUID QUIP TECHNOLOGIES, LLC
Reel/Frame 049476/0914 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 10, 2018
From: JAKEL, NEAL; POLLMEIER, ALBERT
To: FLUID QUIP PROCESS TECHNOLOGIES, LLC
Reel/Frame 046610/0620 →
Continuity (1)
Related Publication 20190309377A1 · Oct 10, 2019