IP Library Granted Patent US 10,906,899
Granted Patent B2
US 10,906,899 · App. 16/099,969 · Granted Feb 2, 2021

Bicyclic fused pyrazole derivatives for the treatment of RSV

Inventors: Richard K. Plemper (Decatur, GA); Eddy Lee (Alpharetta, GA); John Vernachio (Alpharetta, GA); Elyse Bourque (L'etang-du Nord, CA)
Assignee: GEORGIA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
C07D471/04A61K31/437A61K31/444A61P31/12C07D519/00C12N2760/18511
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Quick Facts
Patent No.
US 10,906,899
App. No.
16/099,969
Granted
Feb 2, 2021
Kind
B2
Abstract

Disclosed herein are compounds and compositions for treating or inhibiting RSV and related members of the pneumovirus and paramyxovirus families such as human metapneumovirus, mumps virus, human parainfluenzaviruses, and Nipah and hendra virus, and methods of treatment or prevention thereof.

Claims (49)

1. A method of inhibiting RSV, comprising administering to a patient in need thereof, an effective amount of a compound of Formula 1b:

or a pharmaceutically acceptable salt, diastereomer, or enantiomer thereof, wherein:

R 0 is a monocyclic or bicyclic heteroaryl-alkyl having at least three carbon atoms and to three heteroatoms selected from the group consisting of O, S, and N, wherein said heteroaryl is substituted with Cl, F, or methoxy;

R 1 and R b together form a double bond;

R 2 is phenyl-alkyl, wherein the phenyl is optionally substituted with methoxy;

R 3 is a monocyclic or bicyclic heteroaryl having one to three heteroatoms selected from the group consisting of O, S, and N, wherein the heteroaryl is optionally substituted with alkoxy, alkyl, oxycycloalkyl, Cl, or F;

R 4 and R 5 together form a carbonyl;

R 6 and R 8 together form a double bond;

R 7 is alkyl or aryl optionally substituted with —R c or —OR c ; and

R a is selected from the group consisting of —R c , —OR c , —N(R c ) 2 , —SR c , —SO 2 R c , —SO 2 N(R c ) 2 ; —C(O)R c , OC(O)R c , —COOR c , —C(O)N(R c ) 2 , —OC(O)N(R c ) 2 , —N(R c )C(O), —N(R c )C(O)N(R c ) 2 , —F, —Cl, —Br, —I, —CN, and —NO 2 ;

wherein R c is selected from the group consisting of hydrogen, C 1-8 alkyl, C 3-8 cycloalkyl, a monocyclic or bicyclic heterocyclyl having from two to eight carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N, C 6-12 aryl, a monocyclic or bicyclic heteroaryl having from three to twelve carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N, C 1-8 alkyl-C 3-8 cycloalkyl, a monocyclic or bicyclic heterocyclyl-alkyl having from three to sixteen carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N, C 1-8 alkyl-C 6-12 aryl, and a monocyclic or bicyclic heteroaryl-alkyl having from four to twenty carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N.

2. The method according to claim 1 , wherein R 7 is C 6 aryl.

3. The method according to claim 1 , wherein R 7 has the formula:

4. The method according to claim 1 , wherein R 7 has the formula:

5. The method according to claim 1 , wherein R 3 is a monocyclic or bicyclic heteroaryl having from three to twelve carbon atoms.

6. The method according to claim 1 , wherein R a is hydrogen.

7. The method according to claim 1 , wherein R 7 is C 1-8 alkyl.

8. The method according to claim 1 , wherein R 7 is methyl.

9. The method according to claim 1 , wherein R 2 is an unsubstituted phenyl-alkyl.

10. The method according to claim 1 , wherein R 0 is CH 2 -heteroaryl.

11. The method according to claim 1 , wherein R 0 is CH 2 -furan-2-yl.

12. The method according to claim 1 , wherein R 3 has the formula:

13. The method according to claim 1 , wherein R 3 has the formula:

14. A method of treating an RSV infection, comprising administering to a patient in need thereof an effective amount of a compound of Formula 1b:

or a pharmaceutically acceptable salt, diastereomer, or enantiomer thereof, wherein:

R 0 is a monocyclic or bicyclic heteroaryl-alkyl having at least three carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N, wherein said heteroaryl is substituted with Cl, F, or methoxy,

R 1 and R b together form a double bond;

R 2 is a phenyl-alkyl, wherein the phenyl is optionally substituted with methoxy;

R 3 is a monocyclic or bicyclic heteroaryl having one to three heteroatoms selected from the group consisting of O, S, and N, wherein the heteroaryl is optionally substituted with alkoxy, alkyl, oxycycloalkyl, Cl, or F;

R 4 and R 5 together form a carbonyl;

R 6 and W together form a double bond;

R 7 is alkyl or aryl optionally substituted with —R c or —OR c ; and

R a is selected from the group consisting of —R c , —OR c ′, —N(R c ) 2 , —SR c , —SO 2 R c , —SO 2 N(R c ) 2 —C(O)R c , OC(O)R c , —COOR c , —C(O)N(R c ) 2 , —OC(O)N(R c ) 2 , —N(R c )C(O), —N(R c )C(O)N(R c ) 2 , —F, —Cl, —Br, —I, —CN, and —NO 2 ;

wherein R c is selected from the group consisting of hydrogen, C 1-8 alkyl, C 3-8 cycloalkyl, a monocyclic or bicyclic heterocyclyl having from two to eight carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N, C 6-12 aryl, a monocyclic or bicyclic heteroaryl having from three to twelve carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N, C 1-8 alkyl-C 3-8 cycloalkyl, a monocyclic or bicyclic heterocyclyl-alkyl having from three to sixteen carbon atoms and one to three heteroatoms selected from the group consisting of 0, S, and N, C 1-8 alkyl-C 6-12 aryl, and a monocyclic or bicyclic heteroaryl-alkyl having from four to twenty carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N.

15. The method of treating an RSV infection according to claim 14 wherein the compound is administered via a route of administration selected from the group consisting of buccal, oral, intravenous, inhalation, intradermal, intramuscular, topical, subcutaneous, rectal, vaginal, parenteral, pulmonary, intranasal, and ophthalmic.

16. A compound of Formula 1b:

or a pharmaceutically acceptable salt, diastereomer, or enantiomer thereof, wherein:

R 0 is a monocyclic or bicyclic heteroaryl-alkyl having at least three carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N, wherein said heteroaryl is substituted with Cl, F, or methoxy,

R 1 and R b together form a double bond;

R 2 is a phenyl-alkyl, wherein the phenyl is optionally substituted with methoxy;

R 3 is a monocyclic or bicyclic heteroaryl having one to three heteroatoms selected from the group consisting of O, S, and N, wherein the heteroaryl is optionally substituted with alkoxy, alkyl, oxycycloalkyl, Cl, or F;

R 4 and R 5 together form a carbonyl;

R 6 and W together form a double bond;

R 7 is alkyl or aryl optionally substituted with —R c or —OR c ; and

R a is selected from the group consisting of —R c , —OR c ′, —N(R c ) 2 , —SR c , —SO 2 R c , —SO 2 N(R c ) 2 —C(O)R c , OC(O)R c , —COOR c , —C(O)N(R c ) 2 , —OC(O)N(R c ) 2 , —N(R c )C(O), —N(R c )C(O)N(R c ) 2 , —F, —Cl, —Br, —I, —CN, and —NO 2 ;

wherein R c is selected from the group consisting of hydrogen, C 1-8 alkyl, C 3-8 cycloalkyl, a monocyclic or bicyclic heterocyclyl having from two to eight carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N, C 6-12 aryl, a monocyclic or bicyclic heteroaryl having from three to twelve carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N, C 1-8 alkyl-C 3-8 cycloalkyl, a monocyclic or bicyclic heterocyclyl-alkyl having from three to sixteen carbon atoms and one to three heteroatoms selected from the group consisting of 0, S, and N, C 1-8 alkyl-C 6-12 aryl, and a monocyclic or bicyclic heteroaryl-alkyl having from four to twenty carbon atoms and one to three heteroatoms selected from the group consisting of O, S, and N.

17. The compound according to claim 16 wherein the compound is selected from the group consisting of:

18. A pharmaceutical composition comprising the compound of claim 16 and a pharmaceutically acceptable carrier, vehicle, or excipient.

19. The pharmaceutical composition according to claim 18 wherein the compound is selected from the group consisting of:

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 18, 2020
From: PLEMPER, RICHARD K.
To: GEORGIA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
Reel/Frame 054410/0870 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 18, 2020
From: LEE, EDDY; VERNACHIO, JOHN; BOURQUE, ELYSE
To: GEORGIA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
Reel/Frame 054411/0066 →
CONFIRMATORY LICENSE Recorded Apr 23, 2019
From: GEORGIA STATE UNIVERSITY
To: NATIONAL INSTITUTES OF HEALTH (NIH), U.S. DEPT. OF HEALTH AND HUMAN SERVICES (DHHS), U.S. GOVERNMENT
Reel/Frame 048973/0758 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 5, 2019
From: VAXART, INC.
To: GEORGIA STATE UNIVERSITY RESEARCH FOUNDATION, INC.
Reel/Frame 048499/0333 →
Continuity (3)
Provisional Application 62359894 · Jul 8, 2016
Provisional Application 62333992 · May 10, 2016
Related Publication 20190144441A1 · May 16, 2019