IP Library Granted Patent US 10,434,486
Granted Patent B2
US 10,434,486 · App. 16/072,052 · Granted Oct 8, 2019

Device for producing particles and method for producing particles

Inventor: Yo Doya (Tokyo, JP)
Assignee: Tsukishima Kikai Co., Ltd.
B01J19/0066B01D9/005B01D9/02B01F3/08B01F5/0065B01F5/10B01F7/16B01F7/26B01J10/00B01J14/00B01J19/00B01J19/1837C01F7/34C01F11/18C01G9/02C07C227/42C07C229/08B01D2009/0086B01F2005/004B01F2005/0017B01J2204/002B01J2219/00166B01J2219/185B01J2219/1943
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Quick Facts
Patent No.
US 10,434,486
App. No.
16/072,052
Granted
Oct 8, 2019
Kind
B2
Abstract

A method of producing particles by bringing plural dissimilar materials A and B into contact with each other includes feeding a liquid into a reactor from a first end portion of the reactor such that the liquid flows along the inner peripheral surface of the reactor and generating a vortex flow toward a second end portion in the reactor by the feed of the liquid; disposing a flow-assisting blade capable of rotating around the central axis line in the reactor and rotating the flow-assisting blade; and injecting materials to be contacted A and B into the reactor, discharging a contacted liquid from the second end portion of the reactor, and generating the particles in the contacted liquid.

Claims (16)

1. A method of producing particles by bringing plural dissimilar materials into contact with each other, the method comprising:

feeding a liquid into a reactor from a first end portion of the reactor such that the liquid flows along an inner peripheral surface of the reactor and generating a vortex flow toward a second end portion in the reactor by the feeding of the liquid;

disposing a flow-assisting blade capable of rotating around a central axis line of the reactor and rotating the flow-assisting blade; and

injecting materials to be contacted into the reactor, discharging a contacted liquid from the second end portion of the reactor, and generating particles in the contacted liquid;

wherein the flow-assisting blade has a radius r and wherein the reactor has an inner radius R, and wherein a ratio r/R of the radius r of the flow-assisting blade to the inner radius R of the reactor is ¼ to ¾;

wherein an inlet for the liquid into the reactor has a cross-sectional area of A, and the liquid has an inflow rate Q into the reactor of 0.5 A to 10 A×60×10 3 ; and

wherein an average flow rate of the liquid at the inlet is Vv, and the flow-assisting blade is rotated at a speed that is ½ Vv or more.

2. The method of producing particles according to claim 1 , wherein all or part of the contacted liquid discharged from the second end portion of the reactor is fed into the reactor from the first end portion of the reactor such that the liquid flows along the inner peripheral surface of the reactor.

3. The method of producing particles according to claim 2 , wherein part of the contacted liquid is extracted from a circulation system that transfers the contacted liquid discharged from the second end portion of the reactor to the first end portion of the reactor, and the particles are recovered by solid-liquid separation.

4. The method of producing particles according to claim 1 , wherein the liquid is fed into the reactor from the first end portion at an inflow velocity of 0.5 m/sec or more.

5. The method of producing particles according to claim 1 , wherein the reactor has a ratio L/D of 2 or more of the longitudinal length L to the diameter D of an internal space of the reactor.

6. The method of producing particles according to claim 1 , wherein the flow-assisting blade has a disk shape intersecting with the central axis line of the reactor.

7. The method of producing particles according to claim 1 , wherein the flow-assisting blade has a disk shape having a concave-convex portion in a periphery thereof.

8. The method of producing particles according to claim 1 , wherein the flow-assisting blade has a disk-shaped body intersecting the central axis line of the reactor and a protrusion protruding to the second side at least in a periphery of the disk-shaped body and intersecting a circle having a center on the central axis line.

9. The method of producing particles according to claim 1 , wherein the flow-assisting blade is located closer to the first end portion of the reactor than where the liquid is fed in the first end portion of the reactor.

10. The method of producing particles according to claim 1 , wherein a position at which the materials to be contacted is injected, is disposed outboard from the flow-assisting blade in the direction of the radius around the central axis line in the reactor.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 24, 2025
From: TSUKISHIMA HOLDINGS CO.,LTD.
To: TSUKISHIMA KIKAI CO.,LTD.
Reel/Frame 070301/0675 →
CHANGE OF NAME Recorded Feb 19, 2025
From: TSUKISHIMA KIKAI CO.,LTD.
To: TSUKISHIMA HOLDINGS CO.,LTD.
Reel/Frame 070255/0308 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 27, 2018
From: DOYA, YO
To: TSUKISHIMA KIKAI CO., LTD.
Reel/Frame 046480/0486 →
Priority Claims (1)
JP 2016-013593 · Jan 27, 2016 · national
Continuity (1)
Related Publication 20190022551A1 · Jan 24, 2019