IP Library Granted Patent US 11,742,117
Granted Patent B2
US 11,742,117 · App. 16/003,428 · Granted Aug 29, 2023

Iron nitride permanent magnet and technique for forming iron nitride permanent magnet

Inventors: Jian-Ping Wang (Shoreview, MN); Shihai He (Fremont, CA); Yanfeng Jiang (Minneapolis, MN)
Assignee: Regents of the University of Minnesota
H01F1/01B22D11/0622B22D11/0651B32B15/011C21D1/76C22C38/001C23C8/26C23C8/80H01F1/047H01F7/021H01F41/0253H01F41/0273
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Quick Facts
Patent No.
US 11,742,117
App. No.
16/003,428
Granted
Aug 29, 2023
Kind
B2
Abstract

A permanent magnet may include a Fe 16 N 2 phase constitution. In some examples, the permanent magnet may be formed by a technique that includes straining an iron wire or sheet comprising at least one iron crystal in a direction substantially parallel to a <001> crystal axis of the iron crystal; nitridizing the iron wire or sheet to form a nitridized iron wire or sheet; annealing the nitridized iron wire or sheet to form a Fe 16 N 2 phase constitution in at least a portion of the nitridized iron wire or sheet; and pressing the nitridized iron wires and sheets to form bulk permanent magnet.

Claims (21)

1. A permanent magnet comprising a Fe 16 N 2 phase constitution, wherein the permanent magnet is thicker than 1 millimeter in its smallest dimension, wherein the permanent magnet has an energy product of greater than about 30 MGOe.

2. The permanent magnet of claim 1 , wherein the permanent magnet has an energy product of greater than about 60 MGOe.

3. The permanent magnet of claim 2 , wherein the permanent magnet has an energy product of greater than about 65 MGOe.

4. The permanent magnet of claim 3 , wherein the permanent magnet has an energy product of greater than about 100 MGOe.

5. The permanent magnet of claim 2 , wherein the permanent magnet has an energy product of between about 60 MGOe and about 135 MGOe.

6. The permanent magnet of claim 1 , further comprising at least one magnetic domain wall pinning site.

7. The permanent magnet of claim 1 , further comprising a phase stabilization dopant element comprising at least one of Ti, Co, Ta, Ni, Mn, Zr, Mo, Nb, Nd, Ga, Ge, C, B, Si, P, Cr, Cu, or Zn.

8. The permanent magnet of claim 1 , wherein the permanent magnet further comprises a Fe 8 N phase constitution.

9. The permanent magnet of claim 1 , wherein the permanent magnet consists essentially of the Fe 16 N 2 phase constitution.

10. The permanent magnet of claim 1 , wherein the permanent magnet comprises a wire comprising the Fe 16 N 2 phase constitution.

11. The permanent magnet of claim 10 , wherein the wire defines a major axis extending from a first end of the wire to a second end of the wire, wherein the wire comprises at least one body centered tetragonal (bct) iron nitride crystal, and wherein a <001> axis of the at least one bct iron nitride crystal is parallel to the major axis of the wire.

12. The permanent magnet of claim 1 , further comprising a sheet comprising the Fe 16 N 2 phase constitution.

13. The permanent magnet of claim 12 , wherein the sheet defines a major axis extending from a first end of the sheet to a second end of the sheet, wherein the sheet comprises at least one body centered tetragonal (bct) iron nitride crystal, and wherein a <001> axis of the at least one bct iron nitride crystal is parallel to the major axis of the sheet.

14. The permanent magnet of claim 1 , wherein the permanent magnet is thicker than 10 millimeters.

15. The permanent magnet of claim 1 , wherein the permanent magnet comprises at least one body centered tetragonal (bct) iron crystal unit cell elongated along a <001> axis between about 0.3% and about 7% compared to an unstrained iron body centered cubic (bcc) crystal unit cell.

16. The permanent magnet of claim 1 , wherein the permanent magnet comprises between about 8 and about 12 at % N.

17. A permanent magnet comprising a Fe 16 N 2 phase constitution, wherein the permanent magnet has an energy product of greater than about 60 MGOe.

18. The permanent magnet of claim 17 , further comprising at least one magnetic domain wall pinning site.

19. The permanent magnet of claim 17 , further comprising a phase stabilization dopant element comprising at least one of Ti, Co, Ta, Ni, Mn, Zr, Mo, Nb, Nd, Ga, Ge, C, B, Si, P, Cr, Cu, or Zn.

20. The permanent magnet of claim 17 , wherein the permanent magnet further comprises a Fe 8 N phase constitution.

21. The permanent magnet of claim 17 , wherein the permanent magnet consists essentially of the phase constitution.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 7, 2024
From: WANG, JIAN-PING; HE, SHIHAI; JIANG, YANFENG
To: REGENTS OF THE UNIVERSITY OF MINNESOTA
Reel/Frame 066400/0669 →
CONFIRMATORY LICENSE Recorded Jan 2, 2024
From: REGENTS OF UNIVERSITY OF MINNESOTA
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 066173/0989 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 18, 2018
From: WANG, JIAN-PING; HE, SHIHAI; JIANG, YANFENG
To: REGENTS OF THE UNIVERSITY OF MINNESOTA
Reel/Frame 046379/0935 →
Continuity (3)
Division 14238835
Provisional Application 61524423 · Aug 17, 2011
Related Publication 20180294078A1 · Oct 11, 2018