IP Library Granted Patent US 10,883,925
Granted Patent B2
US 10,883,925 · App. 16/139,555 · Granted Jan 5, 2021

Spectrophotometer for use in explosive atmospheres

Inventors: Dorian Cauceglia (Cape Coral, FL); Thomas R. Whiteside (North Fort Myers, FL); Michael J. Goodman (Fort Myers, FL); Charlie G. Pasquariello (Fort Myers, FL); Nicholas J. Pusateri (Cape Coral, FL); Thomas F. Grassi (Fort Myers, FL)
Assignee: HF Scientific, Inc.
G01N21/251G01J3/50G01N21/255G01N21/274G01N33/1886G01N2201/0236
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Quick Facts
Patent No.
US 10,883,925
App. No.
16/139,555
Granted
Jan 5, 2021
Kind
B2
Abstract

A spectrophotometer includes an electronics compartment having disposed within, at least one light source, and at least one optical detector. A testing compartment has disposed within, an optical block having at least one fluid connection port, and a first light pipe optically coupled between the at least one light source and the optical block. A second light pipe is optically coupled between the optical block and the at least one optical detector. The testing compartment is adapted to perform spectrophotometry of a fluid sample disposed within a sample container in the optical block, and the electronics compartment is electrically isolated from the testing compartment. A spectrophotometer for use in an explosive atmosphere and a method of measuring a presence or concentration of an organic or inorganic compound in a fluid in an explosive atmosphere are also described.

Claims (45)

1. A spectrophotometer comprising:

an electronics compartment having disposed within:

at least one light source;

at least one optical detector;

a testing compartment having disposed within:

an optical block having at least one fluid connection port;

a first flexible light pipe optically coupled between said at least one light source and said optical block;

a second flexible light pipe optically coupled between said optical block and said at least one optical detector; and

wherein said testing compartment is adapted to perform spectrophotometry of a fluid sample disposed within a sample container in said optical block, wherein said fluid sample is combined with at least a first reagent, and said electronics compartment is electrically isolated from said testing compartment.

2. The spectrophotometer of claim 1 , wherein at least one of said first flexible light pipe or said second flexible light pipe comprise an acrylic plastic.

3. The spectrophotometer of claim 1 , wherein at least one of said first flexible light pipe or said second flexible light pipe comprise a PTC (push to connect) connector to mechanically coupled said at least one of said flexible light pipe or said second flexible light pipe to said optical block.

4. The spectrophotometer of claim 1 , further comprising an additional flexible light pipe to illuminate the fluid sample in said optical block with a back light for visual observation of a presence and color of the fluid sample.

5. The spectrophotometer of claim 1 , further comprising an additional flexible light pipe to illuminate the fluid sample in said optical block with a calibration light to automatically determine a presence of fluid in said optical block.

6. The spectrophotometer of claim 1 , wherein said at least one light source comprises a visible light.

7. The spectrophotometer of claim 1 , wherein said spectrophotometer comprises a colorimeter, and wherein said at least one optical detector measures an amplitude of light at a particular color.

8. The spectrophotometer of claim 1 , wherein said at least one optical detector measures an amplitude of light at a particular color of light transmission through the fluid sample disposed in said optical block and wherein said fluid sample is combined with at least a first reagent.

9. The spectrophotometer of claim 8 , wherein said spectrophotometer measures a level of chlorine in a ship's ballast water.

10. The spectrophotometer of claim 1 , wherein said first flexible light pipe is optically coupled substantially continuously over an entire optical path between said at least one light source and said optical block.

11. A spectrophotometer for use in an explosive atmosphere comprising:

a purged compartment having disposed within:

at least one light source;

at least one detector;

a non-purged compartment having disposed within:

an optical block having at least one fluid connection port;

a first flexible light pipe optically coupled between said at least one light source and said optical block;

a second flexible light pipe optically coupled between said optical block and said at least one detector; and

wherein said non-purged compartment is adapted to perform spectrophotometry of a fluid sample disposed within a sample container in said optical block, wherein said fluid sample is combined with at least a first reagent, and said purged compartment is electrically isolated from said non-purged compartment.

12. The spectrophotometer of claim 11 , wherein at least one of said first flexible light pipe or said second flexible light pipe comprise an acrylic plastic.

13. The spectrophotometer of claim 11 , wherein at least one of said first flexible light pipe or said second flexible light pipe comprise a PTC (push to connect) connector to mechanically coupled said at least one of said first light pipe or said second flexible light pipe to said optical block.

14. The spectrophotometer of claim 11 , further comprising an additional flexible light pipe to illuminate the fluid sample in said optical block with a back light for visual observation of a presence and color of the fluid sample.

15. The spectrophotometer of claim 11 , further comprising an additional flexible light pipe to illuminate the fluid sample in said optical block with a calibration light to automatically determine a presence of fluid in said optical block.

16. The spectrophotometer of claim 11 , wherein said at least one light source comprises a visible light.

17. The spectrophotometer of claim 11 , wherein said spectrophotometer comprises a colorimeter, and wherein said detector measures an amplitude of light at a particular color.

18. The spectrophotometer of claim 11 , wherein said detector measures an amplitude of light at a particular color of light transmission through the fluid sample disposed in said optical block and wherein said fluid sample is combined with at least a first reagent.

19. The spectrophotometer of claim 11 , wherein said spectrophotometer measures a level of chlorine in a ship's ballast water.

20. A method of measuring a presence or concentration of an organic or inorganic compound in a fluid in an explosive atmosphere comprising:

providing a spectrophotometer comprising: a purged compartment having disposed within: at least one light source, at least one detector, a non-purged compartment having disposed within: an optical block having at least one fluid connection port, a first flexible light pipe optically coupled between said at least one light source and said optical block, and a second flexible light pipe optically coupled between said optical block and said at least one detector;

purging said purged compartment with a positive air pressure;

filling a sample container with the fluid to be tested;

injecting at least one reagent into the fluid;

measuring an amount transmission of a light from said light source transmitted through said fluid and reagent via said first flexible light pipe and said second flexible light pipe to said detector; and

determining the presence or concentration of the organic or inorganic compound in the fluid in the explosive atmosphere based on said amount transmission of the light.

21. The method of claim 20 , wherein said step of injecting, comprises injecting at least one reagent for a detection of chlorine into said fluid, and said step of determining the presence or concentration comprises determining the presence or concentration of chlorine in a ship's ballast water.

22. The method of claim 20 , wherein said step of injecting, comprises injecting at least one reagent to determine the presence or concentration of a micro-organism into said fluid, and said step of determining the presence or concentration comprises determining the presence or concentration of the micro-organism in the fluid.

23. The method of claim 20 , wherein said step of injecting, comprises injecting at least one reagent for to determine the presence or concentration of a heavy metal into said fluid, and said step of determining the presence or concentration comprises determining the presence or concentration of the heavy metal in the fluid.

Assignments (2)
CHANGE OF NAME Recorded Mar 16, 2021
From: HF SCIENTIFIC, INC.
To: HF SCIENTIFIC, LLC
Reel/Frame 055603/0547 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 24, 2018
From: CAUCEGLIA, DORIAN; WHITESIDE, THOMAS R.; GOODMAN, MICHAEL J.; PASQUARIELLO, CHARLIE G.; PUSATERI, NICHOLAS J.; GRASSI, THOMAS F.
To: HF SCIENTIFIC, INC.
Reel/Frame 046951/0189 →
Continuity (1)
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