IP Library Granted Patent US 11,247,976
Granted Patent B2
US 11,247,976 · App. 16/097,541 · Granted Feb 15, 2022

Synthetic ligands that modulate the activity of the RhlR quorum sensing receptor

Inventors: Helen Blackwell (Middleton, WI); Michelle E. Boursier (Madison, WI); Joseph D. Moore (Wayne, PA)
Assignee: Wisconsin Alumni Research Foundation
C07D307/33C07C201/00C07C233/06C07C233/32C07C233/58C07C233/60C07C233/61C07C235/22C07D207/09C07D207/273C07D307/14C07D307/22C07D333/36C07C2601/04C07C2601/08
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Quick Facts
Patent No.
US 11,247,976
App. No.
16/097,541
Granted
Feb 15, 2022
Kind
B2
Abstract

RhlR modulators including agonist and antagonists which are useful for modulating QS phenotypes in Gram-negative bacteria. Certain compounds of general formula A-W-HG having various carbocyclic ad heterocyclic head groups (HG) and various tail groups (A), where —W— is —CO—NH—, —SO 2 —NH—, —CO—NH—CH 2 —, or —SO 2 —NH—CH 2 — are RhlR agonists or antagonists. The compounds are useful in methods of modulating quorum sensing in Gram-negative bacteria, particularly in Pseudomonas . Compositions including certain RhlR modulators are useful for decreasing the virulence of Gram-negative bacteria. Pharmaceutical compositions comprising certain RhlR modulators are useful for treatment of infections of Gram-negative bacteria.

Claims (37)

1. A compound of formula:

A-W-HG

where:

—W— is —CO—NH—, —SO 2 —NH—, —CO—NH—CH 2 —, or —SO 2 —NH—CH 2 —;

A is selected from cyclobutyl, and —CH 2 —cyclopropyll and

HG is selected from the group of moieties of formula:

where:

X is CH 2

Y is O or S and

Z is C=O or CH(OH).

2. The compound of claim 1 , wherein X=CH 2 , Y=O and Z=CO or CH(OH).

3. The compound of claim 1 which is:

4. The compound of claim 1 which is:

5. The compound of claim 2 , wherein W is —CO—NH—.

6. The compound of claim 1 , wherein W is —CO—NH—.

7. The compound of claim 1 , wherein HG is:

8. The compound of claim 7 , wherein A is cyclopropyl, cyclobutyl, or CH 2 cyclopropy.

9. The compound of claim 8 , wherein W is —CO—NH—.

10. A compound of formula:

A-W-HG

where:

—W— is —CO—NH—, —SO 2 —NH—, —CO—NH—CH 2 —, or —SO 2 —NH—CH 2 —;

A is selected from cyclopropyl, cyclobutyl, and —CH 2 —cyclopropyl; and

HG is selected from the group of moieties of formula:

where:

X is CH 2

Y is S; and

Z is C=O or CH(OH).

11. The compound of claim 10 , wherein X=CH 2 ; Y=S;

and Z=CO.

12. The compound of claim 10 , wherein A is cyclobutyl or —CH 2 —cyclopropyl.

13. The compound of claim 11 , wherein W is —CO—NH—.

14. The compound of claim 10 , wherein W is —CO—NH—.

15. A method for modulating RhIR of a Gram-negative bacterium which comprises contacting the bacterium with one or more compounds of claim 1 .

16. A method of treating an infection of a Gram-negative bacterium by administering to an individual in need of treatment a therapeutically effective amount of a compound of claim 1 .

17. A method of treating an infection of a Gram-negative bacterium by administering to an individual in need of treatment a therapeutically effective amount of a compound of claim 10 .

18. A method for modulating RhIR of a Gram-negative bacterium which comprises contacting the bacterium with one or more compounds of claim 10 .

Assignments (2)
CONFIRMATORY LICENSE Recorded Dec 4, 2018
From: UNIVERSITY OF WISCONSIN-MADISON
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 047714/0088 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 30, 2018
From: BLACKWELL, HELEN; BOURSIER, MICHELLE; MOORE, JOSEPH
To: WISCONSIN ALUMNI RESEARCH FOUNDATION
Reel/Frame 047633/0541 →
Continuity (3)
Provisional Application 62376291 · Aug 17, 2016
Provisional Application 62329942 · Apr 29, 2016
Related Publication 20190144407A1 · May 16, 2019