IP Library Granted Patent US 10,357,474
Granted Patent B2
US 10,357,474 · App. 15/996,101 · Granted Jul 23, 2019

Preparation and use of a composition for prevention and mitigation of the effects of radiation

Inventors: Cesar M. Compadre (Little Rock, AR); Philip Breen (Little Rock, AR); Nukhet Aykin-Burns (Little Rock, AR); Martin Hauer-Jensen (Little Rock, AR); Raul G. Enriquez (Coyoacan, MX); Sujay Kharade (Little Rock, AR); Omar Malagon (Loja, EC); Yadira Ordonez (Loja, EC); Edgar Ojeda (Loja, EC); Shraddha Thakkar (Little Rock, AR); E. Nathalie Pineda (Little Rock, AR); Darin Jones (Little Rock, AR)
Assignees: BIOVENTURES, LLC; UNIVERSIDAD TECNICA PARTICULAR DE LOJA; THE UNITED STATES OF AMERICA, AS REPRESENTED BY THE DEPARTMENT OF VETERANS AFFAIRS
A61K31/355A61K36/185A61K2236/00A61K2236/35A61K2236/55
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Quick Facts
Patent No.
US 10,357,474
App. No.
15/996,101
Granted
Jul 23, 2019
Kind
B2
Abstract

Plant extracts, compositions, pharmaceutical compositions and methods of making and using the same are provided herein. The compositions comprise γ-tocotrienol (GT3) and δ-tocotrienol (DT3) in ratios wherein the DT3 is predominate. The compositions are useful for radioprotection and radiomitigation in subjects in need thereof.

Claims (21)

1. A method of treating a subject in need of a radioprotectant or for treatment of radiation exposure, the method comprising administering an effective amount of a tocotrienol composition comprising δ-tocotrienol and γ-tocotrienol in a ratio of between 2:1 and 10:1.

2. The method of claim 1 , wherein the tocotrienol composition comprises δ-tocotrienol and γ-tocotrienol in a ratio of between 5:1 and 9:1.

3. The method of claim 1 , wherein the tocotrienol composition comprises an annatto seed extract.

4. The method of claim 3 , wherein the annatto seed extract is prepared from a method comprising:

extracting oil from annatto seeds to produce an annatto seed oil, the annatto seed oil comprising δ-tocotrienol and γ-tocotrienol, and

enriching δ-tocotrienol or γ-tocotrienol from the annatto seed oil.

5. The method of claim 4 , wherein the method comprises enriching δ-tocotrienol and γ-tocotrienol from the annatto seed oil.

6. The method of claim 1 , wherein the tocotrienol composition comprises a total tocotrienol content of between 15% and 95%.

7. The method of claim 6 , wherein the total tocotrienol content is at least 50%.

8. The method of claim 1 , wherein the tocotrienol composition comprises a total tocotrienol content of at least 100 mg/mL.

9. The method of claim 8 , wherein the total tocotrienol content is at least 500 mg/mL.

10. The method of claim 1 , wherein the tocotrienol composition comprises a tocopherol content of less than 5%.

11. The method of claim 10 , wherein the tocopherol content is less than 1%.

12. The method of claim 1 , wherein the tocotrienol composition comprises a total tocotrienol content of between 15% and 95% and a tocopherol content of less than 5%.

13. The method of claim 2 , wherein the tocotrienol composition comprises an annatto seed extract having δ-tocotrienol and γ-tocotrienol in a ratio of between 5:1 and 9:1.

14. The method of claim 1 , wherein the tocotrienol composition is a pharmaceutical composition further comprising a pharmaceutically acceptable carrier.

15. The method of claim 14 , wherein the pharmaceutical composition comprises a dosage form having a total tocotrienol content of least 1 g.

16. The method of claim 15 , wherein the pharmaceutical composition comprises an annatto seed extract.

17. The method of claim 16 , wherein the annatto seed extract is prepared from a method comprising:

extracting oil from annatto seeds to produce an annatto seed oil, the annatto seed oil comprising δ-tocotrienol and γ-tocotrienol, and

enriching δ-tocotrienol or γ-tocotrienol from the annatto seed oil.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 6, 2019
From: THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ARKANSAS
To: BIOVENTURES, LLC
Reel/Frame 048249/0609 →
CONFIRMATORY LICENSE Recorded Feb 1, 2019
From: UNIVERSITY OF ARKANSAS FOR MED SCIS
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 049809/0641 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2018
From: COMPADRE, CESAR; BREEN, PHILIP J.; AYKIN-BURNS, NUKHET; HAUER-JENSEN, MARTIN; ENRIQUEZ, RAUL G.; KHARADE, SUJAY; JONES, DARIN; THAKKAR, SHRADDHA
To: THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ARKANSAS
Reel/Frame 046728/0150 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2018
From: MALAGON, OMAR; ORDONEZ, YADIRA; OJEDA, EDGAR
To: UNIVERSIDAD TECNICA PARTICULAR DE LOJA
Reel/Frame 046728/0666 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2018
From: HAUER-JENSEN, MARTIN
To: UNITED STATES OF AMERICA, AS REPRESENTED BY THE DEPARTMENT OF VETERANS AFFAIRS
Reel/Frame 046728/0886 →
Continuity (3)
Continuation 15021376
Provisional Application 61877655 · Sep 13, 2013
Related Publication 20180271829A1 · Sep 27, 2018