IP Library Granted Patent US 11,248,344
Granted Patent B2
US 11,248,344 · App. 16/067,234 · Granted Feb 15, 2022

Method for producing cellulose pulp, cellulose pulp and use thereof, paper

Inventors: Otávio Mambrim Filho (Aracruz, BR); Leonardo Alves De Melo (São José dos Campos, BR)
Assignee: Suzano S.A.
D21H11/20D21C3/02D21C5/00D21C9/10D21C9/12D21C9/123D21C9/18D21H11/04D21H11/12D21H17/005D21H17/21D21H17/28D21H21/10D21H21/18D21H23/04
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Quick Facts
Patent No.
US 11,248,344
App. No.
16/067,234
Granted
Feb 15, 2022
Kind
B2
Abstract

The present invention relates to an enhanced process for the production of cellulose pulps with increased quality and applicability of said pulps, especially their physical resistance properties and degree of resistance to drainage, through an enzymatic treatment step comprised in the production process of said cellulose pulp, concomitantly with the polymer dosage based on carbohydrates.

Claims (43)

1. Process for producing cellulose pulp from cellulosic feedstock characterized by comprising the steps of:

a) treating the cellulosic feedstock through a chemical or semi-chemical pulping process to produce brown cellulose pulp;

b) bleaching the brown cellulose pulp through a bleaching sequence to obtain a white slurry pulp;

c) adding a starch to the white slurry pulp, wherein the dosage of said starch ranges from 2 to 12 kg/ton of cellulose pulp;

d) adding at least one enzyme to the white slurry pulp which is already doped with the starch to form a doped white slurry pulp, wherein the addition of the at least one enzyme (EZ) takes place according to the following conditions:

i. reaction temperature between 40 and 90° C.;

ii. reaction pH between 3.0 and 9.0;

iii. reaction time between 10 and 300 minutes;

iv. enzyme amount between 10-200 g of the at least one enzyme per ton of cellulose pulp;

e) conveying the doped white slurry pulp to and through a reaction tower before a drying machine; and

f) drying the doped white slurry pulp, and denaturing the at least one enzyme, to obtain the cellulose pulp;

wherein the at least one enzyme comprises a cellulase; and

wherein the cellulose pulp has a zeta potential from about 5 to about 10 percent less than a pulp prepared in an otherwise identical manner but without the addition of starch and without the addition of enzyme.

2. Process according to claim 1 , wherein the cellulosic feedstock is a vegetable fiber.

3. Process according to claim 2 , wherein the vegetable fiber is a hardwood fiber.

4. Process according to claim 1 , wherein the pulping process is a Kraft process.

5. Process according to claim 1 , wherein bleaching comprises using an ECF or TCF bleaching sequence.

6. Process according to claim 1 , wherein the addition of the at least one enzyme (EZ) takes place according to the following conditions:

i. reaction temperature between 50 and 80° C.;

ii. reaction pH between 3.5 and 8.0;

iii. reaction time between 30 and 120 minutes;

iv. enzyme amount between 20-100 g of the at least one enzyme per ton of cellulose pulp.

7. Process for producing cellulose pulp from cellulosic feedstock characterized by comprising the steps of:

a) treating the cellulosic feedstock through a chemical or semi-chemical pulping process to produce brown cellulose pulp;

b) bleaching the brown cellulose pulp through a bleaching sequence to obtain a white slurry pulp;

c) adding at least one enzyme to the white slurry pulp, wherein the addition of the at least one enzyme (EZ) takes place according to the following conditions:

i. reaction temperature between 40 and 90° C.;

ii. reaction pH between 3.0 and 9.0;

iii. reaction time between 10 and 300 minutes;

iv. enzyme amount between 10-200 g of the at least one enzyme per ton of cellulose pulp;

d) adding a starch to the white slurry pulp already doped with the at least one enzyme to form a doped white slurry pulp, wherein the dosage of said starch ranges from 2 to 12 kg/ton of cellulose pulp;

e) conveying the doped white slurry pulp to and through a reaction tower before a drying machine; and

f) drying the doped white slurry pulp, and denaturing the at least one enzyme, to obtain the cellulose pulp;

wherein the at least one enzyme comprises a cellulase; and

wherein the cellulose pulp has a zeta potential from about 5 to about 10 percent less than a pulp prepared in an otherwise identical manner but without the addition of starch and without the addition of enzyme.

8. Process according to claim 7 , wherein the cellulosic feedstock comprises a vegetable hardwood fiber.

9. Process according to claim 8 , wherein the vegetable fiber is a eucalyptus fiber.

10. Process according to claim 7 wherein the pulping process is a Kraft process.

11. Process according to claim 7 wherein the addition of the at least one enzyme (EZ) takes place according to the following conditions:

i. reaction temperature between 50 and 80° C.;

ii. reaction pH between 3.5 and 8.0;

iii. reaction time between 30 and 120 minutes;

iv. enzyme amount between 20-100 g of the at least one enzyme per ton of cellulose pulp.

Assignments (2)
MERGER AND CHANGE OF NAME Recorded Nov 11, 2019
From: FIBRIA CELULOSE S.A.; SUZANO S.A.
To: SUZANO S.A.
Reel/Frame 051071/0461 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 6, 2018
From: MAMBRIM FILHO, OTÁVIO; ALVES DE MELO, LEONARDO
To: FIBRIA CELULOSE S.A.
Reel/Frame 047416/0759 →
Priority Claims (1)
BR 102015032911-3 · Dec 29, 2015 · national
Continuity (1)
Related Publication 20190062999A1 · Feb 28, 2019