IP Library Granted Patent US 10,514,361
Granted Patent B2
US 10,514,361 · App. 16/107,792 · Granted Dec 24, 2019

Tattletale ion-implanted nanoparticles

Inventors: Timothy J. Boyle (Albuquerque, NM); Khalid Mikhiel Hattar (Albuquerque, NM); Fernando Henry Garzon (Santa Fe, NM); Stephen J. Bauer (Albuquerque, NM)
Assignees: National Technology & Engineering Solutions of Sandia, LLC; STC.UNM
G01N27/622G01K3/00H01J37/08B82Y15/00B82Y40/00C04B41/0027C04B2235/3218C04B2235/3225C04B2235/3229H01J2237/31701
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Quick Facts
Patent No.
US 10,514,361
App. No.
16/107,792
Granted
Dec 24, 2019
Kind
B2
Abstract

Ion-doped metal or ceramic nanoparticles can be added into, for example, a component that upon exposure to an environmental stimulus, will release the ion and ‘tattle’ on any impending destruction.

Claims (20)

1. A tattletale nanoparticle, comprising an ion-implanted nanoparticle that releases the implanted ion in response to a stimulus, and detecting the released implanted ions.

2. The tattletale nanoparticle of claim 1 , wherein the nanoparticle is implanted to a dose, of greater than 1 e 15 ions/cm 2 .

3. The tattletale nanoparticle of claim 1 , wherein the nanoparticle comprises a ceramic nanoparticle.

4. The tattletale nanoparticle of claim 3 , wherein the ceramic nanoparticle comprises beohmite, yttria, or ceria.

5. The tattletale nanoparticle of claim 1 , wherein the nanoparticle comprises a metal nanoparticle.

6. The tattletale nanoparticle of claim 1 , wherein the implanted ion comprises a noble gas.

7. The tattletale nanoparticle of claim 1 , wherein the implanted ion comprises an ionizable gas.

8. The tattletale nanoparticle of claim 1 , wherein the implanted ion comprises a reactive dopant or controlled ion alloy.

9. The tattletale nanoparticle of claim 1 , wherein the stimulus comprises a physical stimulus.

10. The tattletale nanoparticle of claim 9 , wherein the physical stimulus comprises heating the nanoparticle to above a release temperature.

11. The tattletale nanoparticle of claim 9 , wherein the physical stimulus comprises mechanical crushing.

12. The tattletale nanoparticle of claim 1 , wherein the stimulus comprises a chemical stimulus.

13. A method for non-destructive testing, comprising:

providing a plurality of ion-implanted metal or ceramic nanoparticles in a component under test,

exposing the component to an environmental stimulus, thereby causing the implanted ion to be released in response to the environmental stimulus, and

detecting the released implanted ions.

14. The method of claim 13 , wherein the environmental stimulus comprises a physical stimulus.

15. The method of claim 13 , wherein the environmental stimulus comprises a chemical stimulus.

16. The method of claim 13 , wherein the released implanted ions are detected with a mass spectrometer.

17. The method of claim 16 , wherein the mass spectrometer comprises a sublimation pumped mass spectrometer.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 2, 2019
From: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC; STC.UNM
Reel/Frame 048773/0001 →
CONFIRMATORY LICENSE Recorded Nov 19, 2018
From: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 047535/0726 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 13, 2018
From: BOYLE, TIMOTHY J.; HATTAR, KHALID MIKHIEL; GARZON, FERNANDO HENRY; BAUER, STEPHEN J.
To: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
Reel/Frame 047508/0456 →
CONFIRMATORY LICENSE Recorded Oct 16, 2018
From: NATIONAL TECHNOLOGY & ENGINEERING SOLUTIONS OF SANDIA, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 047240/0110 →
Continuity (2)
Provisional Application 62551336 · Aug 29, 2017
Related Publication 20190064111A1 · Feb 28, 2019