IP Library › Granted Patent US 10,435,576
Granted Patent B2
US 10,435,576 · App. 15/990,234 · Granted Oct 8, 2019

Water soluble polymer compositions

Inventors: Philip Brunner (Hudson, WI); Gavriel DePrenger-Gottfried (Hudson, WI); Nathan Ockwig (Eagan, MN)
Assignee: Infinite Material Solutions, LLC
C09D11/38B29C64/40B33Y70/00C08K5/1535C09D11/102C09D11/106C09D11/14B29K2029/00B29K2995/0062B33Y80/00
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Quick Facts
Patent No.
US 10,435,576
App. No.
15/990,234
Granted
Oct 8, 2019
Kind
B2
Abstract

A water soluble polymer composition includes a water soluble polymer and a sugar and may be used as a support in additive manufacturing processes.

Claims (24)

1. A water soluble polymer composition comprising:

a semi-crystalline water soluble polymer; and

a sugar having a melting point of at least 200° C.;

wherein the semi-crystalline water soluble polymer and the sugar are melt processable and substantially miscible and form a water soluble polymer composition; and

wherein the water soluble polymer composition is substantially dry.

2. The water soluble polymer composition of claim 1 , wherein the water soluble polymer composition is substantially stable at a build chamber temperature of at least about 140° C.

3. The water soluble polymer composition of claim 1 , wherein the water soluble polymer composition is substantially stable at a build chamber temperature of at least about 150° C.

4. The water soluble polymer composition of claim 1 , wherein the water soluble polymer composition is substantially stable at a build chamber temperature of at least about 170° C.

5. The water soluble polymer composition of claim 1 , wherein the water soluble polymer composition is substantially stable at a build chamber temperature of at least about 190° C.

6. The water soluble polymer composition of claim 1 , wherein the water soluble polymer composition is substantially stable at a build chamber temperature of at least about 210° C.

7. The water soluble polymer composition according to claim 1 , wherein the semi-crystalline water soluble polymer comprises butendiol vinylalcohol copolymer.

8. The water soluble polymer composition according to claim 1 , wherein the sugar comprises trehalose.

9. The water soluble polymer composition according to claim 1 , further comprising one or more additives or further polymers.

10. The water soluble polymer composition according to claim 1 , wherein the water soluble polymer composition is semi-crystalline.

11. The water soluble polymer composition according to claim 1 , wherein the water soluble polymer composition has a dissolution rate of at least about 400 mg/min according to Dissolution Test Method 2.

12. The water soluble polymer composition according to claim 1 , wherein the water soluble polymer composition has a dissolution rate of at least about 600 mg/min as determined by Dissolution Test Method 2.

13. A water soluble support composition comprising: a semi-crystalline water soluble polymer having a dissolution rate of at least 100 mg/min according to Dissolution Test Method 2 and is substantially stable at build chamber temperatures of at least 140° C.

14. A water soluble support composition of claim 13 , wherein the semi-crystalline water soluble polymer is drawn down during processing.

15. A three-dimensional printed article comprising:

a three-dimensional printed object generally disposed on a substantially horizontal build plate; and

one or more soluble supports positioned about and supporting one or more portions of the three-dimensional printed object, the soluble supports comprising a water soluble polymer composition;

wherein the water soluble polymer composition is formed by melt processing a semi-crystalline water soluble polymer and a sugar having a melting point of at least 200° C.; and

wherein the semi-crystalline water soluble polymer and the sugar are substantially miscible.

16. The three-dimensional printed article according to claim 15 , wherein the semi-crystalline water soluble polymer comprises butendiol vinylalcohol copolymer.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 29, 2023
From: INFINITE MATERIAL SOLUTIONS, LLC
To: INTERFACIAL CONSULTANTS LLC
Reel/Frame 064111/0244 →
CORRECTIVE ASSIGNMENT TO CORRECT THE EXHIBIT A WITH AMENDMENT TO ASSIGNMENT PREVIOUSLY RECORDED ON REEL 048952 FRAME 0299. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Aug 14, 2019
From: INTERFACIAL CONSULTANTS LLC
To: INFINITE MATERIAL SOLUTIONS, LLC
Reel/Frame 050048/0276 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 22, 2019
From: INTERFACIAL CONSULTANTS LLC
To: INFINITE MATERIAL SOLUTIONS, LLC
Reel/Frame 048952/0299 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 8, 2018
From: BRUNNER, PHILIP; DEPRENGER-GOTTFRIED, GAVRIEL; OCKWIG, NATHAN; CERNOHOUS, JEFFREY J.; CERNOHOUS, BRANDON J.
To: INTERFACIAL CONSULTANTS LLC
Reel/Frame 046582/0240 →
Continuity (2)
Provisional Application 62511585 · May 26, 2017
Related Publication 20180340089A1 · Nov 29, 2018