IP Library Granted Patent US 10,702,863
Granted Patent B2
US 10,702,863 · App. 16/044,642 · Granted Jul 7, 2020

Water softening compositions

Inventors: Geoffrey A. Brown (Overland Park, KS); Kristopher Lee Shelite (Moundridge, KS); Darlene R. Linscott (Kansas City, MO); Jerry L. Poe (Hutchinson, KS)
Assignee: Compass Minerals America Inc.
B01J49/05B01J39/07B01J49/53B01J49/60C02F1/42C02F1/683C02F2001/425C02F2303/16Y02W10/37
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Quick Facts
Patent No.
US 10,702,863
App. No.
16/044,642
Granted
Jul 7, 2020
Kind
B2
Abstract

Novel water softening products and methods of treating hard water are provided. The products comprise a salt and a metal chelating agent. The products are useful for regenerating ion exchange material in a water softening system and providing softened water containing both sodium and potassium ions, while having dramatically increased efficiencies over prior art products.

Claims (18)

1. A product capable of regenerating an ion exchange material in a water softening system by replenishing said ion exchange material with sodium and/or potassium ions and removing calcium and/or magnesium ions from said ion exchange material, said product consisting essentially of a metal chelating agent intermixed with a salt, wherein:

said metal chelating agent is selected from the group consisting of sodium citrate, potassium citrate, sodium succinate, potassium succinate, aspartate, maleate, ethylenediamine tetraacetate, ethylene glycol tetraacetate, polymerized amino acids, 1,2-bis(o-aminophenoxy)ethane-N,N,N′,N′-tetraacetate, sulfonated polycarboxylate copolymers, polymethacrylate, and mixtures thereof, and is present at levels of less than about 75 ppm, based on said salt; and

said salt is selected from the group consisting of NaCl, KCl, K 2 SO 4 , NaHCO 3 , Na 2 SO 4 , NaH 2 PO 4 , KHCO 3 , KH 2 PO 4 , K 2 HPO 4 , K 3 PO 4 , Na 3 PO 4 , Na 2 CO 3 , K 2 CO 3 , and mixtures thereof,

said product being a solid.

2. An aqueous dispersion or solution capable of regenerating an ion exchange material in a water softening system by replenishing said ion exchange material with sodium and/or potassium ions and removing calcium and/or magnesium ions from said ion exchange material, said aqueous dispersion or solution consisting essentially of a metal chelating agent and a salt, wherein:

said metal chelating agent is selected from the group consisting of sodium citrate, potassium citrate, sodium succinate, potassium succinate, aspartate, maleate, ethylenediamine tetraacetate, ethylene glycol tetraacetate, polymerized amino acids, 1,2-bis(o-aminophenoxy)ethane-N,N,N′,N′-tetraacetate, sulfonated polycarboxylate copolymers, polymethacrylate, and mixtures thereof, and is present at levels of less than about 75 ppm, based on said salt; and

said salt is selected from the group consisting of NaCl, KCl, K 2 SO 4 , NaHCO 3 , Na 2 SO 4 , NaH 2 PO 4 , KHCO 3 , KH 2 PO 4 , K 2 HPO 4 , K 3 PO 4 , Na 3 PO 4 , Na 2 CO 3 , K 2 CO 3 , and mixtures thereof.

3. A product capable of regenerating an ion exchange material in a water softening system by replenishing said ion exchange material with sodium and/or potassium ions and removing calcium and/or magnesium ions from said ion exchange material, said product consisting essentially of a metal chelating agent intermixed with a salt, wherein:

said metal chelating agent is selected from the group consisting of sodium citrate, potassium citrate, sodium succinate, potassium succinate, aspartate, maleate, ethylene glycol tetraacetate, polymerized amino acids, 1,2-bis(o-aminophenoxy)ethane-N,N,N′,N′-tetraacetate, sulfonated polycarboxylate copolymers, polymethacrylate, and mixtures thereof, and is present at levels of less than about 75 ppm, based on said salt; and

said salt is selected from the group consisting of NaCl, KCl, K 2 SO 4 , NaHCO 3 , Na 2 SO 4 , NaH 2 PO 4 , KHCO 3 , KH 2 PO 4 , K 2 HPO 4 , K 3 PO 4 , Na 3 PO 4 , Na 2 CO 3 , K 2 CO 3 , and mixtures thereof,

said product being a solid.

4. A product capable of regenerating an ion exchange material in a water softening system by replenishing said ion exchange material with sodium and/or potassium ions and removing calcium and/or magnesium ions from said ion exchange material, said product consisting essentially of a metal chelating agent intermixed with a salt, wherein:

said metal chelating agent is selected from the group consisting of sodium citrate, potassium citrate, sodium succinate, potassium succinate, aspartate, maleate, ethylenediamine tetraacetate, ethylene glycol tetraacetate, polymerized amino acids, 1,2-bis(o-aminophenoxy)ethane-N,N,N′,N′-tetraacetate, sulfonated polycarboxylate copolymers, polymethacrylate, and mixtures thereof, and is present at levels of less than about 75 ppm, based on said salt; and

said salt is selected from the group consisting of K 2 SO 4 , NaHCO 3 , Na 2 SO 4 , NaH 2 PO 4 , KHCO 3 , KH 2 PO 4 , K 2 HPO 4 , K 3 PO 4 , Na 3 PO 4 , Na 2 CO 3 , K 2 CO 3 , and mixtures thereof,

said product being a solid.

5. An aqueous dispersion or solution capable of regenerating an ion exchange material in a water softening system by replenishing said ion exchange material with sodium and/or potassium ions and removing calcium and/or magnesium ions from said ion exchange material, said aqueous dispersion or solution consisting essentially of a metal chelating agent and a salt, wherein:

said metal chelating agent is selected from the group consisting of sodium citrate, potassium citrate, sodium succinate, potassium succinate, aspartate, maleate, ethylenediamine tetraacetate, ethylene glycol tetraacetate, polymerized amino acids, 1,2-bis(o-aminophenoxy)ethane-N,N,N′,N′-tetraacetate, sulfonated polycarboxylate copolymers, polymethacrylate, and mixtures thereof, and is present at levels of less than about 75 ppm, based on said salt; and

said salt is selected from the group consisting of K 2 SO 4 , NaHCO 3 , Na 2 SO 4 , NaH 2 PO 4 , KHCO 3 , KH 2 PO 4 , K 2 HPO 4 , K 3 PO 4 , Na 3 PO 4 , Na 2 CO 3 , K 2 CO 3 , and mixtures thereof.

Assignments (2)
PATENT SECURITY AGREEMENT Recorded Jan 3, 2020
From: COMPASS MINERALS AMERICA INC.; COMPASS MINERALS OGDEN INC.; COMPASS MINERALS USA INC.
To: JPMORGAN CHASE BANK, N.A., AS AGENT
Reel/Frame 051463/0197 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 25, 2018
From: BROWN, GEOFFREY A.; SHELITE, KRISTOPHER LEE; LINSCOTT, DARLENE R.; POE, JERRY L.
To: COMPASS MINERALS AMERICA INC.
Reel/Frame 046453/0710 →
Continuity (3)
Continuation 14461058 · Aug 15, 2014
Provisional Application 61866406 · Aug 15, 2013
Related Publication 20180326411A1 · Nov 15, 2018