IP Library Granted Patent US 10,793,777
Granted Patent B2
US 10,793,777 · App. 16/032,708 · Granted Oct 6, 2020

Low density closed cell composite aerogel foam and articles including same

Inventors: Jeffrey Nash (Cincinnati, OH); Michael Glenn Markesbery (Cincinnati, OH); Rithvik Venna (Broadview Heights, OH)
Assignee: LUKLA INC.
C09K21/02B01J13/0091B32B5/18C01B33/159C08J9/0066C08J9/35C08J2201/03C08J2205/026C08J2205/052C08J2309/02C08J2323/06C08J2323/08C08J2333/00C08J2367/00C08J2375/04
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Quick Facts
Patent No.
US 10,793,777
App. No.
16/032,708
Granted
Oct 6, 2020
Kind
B2
Abstract

A composite foam is provided having silica aerogel particles dispersed in a closed cell polymeric foam. The silica aerogel particles are included in a volume fraction between 2 and 60%, and the composite foam has a thermal conductivity of 40 kW/mK or less and a density of 60 kg/m 3 or less. In another embodiment, a composite foam is provided having a perforated closed cell polymeric foam and 2-60% hydrophobic silica aerogel particles by volume with a particle size distribution of 1 to 50 μm, where the composite foam has a thermal conductivity of 30 kW/mK or less, a density of 20-45 kg/m 3 , and an air permeability of 20-40 cubic feet per minute.

Claims (32)

1. A composite foam comprising:

silica aerogel particles dispersed in a closed cell polymeric foam,

wherein the composite foam includes the silica aerogel particles in a volume fraction between 2 and 60%, and has a thermal conductivity of 40 kW/mK or less and a density of 60 kg/m 3 or less, and is perforated with an air permeability of 5-60 cubic feet per minute.

2. The composite foam of claim 1 , wherein the density is 50 kg/m 3 or less.

3. The composite foam of claim 1 , wherein the density is 20-45 kg/m 3 .

4. The composite foam of claim 1 , wherein the density is 30-40 kg/m 3 .

5. The composite foam of claim 1 , wherein the thermal conductivity is 30 kW/mK or less.

6. The composite foam of claim 1 , wherein the silica aerogel particles are hydrophobic.

7. The composite foam of claim 6 , wherein a water absorption of the composite foam is 0.1% by volume or less.

8. The composite foam of claim 1 , wherein the composite foam has an average thickness between 1.5 to 6 mm.

9. The composite foam of claim 1 , wherein the composite foam includes perforations having a diameter of 1 mm or less.

10. The composite foam of claim 1 , wherein the silica aerogel particles are included in a volume fraction from 3-40%.

11. The composite foam of claim 1 , wherein the silica aerogel particles have a particle size distribution of 0.1-100 microns.

12. The composite foam of claim 1 , wherein the silica aerogel particles have a particle size distribution of 0.5-70 microns.

13. The composite foam of claim 1 , wherein the silica aerogel particles have a particle size distribution of 1-50 microns.

14. The composite foam of claim 1 , wherein the silica aerogel particles have a median particle size of 2-10 microns.

15. A composite foam comprising:

silica aerogel particles dispersed in a closed cell polymeric foam,

wherein the composite foam includes the silica aerogel particles in a volume fraction between 2 and 60%, and has a thermal conductivity of 40 kW/mK or less and a density of 60 kg/m 3 or less, and the silica aerogel particles have a particle size distribution of 0.5-50 microns with a d(10) in the range of 1-3 microns, a d(90) in the range of 8-30 microns, and a d(50) in the range of 2-7 microns.

16. The composite foam of claim 1 , further comprising a flame inhibiting chemical.

17. The composite foam of claim 1 , further comprising an anti-microbial agent.

18. The composite foam of claim 1 , wherein the composite foam has a face surface and a back surface, the composite foam further comprising:

a textile laminated on at least one of the face surface or the back surface.

19. A composite foam comprising:

a perforated closed cell polymeric foam; and

2-60% hydrophobic silica aerogel particles by volume having a particle size distribution of 1 to 50 μm, wherein the silica aerogel particles have a particle size distribution with a d(10) in the range of 1-3 microns, a d(90) in the range of 8-30 microns, and a d(50) in the range of 2-7 microns,

wherein the composite foam has a thermal conductivity of 30 kW/mK or less, a density of 20-45 kg/m 3 , and an air permeability of 20-40 cubic feet per minute.

20. The composite foam of claim 19 , wherein a water absorption of the composite foam is 0.1% by volume or less.

21. The composite foam of claim 19 , wherein the composite foam has an average thickness between 1.5 to 6 mm.

22. The composite foam of claim 19 , wherein the perforated closed cell polymeric foam includes perforations having a diameter of 1 mm or less.

23. The composite foam of claim 19 , wherein the composite foam has a face surface and a back surface, the composite foam further comprising:

a textile laminated on at least one of the face surface or the back surface.

Assignments (6)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jan 23, 2024
From: ENLIGHTENMENT CAPITAL SOLUTIONS SBIC FUND, L.P., AS AGENT
To: LUKLA INC.
Reel/Frame 066364/0524 →
RELEASE OF SECURITY INTEREST Recorded Jun 1, 2021
From: VENTURE LENDING & LEASING VIII, INC.; VENTURE LENDING & LEASING IX, INC.
To: LUKLA INC.
Reel/Frame 056404/0601 →
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded May 28, 2021
From: LUKLA INC.
To: ENLIGHTENMENT CAPITAL SOLUTIONS SBIC FUND, L.P., AS AGENT
Reel/Frame 056422/0296 →
SECURITY INTEREST Recorded Nov 22, 2019
From: LUKLA INC.
To: VENTURE LENDING & LEASING IX, INC.; VENTURE LENDING & LEASING VIII, INC.
Reel/Frame 051097/0812 →
CONVERSION Recorded Apr 4, 2019
From: LUKLA LLC
To: LUKLA INC.
Reel/Frame 048806/0787 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 11, 2018
From: NASH, JEFFREY; MARKESBERY, MICHAEL GLENN; VENNA, RITHVIK
To: LUKLA LLC
Reel/Frame 046322/0397 →
Continuity (2)
Provisional Application 62531058 · Jul 11, 2017
Related Publication 20190016957A1 · Jan 17, 2019