Carbon nanotube sensing system, carbon nanotube dew point hygrometer, method of use thereof and method of forming a carbon nanotube dew point hygrometer
View Patent ↗A system, a method of use, and a Carbon Nanotube (CNT) condensation sensor for determining a dew point and/or ice point is provided. For example, a sensing system may include a thermal device configured to generate heating or cooling to change a temperature of a surface, a temperature sensor for measuring the temperature of the surface, a controller configured to control the thermal device, a carbon nanotube (CNT) condensation sensor mounted on the surface having a moisture sensitive resistance and a processor configured to determine one or more parameters based on the moisture sensitive resistance of the CNT condensation sensor and the temperature measured by the temperature sensor. The one or more parameter can be used to determine the dew point and/or ice point. A method for forming a carbon nanotube (CNT) condensation sensor is also provided.
1. A method for making a carbon nanotube (CNT) condensation sensor comprising:
placing at least one carbon nanotube in an acid solution generating a dispersion;
applying mechanical energy to the dispersion with the at least one carbon nanotube for a first predetermined time;
heating the dispersion with the at least one carbon nanotube to a first predetermined temperature for a second predetermined time;
applying mechanical energy to the dispersion with the at least one carbon nanotube while heating;
cooling the dispersion with the at least one carbon nanotube to a second predetermined temperature, after heating, for a third predetermined time;
applying mechanical energy to the dispersion with the at least one carbon nanotube while cooling;
filtering the dispersion with the at least one carbon nanotube using deionized water;
heating the filtered dispersion with the at least one carbon nanotube to a third determined temperature for a fourth predetermined time to generate a carbon nanotube powder;
placing the carbon nanotube powder in deionized water;
depositing the carbon nanotube powder in deionized water on a surface as a carbon nanotube film; and
placing the carbon nanotube film on an insulating dielectric surface, the insulating dielectric surface having a pattern of conductive material deposited on a portion of the insulating dielectric surface as an electric contact, the pattern of conductive material making contact with the carbon nanotube film.
2. The method for making a carbon nanotube (CNT) condensation sensor according to claim 1 , wherein the first predetermined time is about 1 hour to about 24 hours and the applied mechanical energy is sonication.
3. The method for making a carbon nanotube (CNT) condensation sensor according to claim 1 , wherein the first predetermined temperature is about 45° C. to about 70° C.
4. The method for making a carbon nanotube (CNT) condensation sensor according to claim 3 , wherein the second predetermined time is about 1 hour to about 24 hours.
5. The method for making a carbon nanotube (CNT) condensation sensor according to claim 3 , wherein the applying mechanical energy while heating is stirring.
6. The method for making a carbon nanotube (CNT) condensation sensor according to claim 1 , wherein the second predetermined temperature is about 20° C. to about 40° C.
7. The method for making a carbon nanotube (CNT) condensation sensor according to claim 6 , wherein the third predetermined time is about 1 day to about 5 days.
8. The method for making a carbon nanotube (CNT) condensation sensor according to claim 7 , wherein the applying mechanical energy while cooling is stirring.
9. The method for making a carbon nanotube (CNT) condensation sensor according to claim 1 , wherein the third predetermined temperature is about 70° C. to about 120° C.
10. The method for making a carbon nanotube (CNT) condensation sensor according to claim 1 , wherein the fourth predetermined time is about 1 hour to about 24 hours.
11. The method for making a carbon nanotube (CNT) condensation sensor according to claim 1 , wherein the insulating dielectric surface is selected from a group consisting of aluminum oxide and silicon dioxide.
12. The method for making a carbon nanotube (CNT) condensation sensor according to claim 1 , wherein the depositing is by filtration onto the surface, and wherein the surface is removable or dissolvable.
13. The method for making a carbon nanotube (CNT) condensation sensor according to claim 1 , wherein the acid solution comprises concentrated sulfuric acid and concentrated nitric acid.