Full-field statistical and characterizing method of fluid micro-explored strain for alloy microstructure
The invention relates to a full-field statistical & characterizing method of fluid micro-explored strain for alloy microstructure, comprising the following steps: a. grinding and polishing the surface of an alloy sample to mirror with no grinding defects, and then determining a to-be-measured area on the surface of the alloy sample; b. utilizing a white light interferometry 3D surface profiler to perform initial morphology measurement on the surface of an alloy sample; c. utilizing an isostatic pressing technology to obtain the microstructure deformation on the surface of the alloy sample, and then utilizing a white light interferometry 3D surface profiler to perform deformed morphology measurement on the surface of the alloy sample to obtain a changing spectrum of micro morphology of the microstructures on the surface of the alloy; and d. performing trans-scale and rapid quantitative statistical distribution characterization on the morphology change before and after isostatic pressing of the microstructures in the to-be-measured area of the alloy, so as to obtain a corresponding full-field metallography. In the present invention, the sample pretreatment is simple, the analysis speed is rapid, the scanning area is large, and the requirement of high throughput trans-scale analysis can be satisfied, so as to instruct the extraction of the material metallography feature unit.
1. A full-field statistical & characterizing method of fluid micro-explored strain for alloy microstructure, comprising the following steps:
a. grinding and polishing the surface of an alloy sample to mirror with no grinding defects, and then determining a to-be-measured area on the surface of the alloy sample;
b. utilizing a white light interferometry 3D surface profiler to perform initial morphology measurement on the surface of the alloy sample to obtain the size, spacing and length-width ratio of microstructures on initial alloy surface;
c. utilizing isostatic pressing technology to obtain the microstructure deformation on the surface of the alloy sample, and then utilizing a white light interferometry 3D surface profiler to perform deformed morphology measurement on the surface of the alloy sample to obtain the size, spacing and length-width ratio of the deformed microstructures on the surface of the alloy; performing statistical analysis on the comparison between the size, spacing and length-width ratio of the microstructures on the initial alloy surface and those of the microstructures on the deformed alloy surface to obtain deformation data on the surface of the alloy, and mapping to obtain the deformation strength of the microstructures on the surface of the alloy; and calculating to obtain a changing spectrum of micro morphology of the size, spacing and length-width ratio of the microstructures on the surface of the alloy base on distribution of deformation strength of the microstructures on the surface of the alloy;
d. performing trans-scale and rapid quantitative statistical distribution characterization on the morphology change before and after isostatic pressing of the microstructures in the to-be-measured area of the alloy, so as to obtain a corresponding full-field metallographic spectrum.
2. The full-field statistical & characterizing method of fluid micro-explored strain for alloy microstructure of claim 1 , wherein the alloy sample is prepared based on the requirement of metallography analysis.
3. The full-field statistical & characterizing method of fluid micro-explored strain for alloy microstructure of claim 1 , wherein in step a, the size of the to-be-measured area is 1˜25 mm×1˜25 mm.
4. The full-field statistical & characterizing method of fluid micro-explored strain for alloy microstructure of claim 1 , wherein in steps b and c, analysis method in measuring software of the white light interferometry 3D surface profiler is set to be a surface scanning mode, and scanned area is larger than the to-be-measured area.
5. The full-field statistical & characterizing method of fluid micro-explored strain for alloy microstructure of claim 1 , wherein in steps b and c, the white light interferometry 3D surface profiler performs multiple scanning directly to obtain morphology change and the distributed digital signals of the surface of the alloy sample.
6. The full-field statistical & characterizing method of fluid micro-explored strain for alloy microstructure of claim 1 , wherein in step c, the isostatic pressing technology is as follows: the alloy sample is placed in an isostatic pressing machine, a pressure of 50-200 MPa is applied in room temperature for 10-30 minutes, thereby enabling the microstructures on the surface of the alloy sample to form a vertical elastic plastic deformation.
7. The full-field statistical & characterizing method of fluid micro-explored strain for alloy microstructure of claim 6 , wherein the pressure transmission medium in the isostatic pressing machine is liquid or gas which can effectively transmit pressure and has no corrosion and pollution to the to-be-measured sample.
8. The full-field statistical & characterizing method of fluid micro-explored strain for alloy microstructure of claim 1 , wherein in step d, the changing spectrum of micro morphology obtained in step c is converted to a data matrix form; with the data matrix as a mapping map, the isostatic pressing deformation data corresponding to the to-be-measured area are respectively calculated, thereby realizing rapid and trans-scale quantitative statistics and characterization analysis of metallography of the microstructures in the to-be-measured area.