IP Library Granted Patent US 10,485,878
Granted Patent B2
US 10,485,878 · App. 15/990,111 · Granted Nov 26, 2019

PSMA binding ligand-linker conjugates and methods for using

Inventors: Philip S. Low (West Lafayette, IN); Sumith A. Kularatne (West Lafayette, IN)
Assignee: Purdue Research Foundation
A61K47/64A61K31/426A61K31/475A61K31/4745A61K47/54A61K47/542A61K47/547A61K47/548A61K49/0041A61K49/0043A61K49/0052A61K49/0056A61K51/04A61K51/0402A61K51/0489A61K51/088C07C323/52C07D207/416C07K5/08
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Quick Facts
Patent No.
US 10,485,878
App. No.
15/990,111
Granted
Nov 26, 2019
Kind
B2
Abstract

Described herein are prostate specific membrane antigen (PSMA) binding conjugates that are useful for delivering therapeutic, diagnostic and imaging agents. Also described herein are pharmaceutical composition containing them and methods of using the conjugates and compositions. Also described are processes for manufacture of the conjugates and the compositions containing them.

Claims (26)

1. A compound of the formula

B-L-D

or a salt thereof, wherein

B is a ligand of prostate specific membrane antigen (PSMA) comprising a urea of two amino acids, wherein each amino acid is independently an aminoalkylcarboxylate substituted with alkyl, hydroxyalkyl, sulfhydrylalkyl, aminoalkyl, or carboxyalkyl;

L is a linker comprising a carbonyl and a divalent radical selected from the group consisting of alkane, alkene, alkyne, cycloalkane, arylene, and imide and the linker has a molecular weight of 30 to 300 g/mol; and

D is a radioisotope covalently bound to the linker.

2. The compound of claim 1 or a salt thereof, wherein B is of the formula

wherein R 1 is hydrogen and R 2 is a substituted carboxylic acid, wherein the substituted carboxylic acid is covalently bound to the linker.

3. The compound of claim 1 or a salt thereof, wherein the divalent radical is an arylene.

4. The compound of claim 2 or a salt thereof, wherein the divalent radical is an arylene.

5. A pharmaceutical composition comprising a compound of claim 1 or a salt thereof and optionally at least one pharmaceutically acceptable carrier, excipient, or a combination thereof.

6. The compound of claim 1 or a salt thereof, wherein the linker comprises nitrogen atoms.

7. The compound of claim 1 or a salt thereof, wherein the carbonyl of the linker is substituted with one or more substituents X 1 selected from the group consisting of alkyl, alkoxy, alkoxyalkyl, hydroxy, hydroxyalkyl, amino, amino alkyl, alkylaminoalkyl, dialkylaminoalkyl, halo, haloalkyl, sulfhydrylalkyl, alkylthioalkyl, aryl, substituted aryl, arylalkyl, substituted arylalkyl, heteroaryl, substituted heteroaryl, carboxy, carboxyalkyl, alkyl carboxylate, alkyl alkanoate, guanidinoalkyl, R 4 -carbonyl, R 5 -carbonylalkyl, R 6 -acylamino, and R 7 -acylaminoalkyl, wherein R 4 , R 5 , R 6 and R 7 are each independently selected from amino acids, amino acid derivatives, and peptides.

8. The compound of claim 1 or a salt thereof, wherein the linker is covalently bound to B via an amide bond.

9. The compound of claim 1 or a salt thereof, wherein the linker is a linear chain at least 5 atoms in length.

10. The compound of claim 1 or a salt thereof, wherein the linker is about 7 atoms in length.

11. The compound of claim 1 or a salt thereof, wherein the linker is about 7 atoms to about 20 atoms in length.

12. A reconstitutable lyophilizate comprising a compound of claim 1 or a salt thereof.

13. The reconstitutable lyophilizate of claim 12 , wherein the lyophilizate comprises a dose of the compound of claim 1 or a salt thereof.

14. A kit comprising the reconstitutable lyophilizate of claim 12 .

15. A compound of the formula

B-L-D

or a salt thereof, wherein

B is a ligand of prostate specific membrane antigen (PSMA) comprising a urea of two amino acids, wherein each amino acid is independently an aminoalkylcarboxylate substituted with alkyl, hydroxyalkyl, sulfhydrylalkyl, amino alkyl, or carboxyalkyl;

L is a linker comprising a carbonyl and a divalent radical selected from the group consisting of alkane, alkene, alkyne, cycloalkane, arylene, and imide and the linker does not have an arylalkyl sidechain; and

D is a radioisotope covalently bound to the linker.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 10, 2019
From: LOW, PHILIP STEWART; KULARATNE, SUMITH A.
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 051224/0323 →
Continuity (6)
Continuation 15606913 · May 26, 2017
Continuation 14794482 · Jul 8, 2015
Continuation 12673931
Provisional Application 61074358 · Jun 20, 2008
Provisional Application 60956489 · Aug 17, 2007
Related Publication 20180289827A1 · Oct 11, 2018
Cited By (6)
US 12,208,102 US 12,297,218 US 12,324,846 US 12,473,265 US 12,496,292 US 12,655,115