IP Library Granted Patent US 11,376,657
Granted Patent B2
US 11,376,657 · App. 16/048,032 · Granted Jul 5, 2022

Porous materials via freeze-casting of metal salt solutions

Inventors: Michael Bagge-Hansen (San Leandro, CA); Patrick G. Campbell (Oakland, CA); Jeffrey Colvin (Pleasanton, CA); Sergei Kucheyev (Oakland, CA); Thomas E. Felter (Livermore, CA)
Assignees: Lawrence Livermore National Security, LLC; National Technology & Engineering Solutions of Sandia, LLC
B22F1/054B22F1/052B22F1/0545B22F1/07B22F3/11B22F9/026B22F9/082B22F9/24B22F9/30C01G3/02C01G3/10C01G5/00C22C1/0425C22C1/0466C22C1/08B22F2009/084B22F2009/0824B22F2009/0832B22F2009/0844B22F2009/0864B22F2201/013B22F2201/20B22F2202/03B22F2301/10B22F2301/255B22F2304/05B22F2304/10B22F2998/10B22F2999/00B82Y40/00C01P2004/60C01P2004/61C01P2006/10C01P2006/14
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,376,657
App. No.
16/048,032
Granted
Jul 5, 2022
Kind
B2
Abstract

Disclosed here is a method for making a nanoporous material, comprising aerosolizing a solution comprising at least one metal salt and at least one solvent to obtain an aerosol, freezing the aerosol to obtain a frozen aerosol, and drying the frozen aerosol to obtain a nanoporous metal compound material. Further, the nanoporous metal compound material can be reduced to obtain a nanoporous metal material.

Claims (9)

1. A composition, comprising:

a nanoporous metal salt material that comprises nanoporous particles or foams having a mean diameter of about 100 microns or less, wherein the nanoporous metal salt material comprises an elemental metal and a salt, the elemental metal is silver, the nanoporous metal salt material has a porosity of at least about 30 percent, and the nanoporous metal salt material has a density of about 1000 mg/cc or less.

2. The composition of claim 1 , wherein the nanoporous particles or foams comprise a network of interconnected ligaments and struts having a mean diameter of about 1000 nm or less.

3. The composition of claim 1 , wherein the nanoporous metal salt material has a porosity of at least about 50%.

4. The composition of claim 1 , wherein the nanoporous metal salt material has a density of about 100 mg/cc or less.

5. The composition of claim 1 , wherein the nanoporous metal salt material has a porosity of at least about 80 percent.

6. The composition of claim 1 , wherein a mean diameter of the nanoporous particles or foams is about 200 nm or less.

7. The composition of claim 1 , wherein at least about 30 percent of the nanoporous particles or foams have diameters that are within about 70 percent to 130 percent of the mean diameter.

8. The composition of claim 1 , wherein at least about 30 percent of the nanoporous particles or foams have diameters that are within about 1-5 microns, 5-10 microns, 10-20 microns, 20-30 microns, or 30-50 microns.

Assignments (2)
CONFIRMATORY LICENSE (SEE DOCUMENT FOR DETAILS) Recorded Sep 16, 2020
From: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 053798/0205 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 31, 2018
From: BAGGE-HANSEN, MICHAEL; COLVIN, JEFFREY D.; KUCHEYEV, SERGEI; CAMPBELL, PATRICK G.
To: LAWRENCE LIVERMORE NATIONAL SECURITY, LLC
Reel/Frame 046509/0516 →
Continuity (2)
Division 14741334 · Jun 16, 2015
Related Publication 20180354030A1 · Dec 13, 2018