IP Library Granted Patent US 10,898,861
Granted Patent B2
US 10,898,861 · App. 16/041,169 · Granted Jan 26, 2021

Ultrathin, conductive and fouling-resistant zwitterionic polymer films

Inventors: Minghui Wang (Quincy, MA); Karen K. Gleason (Cambridge, MA); Peter Kovacik (Oxford, GB)
Assignee: Massachusetts Institute of Technology
B01D65/08B01D67/009B01D67/0088B01D71/56B01D71/64B01D71/68B01D71/72B01D61/025B01D2321/168B01D2325/04B01D2325/18B01D2325/26C02F1/441C02F2101/12C02F2303/20
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,898,861
App. No.
16/041,169
Granted
Jan 26, 2021
Kind
B2
Abstract

Disclosed are methods of preparing antifouling coatings on reverse osmosis membranes with initiated vapor deposition or oxidative vapor deposition. The coatings enhance the stability and lifetime of membranes without sacrificing performance characteristics, such as permeability or salt retention.

Claims (25)

1. A polymer, comprising a plurality of first repeat units, and a plurality of second repeat units; wherein

each of the first repeat units is independently represented by Formula IIA:

wherein, independently for each occurrence,

R 2 is H, alkyl, halo, nitro, or cyano;

Y is a linker that does not comprise an amide bond, an ester bond, or an ether bond; and

X ⊖ is —SO 3 ⊖ or —COO ⊖ ; and

each of the second repeat units is independently represented by Formula IIB:

wherein, independently for each occurrence,

R 2 is H, alkyl, halo, nitro, or cyano.

2. The polymer of claim 1 , wherein R 2 is H.

3. The polymer of claim 1 , wherein X ⊖ is —SO 3 ⊖ .

4. The polymer of claim 1 , wherein the ratio of first repeat units to second repeat units is about 0.8:0.2.

5. The polymer of claim 1 , wherein the ratio of first repeat units to second repeat units is about 2:1.

6. A composition, wherein the composition comprises a substrate and a coating material, wherein the coating material comprises a polymer of claim 1 .

7. The composition of claim 6 , wherein the substrate comprises a polysulfone, a polyimide, or a polyamide.

8. The composition of claim 6 , wherein the substrate is a membrane.

9. The composition of claim 8 , wherein the substrate is a reverse osmosis membrane.

10. An article, comprising a composition of claim 6 ; wherein the article is incorporated into a water desalination device.

11. A method, comprising

contacting, at a first flow rate, a first sample of water with a composition of claim 6 , thereby producing a second sample of water,

wherein the first sample of water comprises a first concentration or first quantity of a substance; the second sample of water comprises a second concentration or second quantity of the substance; and the second concentration or second quantity is substantially lower than the first concentration or first quantity.

12. A method of coating a surface of a substrate, comprising the steps of:

providing a substrate;

exposing a surface of the substrate to plasma for a first period of time at a first pressure, thereby producing a conditioned surface of the substrate; and

contacting the conditioned surface of the substrate with the polymer of claim 1 , thereby producing a polymer-coated substrate.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 3, 2019
From: WANG, MINGHUI; GLEASON, KAREN K.; KOVACIK, PETER
To: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Reel/Frame 050617/0572 →
CONFIRMATORY LICENSE Recorded Jun 4, 2019
From: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 049364/0922 →
Continuity (2)
Provisional Application 62534888 · Jul 20, 2017
Related Publication 20190022594A1 · Jan 24, 2019